System for production of ethanol and co-products with solvent washing of fermentation product

• US 8,454,802 B2
• Filed: 12/23/2009
• Issued: 06/04/2013
• Est. Priority Date: 12/23/2008
• Status: Active Grant

• Current Assignee: Poet Research Inc.
• Original Assignee: Poet Research Inc.
• Inventors: Redford, Steven G.
• Primary Examiner(s): Hopkins, Robert A
• Application Number:
  US12/646,647
• Publication Number:
  US 20100159548A1
• Time in Patent Office: 1,259 Days
• Field of Search: 203/19, 203/47, 210/768, 426/7, 435/161
• US Class Current: 203/19
• CPC Class Codes: A23K 10/37 from waste material from hydrolysates of wood or straw A23K10/32; from molasses A23K10/33
• CPC Class Codes: A23K 10/38 from distillers' or brewers' waste
• CPC Class Codes: A23K 40/20 by moulding, e.g. making cakes or briquettes
• CPC Class Codes: A23K 40/25 by extrusion
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel
• CPC Class Codes: Y02P 60/87 Re-use of by-products of food processing for fodder production

Abstract

A system for the production of ethanol and co-products is provided. The system facilitates an overall reduction in the use of energy, for example, by reducing the mass of wet solids supplied to a distillation system. The system also reduces the amount of energy used to dry the wet solids component of a fermentation product, for example, by increasing the ethanol concentration of the wet solids. The system also facilitates the recovery of co-products including bioproducts and other biochemicals extracted from components of the fermentation product. The solids component of the fermentation product may be dried and constituted into a meal that may be used for animal feed, among other uses.

Claims

1. A method for reducing the water content of a solid component prepared from a fermentation product of a fermentation process in a biorefinery that performs distillation of ethanol wherein the fermentation product provides for an aqueous-ethanolic component and a solids component, the method comprising the steps of:

(a) forming the fermentation product from milled corn;

(b) partially separating the aqueous-ethanolic component from the solids component to provide a separated solids component having a reduced amount of the aqueous-ethanol component; and

(c) conducting at least two separate addition-removal procedures thereto wherein each procedure comprises adding an ethanol solution or solvent to the separated solids component and further wherein the ethanol or solvent content of the each solution is higher than ethanol or solvent content of the aqueous-ethanol component remaining in the separated solids component and then removing at least a portion of liquid therefrom such that after each addition-removal procedure the water content in the separated solids component is lower than the prior procedure.

2. The method of claim 1 wherein the separated solids component comprises proteins derived from corn.

3. The method of claim 1 wherein the partially separating of step (b) is performed by applying at least one of positive pressure, vacuum pressure, or heat to the solids component.

4. The method of claim 1 wherein in each of the steps, the solids component is maintained below a temperature that will result in degradation of the solids component.

5. The method of claim 4 wherein the temperature is maintained below 180°

F.

6. The method of claim 5 wherein the temperature is maintained below 130°

F.

7. The method of claim 1 wherein the solids component or separated solids component comprises particulate matter, the particulate matter being separated from the respective aqueous-ethanol component prior to distillation of the aqueous-ethanol component.

8. The method of claim 1 wherein in step (b), the solids component is separated from the aqueous-ethanol component by centrifugation.

9. The method of claim 1 wherein each step is performed without raising the temperature of the slurry and the solids component above a temperature of about 180°

F.

10. The method of claim 1 wherein steps (b) and (c) are performed in a closed-loop cycle.

11. The method of claim 1 wherein the addition-removal procedures are repeated a sufficient number of times such that the removed liquid component has a water content of less than 1%.

12. A method for reducing the water content of a solid component prepared from a fermentation product of a fermentation process in a biorefinery that performs distillation of ethanol wherein the fermentation product provides for an aqueous-ethanolic component and a solids component, the method comprising the steps of:

(a) forming the fermentation product from milled corn;

(b) partially separating the aqueous-ethanolic component from the solids component to provide a separated solids component having a reduced amount of the aqueous-ethanol component; and

(c) conducting at least two separate addition-removal procedures thereto wherein each procedure comprises adding an ethanol solution and/or hexane to the separated solids component and further wherein the ethanol and/or hexane content of the each solution is higher than ethanol and/or hexane content of the aqueous-ethanol component remaining in the separated solids component and then removing at least a portion of liquid therefrom such that after each addition-removal procedure the water content in the separated solids component is lower than the prior procedure.

13. The method of claim 12 comprising performing subsequent addition-removal procedures until the removed liquid is substantially entirely ethanol.

14. The method of claim 12 wherein the aqueous-ethanol component has an ethanol-to-water ratio below the azeotropic ratio.

15. A method for reducing the water content of a solid component prepared from a fermentation product of a fermentation process in a biorefinery that performs distillation of ethanol wherein the fermentation product provides for an aqueous-ethanolic component and a solids component, the method comprising the steps of:

(a) forming the fermentation product;

(b) partially separating the aqueous-ethanolic component from the solids component to provide a separated solids component having a reduced amount of the aqueous-ethanol component; and

(c) conducting at least three separate addition-removal procedures thereto wherein each procedure comprises adding an ethanol solution to the separated solids component and further wherein the ethanol content of the each solution is higher than ethanol content of the aqueous-ethanol component remaining in the separated solids component and then removing at least a portion of liquid therefrom such that after each addition-removal procedure the water content in the separated solids component is lower than the prior procedure and such that the ethanol content of the removed liquid after at least a third addition-removal procedure is at or above 96% ethanol.