Automated soil measurement device

• US 8,325,336 B2
• Filed: 02/15/2012
• Issued: 12/04/2012
• Est. Priority Date: 05/07/2009
• Status: Active Grant

• Current Assignee: Winfield Solutions LLC (Land O'Lakes Incorporated)
• Original Assignee: Solum, Inc. (Corteva, Inc.)
• Inventors: Preiner, Michael John, Koshnick, Nicholas Carleton, White, Justin Stewart, Strachan, John Paul
• Primary Examiner(s): Stafira, Michael P
• Application Number:
  US13/397,478
• Publication Number:
  US 20120147368A1
• Time in Patent Office: 293 Days
• Field of Search: 356244-246
• US Class Current: 356/244
• CPC Class Codes: G01N 2033/245 for agricultural purposes
• CPC Class Codes: G01N 21/00 Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light G01N3/00 - G01N19/00 take precedence
• CPC Class Codes: G01N 21/276 with alternation of sample and standard in optical path
• CPC Class Codes: G01N 21/33 using ultraviolet light G01N21/39 takes precedence
• CPC Class Codes: G01N 21/552 Attenuated total reflection
• CPC Class Codes: G01N 33/24 Earth materials G01N33/42 takes precedence

Abstract

A system and a method are disclosed for combining a soil sample and extractant in a mixing chamber to produce a liquid extractant-soil mixture. A portion of the liquid extractant-soil mixture is directed from the mixing chamber through a sample measurement chamber coupled to the mixing chamber. The sample measurement chamber is coupled to a light source so that light propagates from the light source through the portion of the liquid extractant-soil mixture to an optical detector which generates an attenuation spectrum indicating light received by the detector at different wavelengths. The sample measurement chamber may include an attenuation cell having a specified optical path between a first measurement window and a second measurement window and angular surface directing particulates in the liquid extractant-soil mixture away from the attenuation cell.

Claims

1. A soil analysis device comprising:

a mixing chamber configured to receive a soil sample and to receive extractant, the mixing chamber configured to produce and store a liquid extractant-soil mixture by combining the soil sample and the extractant;

a sample measurement chamber physically coupled to the mixing chamber, the sample measurement chamber configured to receive a portion of the liquid extractant-soil mixture from the mixing chamber; and

an optical detector optically coupled to the sample measurement chamber, the optical detector configured to receive light propagating from a light source, the light attenuated by the portion of the liquid extractant-soil mixture received from the mixing chamber, the optical detector configured to generate an attenuation spectrum indicating the attenuated light received by the optical detector at different wavelengths.

2. The soil analysis device of claim 1, wherein the sample measurement chamber comprises:

an attenuation cell having a specified optical path length and receiving light from the light source, wherein the portion of the liquid extractant-soil mixture flows through the attenuation cell and attenuates light from the light source and light passing through the portion of liquid extractant-soil mixture is received by the optical detector.

3. The device of claim 2, wherein the attenuation cell receives light from the light source through a first measurement window and the optical detector is coupled to the attenuation cell via a second measurement window.

4. The device of claim 3, wherein the first measurement window and the second measurement window comprise fused silica or quartz windows.

5. The device of claim 3, wherein the first measurement window and the second measurement window include a hydrophilic film.

6. The device of claim 1, wherein the mixing chamber produces the liquid extractant-soil mixture using at least one of:

sonication, heating or chemical addition.

7. The device of claim 1, further comprising:

a motor coupled to a mixing shaft which enters the mixing chamber through an opening and moves responsive to power from the motor so that movement of the mixing chamber combines the soil sample and the extractant to form the liquid extractant-soil mixture.

8. The device of claim 1, wherein the sample measurement chamber receives the portion of the liquid extractant-soil mixture through a channel.

9. The device of claim 8, wherein the channel includes a filter configured to remove particulates from the portion of the liquid extractant-soil mixture prior to the sample measurement chamber receiving the portion of the liquid extractant-soil mixture.

10. The device of claim 1, wherein the mixing chamber is configured to apply centrifugal force to the liquid extractant-soil mixture prior to the sample measurement chamber receiving the portion of the liquid extractant-soil mixture.

11. The device of claim 1, further comprising one or more additional measurement devices coupled to the mixing chamber, the measurement devices configured to determine additional data associated with the liquid extractant-soil mixture.

12. The device of claim 11, wherein the additional data associated with the liquid extractant-soil mixture comprises one or more of:

a moisture content of the soil in the liquid extractant soil-mixture, a viscosity of the liquid extractant-soil mixture, a conductivity of the soil sample, a reflection spectrum of the soil sample and a temperature of the liquid extractant-soil mixture.

13. The device of claim 1, further comprising one or more additional measurement devices coupled to the mixing chamber, the measurement devices configured to determine data associated with the soil sample.

14. The device of claim 13, wherein the data associated with the soil sample comprises one or more of optical reflectivity measurements of the soil sample and conductivity of the soil sample.

20. The soil analysis device of claim 1, comprising

a light source optically coupled to the sample measurement chamber, the light source configured to propagate light through the portion of the liquid extractant-soil mixture received from the mixing chamber.

15. A method for measuring characteristics of a soil sample comprising the steps of:

producing a liquid extractant-soil mixture by combining the soil sample and extractant in a mixing chamber;

directing a portion of the liquid extractant-soil mixture from the mixing chamber into a sample measurement chamber physically coupled to the mixing chamber;

transmitting light from a light source through the portion of the liquid extractant-soil mixture in the sample measurement chamber; and

detecting, with an optical detector optically coupled to the sample measurement chamber, light propagating from the light source, the light attenuated by the portion of the liquid extractant-soil mixture received from the mixing chamber;

generating an absorption spectrum indicating the attenuated light received by the optical detector at different wavelengths; and

determining components of the soil sample from the attenuation spectrum.

16. The method of claim 15, wherein producing the liquid extractant-soil mixture comprises:

combining the soil sample, extractant and received chemicals in the mixing chamber.

17. The method of claim 15, further comprising the step of:

measuring characteristics of the liquid extractant-soil mixture using detectors coupled to the mixing chamber.

18. The method of claim 17, wherein the characteristics of the liquid extractant-soil mixture comprise one or more of a moisture content of a soil sample, a viscosity of the liquid extractant-soil mixture, a conductivity of the soil sample, a reflection spectrum of the soil sample, a pH of the soil sample and a temperature of the liquid extractant-soil mixture.

19. The method of claim 17, wherein the step of determining components of the soil sample from the attenuation spectrum further comprises:

determining components of the soil sample from the attenuation spectrum and the measured characteristics of the liquid extractant soil mixture.