Protective barriers for small devices

• US 7,673,679 B2
• Filed: 09/19/2005
• Issued: 03/09/2010
• Est. Priority Date: 09/19/2005
• Status: Active Grant

• Current Assignee: Schlumberger Technology Corporation (SLB)
• Original Assignee: Schlumberger Technology Corporation (SLB)
• Inventors: Harrison, Christopher, Donzier, Eric P., Vancauwenberghe, Olivier, Chikenji, Akihito, Mullins, Oliver C., Pop, Julian J., Goodwin, Anthony Robert Holmes
• Primary Examiner(s): THOMPSON, KENNETH L
• Application Number:
  US11/231,269
• Publication Number:
  US 20070062695A1
• Time in Patent Office: 1,632 Days
• Field of Search: 166/250.11, 166/250.05, 166/66, 166/242.4, 166/250.01, 166/250.03, 731/521.8, 731/525.4, 731/525.5, 738/624.54
• US Class Current: 166/250.01
• CPC Class Codes: E21B 47/017 Protecting measuring instruments
• CPC Class Codes: E21B 47/10 Locating fluid leaks, intrusions or movements
• CPC Class Codes: E21B 49/10 using side-wall fluid samplers or testers

Abstract

Protective barriers for small devices, such as sensors, actuators, flow control devices, among others, protect the devices from erosive and/or corrosive fluids, for example, formation fluids under harsh downhole conditions. The protective barriers include protective coatings and fluid diverting structures in the fluid flow which facilitate use of the small devices in high temperature-high pressure applications with erosive and/or corrosive fluids that are often found in downhole environments.

Claims

1. A downhole fluids analysis system, comprising:

a small device adapted for downhole use to measure a property of a flowing fluid in contact with the device, wherein the small device is a micro-machined integrated device out of a substrate material; and

a protective barrier for protecting the device against the fluid, wherein the protective barrier comprises two or more layers of coating on the device and the protective barrier comprises at least a first layer of tantalum oxide and a second layer of titanium nitride.

2. The downhole fluids analysis system claimed in claim 1, wherein the tantalum oxide layer protects against corrosion and the titanium nitride layer protects against erosion, the titanium nitride layer being over the tantalum oxide layer.

3. The downhole fluids analysis system claimed in claim 2, wherein the protective barrier further comprises:

an anti-adhesion layer over the titanium nitride layer.

4. The downhole fluids analysis system claimed in claim 1, wherein the protective barrier further comprises:

an anti-adhesion layer as an outer layer on the device.

5. The downhole fluids analysis system claimed in claim 1, and further comprising

a baffle device for deflecting particulate laden flow away from the small device.

6. A downhole fluids analysis system, comprising:

a small device adapted for downhole use to measure a property of a flowing fluid in contact with the device, wherein the small device is a micro-machined integrated device out of a substrate material; and

a protective barrier for protecting the device against the fluid wherein the protective barrier comprises a baffle device for deflecting particulate laden flow away from the device and wherein the protective barrier further comprises;

a tantalum oxide layer on the device for protecting the device against corrosion and a titanium nitride layer on the device for protecting the device against erosion, the titanium nitride layer being over the tantalum oxide layer.

7. A method of downhole fluid sensing with a microelectromechanical systems device having a flexural plate comprising:

establishing fluid communication between the downhole microelectromechanical systems device, adapted for measuring fluid properties under high temperature, high pressure conditions, and subterranean formation fluids in a borehole;

providing a first protective barrier coating on the downhole microelectromechanical systems device for protecting the downhole microelectromechanical systems device against corrosion by the formation fluids by sputtering a coating of tantalum oxide on said microelectromechanical systems device;

providing a second protective barrier coating on the downhole microelectromechanical systems device for protecting the downhole microelectromechanical systems device against erosion by the formation fluids; and

surrounding the flexural plate with the subterranean formation fluids so that, when activated, the flexural plate vibrates and cause the subterranean formation fluids to move.

8. A method of downhole fluid sensing with a flexural-plate microelectromechanical systems device having a planar member with a flexural plate attached thereto along one side comprising:

establishing fluid communication between the downhole microelectromechanical systems device, adapted for measuring fluid properties under high temperature, high pressure conditions, and subterranean formation fluids in a borehole;

providing a first protective barrier coating on the downhole microelectromechanical systems device for protecting the downhole microelectromechanical systems device against corrosion by the formation fluids;

providing a second protective barrier coating on the downhole microelectromechanical systems device for protecting the downhole microelectromechanical systems device against erosion by the formation fluids by depositing by plasma vapor a coating of titanium nitride on said microelectromechanical systems devices; and

surrounding the flexural plate with the subterranean formation fluids so that, when activated, the flexural plate vibrates and cause the subterranean formation fluids to move.

9. A microelectromechanical systems device adapted for downhole fluids sensing comprising:

a microelectromechanical systems device adapted for downhole use to measure a property of a flowing fluid in contact with the microelectromechanical systems device, the microelectromechanical systems devise fabricated on a planar member; and

at least one of a first protective coating on the microelectromechanical systems device to protect the device from downhole fluid corrosion and a second protective coating on the microelectromechanical systems device to protect the device from downhole fluid erosion, said at least one of a first and a second protective coating, having a coating thickness in the range of about 0.01 micrometers to about 100 micrometers in thickness, and

said coating including at least one of an oxide, carbide and nitride of titanium.

10. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 9 wherein said at least one of a first and second protective coating on the microelectromechanical systems device encapsulating the microelectromechanical systems device comprises:

the first protective coating is composed of at least one of an oxide, carbide and nitride of tantalum encapsulating the microelectromechanical systems device; and

the second protective coating is composed of at least one of an oxide, carbide and nitride of titanium encapsulating the first protective coating and the microelectromechanical systems device.

11. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 10 and further comprising:

a third coating of anti-adhesion material encapsulating the microelectromechanical systems device.

12. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 10 wherein said first protective coating comprises:

a coating of tantalum oxide.

13. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 10 wherein at least one of said first and second protective coatings are applied by:

a process of sputtering.

14. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 10 wherein at least one of said first and second protective coatings are applied by:

a process of plasma vapor deposition.

15. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 9 wherein:

said at least one of said first and second protective coatings is applied to be approximately one micrometer in thickness.

16. A microelectromechanical systems device adapted for downhole fluids sensing as defined in claim 9 wherein:

the coating thickness of the at least one of a first and second coatings preferably is in the range of about 0.1 micrometers to about 10 micrometers in thickness.