Gas chromatograph with improved thermal maintenance and process operation using microprocessor control

• US 8,015,856 B2
• Filed: 10/26/2007
• Issued: 09/13/2011
• Est. Priority Date: 09/02/2005
• Status: Active Grant

• Current Assignee: ABB Incorporated (ABB Limited)
• Original Assignee: ABB Incorporated (ABB Limited)
• Inventors: Dilbeck, Rodney Wayne, Acker, Bryan Joseph, Bailey, Max A., Hadley, Vince B., Asher, Jonathan W., Walker, Anthony P.
• Primary Examiner(s): LARKIN, DANIEL SEAN
• Application Number:
  US11/925,132
• Publication Number:
  US 20080092627A1
• Time in Patent Office: 1,418 Days
• Field of Search: 73/233.5, 73/233.6, 73/234.1, 73/234.2
• US Class Current: 73/23.35
• CPC Class Codes: G01N 2030/0095 Separation specially adapted for use outside laboratory, e.g. field sampling, portable equipments
• CPC Class Codes: G01N 2030/025 Gas chromatography
• CPC Class Codes: G01N 2030/8804 automated systems
• CPC Class Codes: G01N 2030/8881 Modular construction, specially adapted therefor
• CPC Class Codes: G01N 30/88 Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
• CPC Class Codes: Y10T 137/86558 Plural noncommunicating flow paths
• CPC Class Codes: Y10T 137/87265 Dividing into parallel flow paths with recombining
• CPC Class Codes: Y10T 137/87716 For valve having a flexible diaphragm valving member
• CPC Class Codes: Y10T 137/87764 Having fluid actuator
• CPC Class Codes: Y10T 137/87893 With fluid actuator

Abstract

A gas chromatograph controlled by a pair of microprocessors to have improved thermal maintenance and process operation. The microprocessors are operable to run independently of each other, with one microprocessor controlling heaters and other control devices and the other microprocessor running a graphical user interface. The two microprocessors are separated by a gas chromatograph assembly that includes one or more separation columns.

Claims

1. A gas chromatograph for analyzing a sample fluid, the gas chromatograph comprising:

a housing defining an enclosed volume;

an enclosure disposed in the enclosed volume of the housing and defining a thermal isolation space;

a separation device operable to separate components of the sample fluid, the separation device being disposed in the thermal isolation space;

a detector for detecting the components of the fluid, the detector being disposed in the thermal isolation space;

a heater for heating the thermal isolation space;

a first microprocessor disposed in the enclosed volume of the housing; and

a second microprocessor connected to the heater and operable to control the heater, the second microprocessor being disposed in the enclosed volume of the housing and being operable to run independently of the first microprocessor.

2. The gas chromatograph of claim 1, further comprising a temperature sensor disposed in the thermal isolation space, and wherein the second microprocessor uses a temperature signal from the temperature sensor to control the heater.

3. The gas chromatograph of claim 2, wherein the gas chromatograph further comprises memory, and wherein the second microprocessor controls the heater in accordance with a proportional-integral-derivate temperature control software routine stored in the memory and executed by the second microprocessor.

4. The gas chromatograph of claim 3, further comprising input circuitry associated with the second microprocessor, the input circuitry conditioning and digitizing the temperature signal from the temperature sensor, the digitized temperature signal being input to the second microprocessor.

5. The gas chromatograph of claim 2, wherein the second microprocessor monitors the power being used by the heater to heat the thermal isolation space and provides information about the monitored power to the first microprocessor.

6. The gas chromatograph of claim 1, further comprising:

a carrier gas line for carrying carrier gas;

a sample inlet line for carrying the sample fluid;

a valve connected to the carrier gas line and the sample inlet line and operable to inject the sample fluid into the carrier gas, the valve being disposed in the thermal isolation space;

a pressure control valve connected into the carrier gas line to regulate the pressure of carrier gas provided to the valve;

a pressure sensor for sensing the pressure of carrier gas provided to the valve, the pressure sensor being disposed in the thermal isolation space in the enclosure.

7. The gas chromatograph of claim 6, wherein the pressure control valve and the pressure sensor are connected to the second microprocessor, and wherein the second microprocessor uses a pressure signal from the pressure sensor to control the pressure control valve.

8. The gas chromatograph of claim 7, wherein the second microprocessor controls the pressure control valve in accordance with a proportional-integral-derivate pressure control software routine stored in the memory and executed by the second microprocessor.

9. The gas chromatograph of claim 7, wherein input circuitry associated with the second microprocessor conditions and digitizes the pressure signal from the pressure sensor, the digitized pressure signal being input to the second microprocessor.

10. The gas chromatograph of claim 7, wherein the second microprocessor uses pulse-width-modulated control signals to control the heater and the pressure control valve.

11. The gas chromatograph of claim 1, further comprising:

a display screen disposed in the enclosed volume of the housing and visible from the exterior of the housing; and

a graphical user interface (GUI) software routine executable by the first microprocessor to display a plurality of windows on the display screen, the windows containing information about the operation of the gas chromatograph.

12. The gas chromatograph of claim 1, further comprising:

at least one computer readable medium;

a boot-up software program stored on the at least one computer readable medium, the boot-up software program being automatically executed by the second microprocessor upon power up of the gas chromatograph to control the heater to establish a start-up value for the temperature in the thermal isolation space, the start-up value being stored on the at least one computer readable medium.

13. The gas chromatograph of claim 12, further comprising:

a carrier gas line for carrying carrier gas;

a sample inlet line for carrying the sample fluid;

a valve connected to the carrier gas line and the sample inlet line and operable to inject the sample fluid into the carrier gas, the valve being disposed in the thermal isolation space;

a pressure control valve connected into the carrier gas line to regulate the pressure of carrier gas provided to the valve; and

a pressure sensor for sensing the pressure of carrier gas provided to the valve, the pressure sensor being disposed in the thermal isolation space in the enclosure; and

wherein the pressure control valve and the pressure sensor are connected to the second microprocessor, and wherein the second microprocessor uses a pressure signal from the pressure sensor to control the pressure control valve.

14. The gas chromatograph of claim 13, wherein the boot-up software program is automatically executed by the second microprocessor upon power up of the gas chromatograph to control the pressure control valve to establish an initial value for the pressure of the carrier gas provided to the valve, the initial value being stored on the at least one computer readable medium.

15. The gas chromatograph of claim 14, wherein the at least one computer readable medium comprises first memory located separate from a second memory, the boot-up software program being stored on the first memory and the initial value for pressure of the carrier gas provided to the valve and the start-up value for the temperature in the thermal isolation space being stored on the second memory.

16. The gas chromatograph of claim 15, further comprising a circuit board secured to the valve and having the second memory mounted thereto, and wherein the separation device, the valve and the circuit board are connected together so as to form a module that is removable as a unit from the gas chromatograph.