System and method for preextraction of hemicellulose through using a continuous prehydrolysis and steam explosion pretreatment process
First Claim
1. A method for pretreating cellulosic biomass feed stock comprising:
- pretreating the feed stock in a first pressurized reactor, wherein the feed stock undergoes hydrolysis in the first pressurized reactor, wherein the feed stock in the first pressurized reactor is under a gauge pressure of at least 1.5 bar;
transferring the feed stock from the first pressurized reactor to a pressurized sealing device, wherein the feed stock in the pressurized sealing device is under a gauge pressure of at least 1.5 bar;
maintaining a vapor phase in the first pressurized reactor by injecting steam into the first pressurized reactor, wherein the injected steam provides heat energy to the feedstock in the first pressurized reactor;
washing the feed stock in a downstream region of the first pressurized reactor or in the pressurized sealing device;
draining a liquid including dissolved hemi-cellulosic material extracted from the feed stock from at least one of the first pressurized reactor and the pressurized sealing device;
discharging the feed stock from the pressurized sealing device through a second pressurized coupling to a second pressurized reactor, wherein the feed stock is maintained at a higher pressure in the second pressurized reactor than in the first pressurized reactor;
in the second pressurized reactor, infusing cells of the feed stock with steam or water vapor by injecting steam or water vapor into the second pressurized reactor, andrapidly releasing a pressure applied to the feed stock infused with water to cause steam expansion in the cells of the feed stock and refine the feed stock.
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Abstract
A method including: pretreating biomass feed stock in a first pressurized reactor, wherein the feed stock undergoes hydrolysis in the first pressurized reactor; discharging the feed stock from the first pressurized reactor to a pressurized sealing device having a first pressurized coupling to a feedstock discharge port of the first pressurized reactor; maintaining a vapor phase in the first pressurized reactor by injecting steam; washing the feed stock; draining dissolved hemi-cellulosic material extracted from the feed stock; discharging the feed stock from the pressurized sealing device through a second pressurized coupling to a second pressurized reactor; in the second pressurized reactor, infusing cells of the feed stock with steam or water vapor, and rapidly releasing the pressure applied to the feed stock to cause steam expansion in the cells of the feed stock and refine the feed stock.
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Citations
21 Claims
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1. A method for pretreating cellulosic biomass feed stock comprising:
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pretreating the feed stock in a first pressurized reactor, wherein the feed stock undergoes hydrolysis in the first pressurized reactor, wherein the feed stock in the first pressurized reactor is under a gauge pressure of at least 1.5 bar; transferring the feed stock from the first pressurized reactor to a pressurized sealing device, wherein the feed stock in the pressurized sealing device is under a gauge pressure of at least 1.5 bar; maintaining a vapor phase in the first pressurized reactor by injecting steam into the first pressurized reactor, wherein the injected steam provides heat energy to the feedstock in the first pressurized reactor; washing the feed stock in a downstream region of the first pressurized reactor or in the pressurized sealing device; draining a liquid including dissolved hemi-cellulosic material extracted from the feed stock from at least one of the first pressurized reactor and the pressurized sealing device; discharging the feed stock from the pressurized sealing device through a second pressurized coupling to a second pressurized reactor, wherein the feed stock is maintained at a higher pressure in the second pressurized reactor than in the first pressurized reactor; in the second pressurized reactor, infusing cells of the feed stock with steam or water vapor by injecting steam or water vapor into the second pressurized reactor, and rapidly releasing a pressure applied to the feed stock infused with water to cause steam expansion in the cells of the feed stock and refine the feed stock. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10)
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11. A method including:
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pretreating biomass feed stock in a first pressurized reactor, wherein the feed stock undergoes hydrolysis in the first pressurized reactor; discharging the feed stock from the first pressurized reactor to a pressurized sealing device having a first pressurized coupling to a feedstock discharge port of the first pressurized reactor; maintaining a vapor phase in the first pressurized reactor by injecting steam into the first pressurized reactor; washing the feed stock in or downstream of the first pressurized reactor; draining dissolved hemi-cellulosic material extracted from the feed stock; discharging the feed stock from the pressurized sealing device through a second pressurized coupling to a second pressurized reactor; in the second pressurized reactor, infusing cells of the feed stock with steam or water vapor; maintaining the feed stock under a pressure of at least 150 kilopascals as the feed stock moves through the first pressurized reactor, from the first pressurized reactor to the second pressurized reactor, and through the second pressurized reactor, and subjecting the feed stock with the infused cells to a rapid pressure release to cause expand and burst the cells of the feed stock. - View Dependent Claims (12, 13, 14, 15, 16, 17, 18, 19, 20, 21)
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Specification