Gas treating method and apparatus

• US 7,740,691 B2
• Filed: 01/10/2006
• Issued: 06/22/2010
• Est. Priority Date: 01/10/2006
• Status: Expired due to Fees

• Current Assignee: Valerus Field Solutions, L.P. (Snc-Lavalin Group Incorporated)
• Original Assignee: Edwin W. Cash
• Inventors: Bradley, Thomas J., Cash, Edwin A.
• Primary Examiner(s): Griffin; Walter D
• Assistant Examiner(s): ROBINSON, RENEE E
• Application Number:
  US11/329,015
• Publication Number:
  US 20070157806A1
• Time in Patent Office: 1,624 Days
• Field of Search: 952/26, 962/62, 962/65, 963/29, 963/51, 261/126
• US Class Current: 96/351
• CPC Class Codes: B01D 53/1425 Regeneration of liquid absorbents
• CPC Class Codes: B01D 53/1462 Removing mixtures of hydrogen sulfide and carbon dioxide
• CPC Class Codes: B01D 53/18 Absorbing units; Liquid distributors therefor B01D3/16, B01D3/26, B01D3/30 take precedence; packing elements B01J19/30, B01J19/32
• CPC Class Codes: C10L 3/10 Working-up natural gas or synthetic natural gas
• CPC Class Codes: C10L 3/102 of acid contaminants

Abstract

A method and apparatus for treating natural gas comprises a contactor having a manifold for spreading gas in the contactor vessel, a plurality of perforated plates above the manifold, a spray system for spraying a treating liquid into an upwardly rising column of gas and a liquid level controller for maintaining the treating liquid above the perforated plates. Gas and liquid from the contactor pass through a cooler and are then separated. A treating liquid regeneration system receives the treating liquid and flashes the liquid at low pressure to separate hydrocarbon gases, hydrocarbon liquid and treating liquid. The treating liquid is regenerated by heating and flashing off contaminant gases and is ultimately redelivered to the contactor.

Claims

1. An apparatus for treating a contaminated gas comprising:

a vessel comprising a pool of contaminant-absorbing liquid, wherein the vessel comprises a generally cylindrical high-pressure vessel operable to operate at a pressure of at least 800 pounds per square inch (psi) over atmospheric pressure;

a manifold for introducing the contaminated gas into the vessel, wherein the manifold introduces the gas into the vessel below the top level of the pool of contaminant-absorbing liquid;

at least one flow disperser contained within the vessel and positioned above the manifold and beneath the level of the pool of contaminant-absorbing liquid; and

one or more spray nozzles contained within the vessel and positioned above the level of the pool of contaminant-absorbing liquid, operable to introduce contaminant-absorbing liquid counter-current to the flow of contaminated gas in the vessel.

2. The apparatus of claim 1 wherein the manifold introduces the gas in a direction away from the flow disperser.

3. The apparatus of claim 1 wherein the flow disperser comprises a perforated plate comprising openings and operable to prevent channeling of the gas in the vessel.

4. The apparatus of claim 1 further comprising a liquid level sensor.

5. The apparatus of claim 1 further comprising one or more downcomers for maintaining the level of the pool of contaminant-absorbing liquid in the vessel, wherein the one or more downcomers deliver overflow contaminant-absorbing liquid to a sump within the vessel.

6. The apparatus of claim 1 wherein the vessel comprises a generally cylindrical high-pressure vessel less than 25 feet in height.

7. The apparatus of claim 1 wherein the contaminated gas comprises natural gas and the contaminant-absorbing liquid comprises an amine.

8. The apparatus of claim 1 wherein the vessel comprises a height of approximately 10 feet.

9. The apparatus of claim 1 wherein the contaminant-absorbing liquid comprises an amine and the quantity of the amine that circulates through the apparatus comprises no more than 30 gallons per minute per 10,000 thousand cubit feet per day (MCFD) of treated contaminated gas.

10. The apparatus of claim 1 wherein the apparatus does not include a demister.

11. An apparatus for treating a contaminated gas comprising:

a vessel comprising a pool of contaminant-absorbing liquid, wherein the vessel comprises a generally cylindrical high-pressure vessel operable to operate at a pressure of at least 800 pounds per square inch (psi) over atmospheric pressure;

a manifold for introducing the contaminated gas into the vessel, wherein the manifold introduces the gas into the vessel below the top level of the pool of contaminant-absorbing liquid;

at least one perforated plate comprising openings and operable to prevent channeling of the gas in the vessel and positioned above the manifold and beneath the level of the pool of contaminant-absorbing liquid;

a liquid level sensor;

one or more downcomers for maintaining the level of the pool of contaminant-absorbing liquid in the vessel, wherein the one or more downcomers deliver overflow contaminant-absorbing liquid to a sump within the vessel; and

one or more spray nozzles contained within the vessel and positioned above the level of the pool of contaminant-absorbing liquid, operable to introduce contaminant-absorbing liquid counter-current to the flow of contaminated gas in the vessel.

12. The apparatus of claim 11 wherein the vessel comprises a height of approximately 10 feet.

13. The apparatus of claim 11 wherein the apparatus does not include a demister.