Method of testing spiral wound modules by thermal imaging

• US 8,348,499 B2
• Filed: 10/13/2010
• Issued: 01/08/2013
• Est. Priority Date: 01/12/2010
• Status: Expired due to Fees

• Current Assignee: Dow Global Technologies LLC (Dow, Inc.)
• Original Assignee: Dow Global Technologies LLC (Dow, Inc.)
• Inventors: Jons, Steven D., Jons, William A.
• Primary Examiner(s): KAPLAN VERBITSKY, GAIL
• Application Number:
  US12/903,254
• Publication Number:
  US 20110170572A1
• Time in Patent Office: 818 Days
• Field of Search: 374/4, 374/141, 374/120, 374/121, 374/135, 374/57, 374/147, 374/167, 374/166, 374/137, 374/29, 374/30, 374/112, 250/338.1, 428/36.9
• US Class Current: 374/4
• CPC Class Codes: B01D 63/10 Spiral-wound membrane modules
• CPC Class Codes: B01D 63/107 Specific properties of the central tube or the permeate channel
• CPC Class Codes: B01D 65/102 Detection of leaks in membranes
• CPC Class Codes: B01D 65/104 Detection of leaks in membrane apparatus or modules
• CPC Class Codes: Y02A 20/131 Reverse-osmosis
• CPC Class Codes: Y10T 428/139 Open-ended, self-supporting conduit, cylinder, or tube-type article

Abstract

Various methods for testing spiral wound modules by thermal imaging are described. In a preferred embodiment, the method(s) includes flowing a gas between a scroll face and permeate collection tube of a spiral wound module and detecting temperature differences on the scroll face. Temperature differentials on the scroll face may be captured as a thermal image. The location(s) of temperature differentials on the scroll face can be correlated to defects in the module. In preferred embodiments, the subject test methods are non-destructive and can be applied to spiral wound modules in either a dry or wet condition.

Claims

1. A method for testing a spiral wound module comprising a permeate collection tube extending between two opposing ends and including a plurality of openings along its length, and at least one membrane envelope wound about the permeate collection tube and forming two opposing scroll faces, wherein the membrane envelope is in fluid communication with the openings along the permeate collection tube;

wherein the method comprises the steps of;

flowing a gas between the scroll face and permeate collection tube wherein the gas has a different temperature than the scroll face; and

detecting temperature differences on the scroll face of the spiral wound module.

2. The method of claim 1 wherein the step of flowing a gas between the scroll face and permeate collection tube comprises drawing negative pressure from the permeate collection tube.

3. The method of claim 1 wherein the step of flowing a gas between the scroll face and permeate collection tube comprises introducing a pressurized gas into the permeate collection tube.

4. The method of claim 1 wherein the difference in temperature between the gas and the scroll face of the spiral wound module is at least 5°

C.

5. The method of claim 1 wherein the step of detecting comprises obtaining a thermal image of the scroll face of the spiral wound module.

6. The method of claim 5 wherein the thermal image of the scroll face of the spiral wound module is recorded by a camera.

7. The method of claim 6 wherein the thermal image is compared with a reference standard.

8. The method of claim 6 wherein the spiral wound module comprises a plurality of membrane envelopes and wherein the thermal image is analyzed for localized inhomogeneities in temperature.

9. The method of claim 1 wherein the membrane envelope comprises a reverse osmosis or nanofiltration membrane.

10. The method of claim 1 wherein the spiral wound module comprising a plurality of membrane envelopes.