Ethanol production process using cold traps

• US 8,524,473 B2
• Filed: 07/17/2012
• Issued: 09/03/2013
• Est. Priority Date: 10/28/2002
• Status: Active Grant

• Current Assignee: Little Sioux Corn Processors
• Original Assignee: Little Sioux Corn Processors
• Inventors: Hammond, Neal, Prevost, John
• Primary Examiner(s): Marx, Irene
• Application Number:
  US13/551,247
• Publication Number:
  US 20120283422A1
• Time in Patent Office: 413 Days
• Field of Search: None
• US Class Current: 435/161
• CPC Class Codes: C11B 1/00 Production of fats or fatty oils from raw materials
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel

Abstract

An improved ethanol production process providing novel stillage treatment is disclosed wherein the stillage is separated into four value added product streams that are subjected to drying conditions reducing or eliminating volatization of any VOC'"'"'s in the product streams.

Claims

1. In an ethanol production process wherein a starch-containing feedstock is hydrolyzed to produce ethanol and whole stillage, the improvement to which comprises:

(a) separating the whole stillage to produce a protein-containing solids stream and a solubles stream, and

(b) drying the protein-containing solids stream in a spray dryer operating at an inlet hot air temperature of less than about 450°

F. and an exhaust temperature of between about 140°

F. and about 170°

F. for a period of time to produce a protein rich product having a water content of less than about 15% by weight, wherein drying the protein-containing solids stream produces a volatile organic compound stream comprised of volatile organic compounds and water vapor;

(c) passing the volatile organic compound stream through a cold trap to produce a water-volatile organic compound liquid; and

(d) passing the water-volatile organic compound liquid through a separator to separate the volatile organic compound and the water to form a volatile organic compound product.

2. The process according to claim 1 wherein the protein-containing solids stream is subjected to an inlet drying temperature less than about 450°

F. and the period of time is less than about 3 minutes.

3. The process according to claim 2 wherein the protein rich product has a product temperature less than about 160°

F. upon completion of the drying.

4. The process according to claim 1 further comprising the steps of:

(e) filtering the solubles stream through a microfilter to form a carotenoid containing retentate and a nutrient containing permeate, and

(f) drying the carotenoid containing retentate for a period of time to produce a carotenoid containing product having a water content of less than about 15% by weight.

5. The process according to claim 4 wherein the carotenoid containing retentate is subjected to an inlet drying temperature less than about 450°

F. and the period of time is less than about 3 minutes.

6. The process according to claim 4 further comprising the steps of:

(g) filtering the nutrient containing permeate through an ultrafilter to form a protein and yeast rich retentate and a nutrient rich permeate, and

(h) drying the protein and yeast rich retentate for a period of time to produce a protein and yeast rich containing product having a water content of less than about 15% by weight.

7. The process according to claim 6 wherein drying the protein and yeast rich retentate produces a volatile organic compound rich gaseous stream and the volatile organic compound rich gaseous stream is processed through a cold trap to produce a liquid volatile organic compound stream and the liquid volatile organic compound stream is treated to remove water contained in the liquid volatile organic compound stream to form a volatile organic compound product.

8. The process according to claim 6 further comprising drying the nutrient rich permeate at a temperature less than about 450°

F. and for a period of time to produce a vitamin and mineral rich product having a water content of less than about 15% by weight.

9. The process according to claim 8 further comprising the steps of passing any volatile organic compounds released during drying of the nutrient rich permeate through a cold trap to produce a water-volatile organic compound liquid;

and passing the water-volatile organic compound liquid through a separator to separate the volatile organic compound and the water to form a volatile organic compound product.

10. The process according to claim 1, wherein the separator is a filter.

11. The process according to claim 9, wherein the separator is a filter.