Automated soil measurement device

• US 8,144,319 B2
• Filed: 05/06/2010
• Issued: 03/27/2012
• Est. Priority Date: 05/07/2009
• Status: Active Grant

• Current Assignee: Winfield Solutions LLC (Land O'Lakes Incorporated)
• Original Assignee: Solum, Inc. (Corteva, Inc.)
• Inventors: Strachan, John Paul, White, Justin Stewart, Koshnick, Nicholas Carleton, Preiner, Michael John
• Primary Examiner(s): Stafira, Michael P
• Application Number:
  US12/775,418
• Publication Number:
  US 20100283993A1
• Time in Patent Office: 691 Days
• Field of Search: 356244-246
• US Class Current: 356/244
• CPC Class Codes: G01N 2033/245 for agricultural purposes
• CPC Class Codes: G01N 21/00 Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light G01N3/00 - G01N19/00 take precedence
• CPC Class Codes: G01N 21/276 with alternation of sample and standard in optical path
• CPC Class Codes: G01N 21/33 using ultraviolet light G01N21/39 takes precedence
• CPC Class Codes: G01N 21/552 Attenuated total reflection
• CPC Class Codes: G01N 33/24 Earth materials G01N33/42 takes precedence

Abstract

A system and a method are disclosed for combining a soil sample and extractant in a mixing chamber to produce a liquid extractant-soil mixture. A portion of the liquid extractant-soil mixture is directed from the mixing chamber through a sample measurement chamber coupled to the mixing chamber. The sample measurement chamber is coupled to a light source so that light propagates from the light source through the portion of the liquid extractant-soil mixture to an optical detector which generates an attenuation spectrum indicating light received by the detector at different wavelengths. The sample measurement chamber may include an attenuation cell having a specified optical path between a first measurement window and a second measurement window and angular surface directing particulates in the liquid extractant-soil mixture away from the attenuation cell.

Claims

1. A measurement chamber for determining a characteristic of a liquid extractant-soil mixture, the measurement chamber comprising:

a first surface having a first orientation, the first surface including a first measurement window holder including a first measurement window allowing transmission of at least ultraviolet light;

a second surface having the first orientation, the second surface having a second measurement window holder including a second measurement window allowing transmission of at least ultraviolet light, the second measurement window having a specified distance from the first measurement window; and

a third surface having a second orientation perpendicular to the first orientation, the third surface coupled to the first surface and to the second surface; and

a first angular surface coupled to the third surface in an orientation which directs particles away from the separation between the first measurement window and the second measurement window.

2. The measurement chamber of claim 1, further comprising:

a fourth surface having the second orientation, the fourth surface coupled to the first surface and to the second surface and the fourth surface parallel to the third surface; and

a second angular surface coupled to the fourth surface in an orientation which directs air bubbles away from the separation between the first measurement window and the second measurement window.

3. The measurement chamber of claim 1, wherein the first measurement window and the second measurement window comprise quartz or fused silica windows.

4. The measurement chamber of claim 1, wherein the first measurement window and the second measurement window include a hydrophilic film.

5. The measurement chamber of claim 1, further comprising:

an optical detector coupled to the second measurement window holder, the optical detector configured to measure ultraviolet light scattered within the separation between the first measurement window and the second measurement window.

6. The measurement chamber of claim 1 coupled to a light source so that light propagating from the light source is attenuated by the liquid extractant-soil mixture and measured by an optical detector coupled to the measurement chamber, the optical detector generating an attenuation spectrum indicating light received by the detector at different wavelengths.

7. The measurement chamber of claim 6, wherein the measurement chamber receives light from the light source through the first measurement window and the optical detector is coupled to the measurement chamber via the second measurement window.

8. The measurement chamber of claim 1, wherein the characteristic of the liquid extractant-soil mixture comprises one or more of:

a viscosity of the liquid extractant-soil mixture, a pH of the liquid extractant-soil mixture, a temperature of the liquid extractant-soil mixture, a moisture content of the soil in the liquid extractant soil-mixture, a conductivity of the soil in the liquid extractant-soil mixture, and a reflection spectrum of the soil in the liquid extractant-soil mixture.

9. The measurement chamber of claim 1, wherein the first and second measurement windows allow transmission of visible light.

10. The measurement chamber of claim 1, wherein the first and second measurement windows allow transmission of near-infrared light.

11. A soil analysis device comprising:

a measurement chamber for determining a characteristic of a liquid extractant-soil mixture, the measurement chamber comprising;

a first surface having a first orientation, the first surface including a first measurement window holder including a first measurement window allowing transmission of at least ultraviolet light;

a second surface having the first orientation, the second surface having a second measurement window holder including a second measurement window allowing transmission of at least ultraviolet light, the second measurement window having a specified distance from the first measurement window; and

a third surface having a second orientation perpendicular to the first orientation, the third surface coupled to the first surface and to the second surface; and

a first angular surface coupled to the third surface in an orientation which directs particles away from the separation between the first measurement window and the second measurement window; and

a mixing chamber coupled to the measurement chamber, the mixing chamber configured to receive a soil sample and to receive extractant, the mixing chamber configured to produce and store the liquid soil-extractant mixture by combining the soil sample and the extractant, the mixing chamber configured to transmit the liquid soil-extractant mixture to the measurement chamber.

12. The device of claim 11, wherein the mixing chamber produces the liquid extractant-soil mixture using at least one of:

sonication, heating or chemical addition.

13. The device of claim 11, wherein the mixing chamber further comprises:

a motor coupled to a mixing shaft which enters the mixing chamber through an opening and moves responsive to power from the motor so that movement of the mixing chamber combines the soil sample and the extractant to form the liquid extractant-soil mixture.

14. The device of claim 11, wherein the measurement chamber receives the liquid extractant-soil mixture through a channel.

15. The device of claim 14, wherein the channel includes a filter configured to remove particulates from the liquid extractant-soil mixture prior to the measurement chamber receiving the liquid extractant-soil mixture.

16. The device of claim 11, wherein the mixing chamber is configured to apply centrifugal force to the liquid extractant-soil mixture prior to the measurement chamber receiving the liquid extractant-soil mixture.

17. A measurement chamber for determining a characteristic of a liquid extractant-soil mixture, the measurement chamber comprising:

a first surface having a first orientation, the first surface including a first measurement window holder including a first measurement window allowing transmission of at least visible light;

a second surface having the first orientation, the second surface having a second measurement window holder including a second measurement window allowing transmission of at least visible light, the second measurement window having a specified distance from the first measurement window; and

a third surface having a second orientation perpendicular to the first orientation, the third surface coupled to the first surface and to the second surface; and

a first angular surface coupled to the third surface in an orientation which directs particles away from the separation between the first measurement window and the second measurement window.

18. The measurement chamber of claim 17, further comprising:

an optical detector coupled to the second measurement window holder, the optical detector configured to measure visible light scattered within the separation between the first measurement window and the second measurement window.

19. A measurement chamber for determining a characteristic of a liquid extractant-soil mixture, the measurement chamber comprising:

a first surface having a first orientation, the first surface including a first measurement window holder including a first measurement window allowing transmission of at least near-infrared light;

a second surface having the first orientation, the second surface having a second measurement window holder including a second measurement window allowing transmission of at least near-infrared light, the second measurement window having a specified distance from the first measurement window; and

a third surface having a second orientation perpendicular to the first orientation, the third surface coupled to the first surface and to the second surface; and

a first angular surface coupled to the third surface in an orientation which directs particles away from the separation between the first measurement window and the second measurement window.

20. The measurement chamber of claim 19, further comprising:

an optical detector coupled to the second measurement window holder, the optical detector configured to measure near-infrared light scattered within the separation between the first measurement window and the second measurement window.