Fluid density from downhole optical measurements

• US 8,434,356 B2
• Filed: 08/18/2009
• Issued: 05/07/2013
• Est. Priority Date: 08/18/2009
• Status: Active Grant

• Current Assignee: Schlumberger Technology Corporation (SLB)
• Original Assignee: Schlumberger Technology Corporation (SLB)
• Inventors: Hsu, Kai, Indo, Kentaro, Mullins, Oliver, Hegeman, Peter S.
• Primary Examiner(s): Williams, Hezron E
• Assistant Examiner(s): NGUYEN, HOANG T
• Application Number:
  US12/543,017
• Publication Number:
  US 20110042070A1
• Time in Patent Office: 1,358 Days
• Field of Search: 731/521.8, 731/522.2, 731/522.4, 731/522.7, 731/522.8, 731/525.2, 166/250.01, 166/250.07, 166/254.2, 175/40, 175/41, 175/48, 175/50
• US Class Current: 73/152.18
• CPC Class Codes: E21B 47/113 using electrical indications; using light radiations
• CPC Class Codes: E21B 49/08 Obtaining fluid samples or testing fluids, in boreholes or wells
• CPC Class Codes: E21B 49/0875 determining specific fluid parameters
• CPC Class Codes: E21B 49/088 combined with sampling

Abstract

A system and method for determining at least one fluid characteristic of a downhole fluid sample using a downhole tool are provided. In one example, the method includes performing a calibration process that correlates optical and density sensor measurements of a fluid sample in a downhole tool at a plurality of pressures. The calibration process is performed while the fluid sample is not being agitated. At least one unknown value of a density calculation is determined based on the correlated optical sensor measurements and density sensor measurements. A second optical sensor measurement of the fluid sample is obtained while the fluid sample is being agitated. A density of the fluid sample is calculated based on the second optical sensor measurement and the at least one unknown value.

Claims

1. A method performed by a device, comprising:

measuring at least one value using a first optical sensor and density sensor of a fluid sample in a downhole tool at a plurality of pressures;

correlating the first optical sensor measurements and the density sensor measurements;

obtaining a second optical sensor measurement of the fluid sample; and

determining a density of the fluid sample based on the second optical sensor measurement and the first optical sensor measurement correlated to the density sensor measurements.

2. The method of claim 1 wherein the first optical sensor measurements and the density measurements are obtained while the fluid sample is not being agitated.

3. The method of claim 1 wherein the second optical measurement is obtained while the fluid is being agitated.

4. The method of claim 1 wherein the first optical sensor measurements and the density measurement are obtained while the fluid is not being agitated and further wherein the second optical measurement is obtained while the fluid is being agitated.

5. The method of claim 1 further comprising determining at least one unknown value of a density calculation based on the correlated optical sensor measurements and the density sensor measurements.

6. The method of claim 1 further comprising:

opening a valve coupling a first fluid flowline and a second fluid flowline to permit the fluid sample to move from the first fluid flowline into the second fluid flowline; and

closing the valve to isolate the second fluid flowline from the first fluid flowline;

moving a piston in a chamber in fluid communication with the second fluid flowline to alter the pressure of the fluid sample contained in the second fluid flowline.

7. The method of claim 5 wherein the determining at least one unknown value includes identifying a least-squares estimate of unknown values m and n.

8. The method of claim 1 further comprising calculating a compressibility of the fluid sample based on the density of the fluid sample.

9. The method of claim 1 wherein the device is a downhole tool positionable in a wellbore below Earth'"'"'s surface, and further comprising

altering the pressure of the fluid sample in the downhole tool for a first period of time until a first stopping threshold is reached while obtaining the first optical sensor measurements and the density sensor measurements.

10. The method of claim 9 further comprising calculating at least one unknown value based on the first optical sensor measurements and the density sensor measurements.

11. The method of claim 10 further comprising:

altering the pressure of the fluid sample for a second period of time until a second stopping threshold is reached;

agitating the fluid sample while the pressure is being altered for the second period of time;

obtaining the second optical sensor measurement while the fluid sample is being agitated; and

calculating a density of the fluid sample based on the second optical sensor measurement and the at least one unknown value.

12. The method of claim 11 wherein calculating the at least one unknown value includes identifying a least-squares estimate of unknown values m and n.

13. The method of claim 12 wherein calculating the density of the fluid sample is based on using the second optical sensor measurement in the equation ρ

=(OD−

n)/m, where ρ

is the density of the fluid sample and OD is an optical density.

14. The method of claim 9 wherein agitating the fluid sample includes circulating the fluid sample in a circulation flow loop in the downhole tool.

15. The method of claim 1 wherein the fluid sample is a liquid.

16. The method of claim 9 wherein altering the pressure of the fluid sample comprises decreasing the pressure.

17. The method of claim 9 wherein altering the pressure of the fluid sample comprises increasing the pressure.

18. The method of claim 9 wherein the first optical sensor measurements comprises at least one of an optical absorption and a transmittance.