Optical sensor and method employing half-core hollow optical waveguide

• US 7,805,028 B2
• Filed: 10/16/2008
• Issued: 09/28/2010
• Est. Priority Date: 03/25/2008
• Status: Expired due to Fees

• Current Assignee: Hewlett-Packard Development Company, L.P. (HP Inc.)
• Original Assignee: Hewlett-Packard Development Company, L.P. (HP Inc.)
• Inventors: Wang, Shih-Yuan, Li, Zhiyong, Wu, Wei, Tang, Jing, Tan, Michael
• Primary Examiner(s): Rojas; Omar
• Application Number:
  US12/253,123
• Publication Number:
  US 20090245718A1
• Time in Patent Office: 712 Days
• Field of Search: 356928-954
• US Class Current: 385/12
• CPC Class Codes: B82Y 20/00 Nanooptics, e.g. quantum optics or photonic crystals
• CPC Class Codes: G01N 2021/0346 Capillary cells; Microcells
• CPC Class Codes: G01N 2021/052 Tubular type; cavity type; multireflective
• CPC Class Codes: G01N 2021/6467 Axial flow and illumination
• CPC Class Codes: G01N 2021/7763 Sample through flow
• CPC Class Codes: G01N 2021/7783 Transmission, loss
• CPC Class Codes: G01N 21/05 Flow-through cuvettes G01N21/09 takes precedence; handling fluid samples G01N1/10
• CPC Class Codes: G01N 21/31 Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry G01N21/72 takes precedence
• CPC Class Codes: G01N 21/645 Specially adapted constructive features of fluorimeters
• CPC Class Codes: G01N 21/658 enhancement Raman, e.g. surface plasmons
• CPC Class Codes: G02B 6/02328 Hollow or gas filled core
• CPC Class Codes: G02B 6/1226 involving surface plasmon interaction

Abstract

An optical sensor, sensing system and method of sensing employ a half-core hollow optical waveguide adjacent to a surface of an optical waveguide layer of a substrate. The half-core hollow optical waveguide and the adjacent optical waveguide layer cooperatively provide both an optical path that confines and guides an optical signal and an internal hollow channel. The optical path and channel extend longitudinally along a hollow core of the half-core hollow optical waveguide. The system further includes an optical source at an input of the optical path and an optical detector at an output of the optical path. A spectroscopic interaction between an analyte material that is introduced into the channel and an optical signal propagating along the optical path determines a characteristic of the analyte material.

Claims

1. An optical sensor comprising:

an optical waveguide layer adjacent to a surface of a substrate; and

a half-core hollow optical waveguide, a half-core side of the hollow optical waveguide being adjacent to a surface of the optical waveguide layer, the half-core hollow optical waveguide and the optical waveguide layer cooperatively forming both an optical path that confines and guides an optical signal and an internal hollow channel that extend longitudinally along a hollow core of the half-core hollow optical waveguide,

wherein a spectroscopic interaction between an analyte within the channel and an optical signal propagating along the optical path determines a characteristic of the analyte.

2. The optical sensor of claim 1, wherein the analyte is a fluid flowing through the channel.

3. The optical sensor of claim 1, wherein the half-core hollow optical waveguide comprises a longitudinal portion of a bisected holey optical waveguide, the hollow core being a longitudinally bisected hole of the holey optical waveguide.

4. The optical sensor of claim 1, wherein the half-core hollow optical waveguide comprises a longitudinal portion of a bisected hollow metal channel waveguide.

5. The optical sensor of claim 1, wherein spectroscopic interaction is one or more of optical absorption, fluorescence, luminescence, and Raman scattering.

6. The optical sensor of claim 1, further comprising a Raman-active surface in the channel and within an optical field region of the optical path, wherein the spectroscopic interaction is one or more of surface enhanced Raman scattering, surface enhanced resonant Raman scattering, and surface enhanced hyper Raman scattering.

7. The optical sensor of claim 6, wherein the Raman-active surface comprises nanostructures deposited on one or both of an interior surface of the hollow core and a portion of a surface of the optical waveguide layer within the channel.

8. The optical sensor of claim 7, wherein the nanostructures comprise one or both of a metal and a metal oxide.

9. The optical sensor of claim 1, further comprising a cover layer adjacent to the optical waveguide layer on the substrate surface, the half-core hollow optical waveguide being embedded in the cover layer.

10. The optical sensor of claim 1, wherein the optical waveguide layer comprises one or more of a slab waveguide, a ridge-loaded optical waveguide and a reverse ridge-loaded optical waveguide.

11. The optical sensor of claim 1, wherein the optical waveguide layer comprises an embedded half-core hollow optical waveguide, a hollow half-core side of both half-core hollow optical waveguides being adjacent at the substrate surface along a longitudinal axis, such that the adjacent half-cores of the two hollow optical waveguides form the hollow channel.

12. The optical sensor of claim 1, further comprising:

an optical source that produces the optical signal; and

a detector that receives a response signal from an output of the optical path, the detector characterizing the spectroscopic interaction to determine the characteristic of the analyte.

21. The optical sensor of claim 1, wherein the optical waveguide layer comprises a different type of optical waveguide than a type of optical waveguide of the half-core hollow optical waveguide.

22. The optical sensor of claim 1, wherein the half-core optical waveguide comprises one of a metal channel optical waveguide, a photonic crystal optical waveguide, a photonic bandgap (PBG) optical fiber, a Bragg fiber and a holey fiber.

23. The optical sensor of claim 1, wherein the optical waveguide layer adjacent to a surface of a substrate comprises a slab waveguide.

13. An optical sensor system comprising:

an optical waveguide layer in a substrate and adjacent to a surface of the substrate;

a half-core hollow optical waveguide having a longitudinal axis and a hollow core collinear with the longitudinal axis, the half-core hollow optical waveguide cooperatively forming both an internal hollow channel and an optical path with the optical waveguide layer, the channel being within an optical field region of the optical path;

an optical source at an input of the optical path; and

an optical detector at an output of the optical path,

wherein the optical detector receives a response signal containing a spectroscopic product of an interaction within the channel between an analyte material to be analyzed and an optical signal produced by the optical source.

14. The optical sensor system of claim 13, wherein the substrate comprises a semiconductor material, the optical source and optical detector being integrated circuit components formed within the semiconductor material.

15. The optical sensor system of claim 13, wherein the substrate further comprises a microfluidic channel that introduces the analyte material into the channel.

16. The optical sensor system of claim 13, further comprising a cover layer adjacent to the surface of the substrate, the half-core hollow optical waveguide being embedded in the cover layer.

17. The optical sensor system of claim 13, further comprising a Raman-active surface in the channel and within the optical field region of the optical path, wherein the spectroscopic product is a result of one or both of surface enhanced Raman scattering (SERS) and surface enhanced resonant Raman scattering (SERRS).

18. A method of optical sensing, the method comprising:

providing an optical path formed by a half-core hollow optical waveguide adjacent to an optical waveguide layer of a substrate, the half-core hollow optical waveguide having a hollow core that cooperatively forms an internal channel with a surface of the substrate such that the channel extends along the optical path;

introducing an analyte into the channel; and

interacting an optical signal with the analyte within the channel to produce a spectroscopic response, the optical signal and the spectroscopic response being guided along the optical path,

wherein the spectroscopic response is characteristic of the analyte.

19. The method of optical sensing of claim 18, further comprising providing a Raman-active material on a surface of the channel, wherein the spectroscopic response is one of surface enhanced Raman scattering (SERS) and surface enhanced resonant Raman scattering.

20. The method of optical sensing of claim 18, wherein providing the optical path comprises:

providing a hollow core optical fiber;

embedding the hollow core optical fiber in a surface of a carrier substrate;

bisecting the hollow core optical fiber to expose the hollow core at the surface; and

bonding the carrier substrate to a surface of the optical waveguide layer, the hollow core being adjacent to the surface of the optical waveguide, such that the optical path is formed coextensive with the internal channel.