Carbon dioxide corn germ oil extraction system

• US 8,603,328 B2
• Filed: 10/28/2009
• Issued: 12/10/2013
• Est. Priority Date: 08/18/2006
• Status: Expired due to Fees

• Current Assignee: MOR Supercritical, LLC
• Original Assignee: MOR Supercritical, LLC
• Inventors: DeLine, Kenneth E., Claycamp, Daniel L., Fetherston, Daniel, Marentis, Rodger T.
• Primary Examiner(s): DRODGE, JOSEPH W
• Application Number:
  US12/589,816
• Publication Number:
  US 20100044205A1
• Time in Patent Office: 1,504 Days
• Field of Search: 210/149, 210/175, 210/259, 210/511, 210/634, 210/85, 210/90, 210/96.1, 210/143, 210/180, 210/182, 210/637, 210/639, 210/808, 554 11- 16, 426/425
• US Class Current: 210/85
• CPC Class Codes: C11B 1/104 using super critical gases or vapours
• CPC Class Codes: C12P 7/06 Ethanol, i.e. non-beverage
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel
• CPC Class Codes: Y02P 20/54 using solvents, e.g. supercritical solvents or ionic liquids

Abstract

Supercritical carbon dioxide extraction of corn germ oil from corn germ utilizing extraction conditions adapted to a dry corn fractionation ethanol production process.

Claims

1. A corn oil extraction system, comprising:

a) a at least one extractor vessel;

b) an amount of corn germ having a substantially fixed location inside said at least one extractor vessel;

c) an amount of supercritical carbon dioxide fluidly engaged to said amount of corn germ inside said at least one extractor vessel;

d) a heat source which maintains said amount of supercritical carbon dioxide at a temperature in a range of about 85°

C. and about 120°

C.;

e) a pressure generator which maintains said amount of supercritical carbon dioxide at a pressure in a range of about 8500 psi and about 12,000 psi;

f) an effluent monitor which monitors an amount of corn oil solubilized in said amount of supercritical carbon dioxide;

g) a temperature adjustment element coupled to said heat source; and

h) a pressure adjustment element coupled to said pressure generator, said temperature adjustment element and said pressure adjustment element responsive to said effluent monitor, said temperature adjustment element and said pressure adjustment element adjusting said temperature and said pressure based on monitoring said amount of corn oil solubilized in said amount of supercritical carbon dioxide to achieve a preselected corn germ extraction efficiency profile.

2. The corn oil extraction system of claim 1, wherein said temperature adjustment element and said pressure adjustment element continuously adjust said temperature of said amount of supercritical carbon dioxide between about 85°

C. and about 120°

C. and said pressure of said amount of carbon dioxide between 8,500 psi and 12,000 psi to to extract said amount of corn germ with said amount of supercritical carbon dioxide at a ratio of between about 2;

1 to about 6;

1 (wt/wt) to said amount of corn oil having a yield of greater than 18 percent of the weight of said corn germ.

3. The corn oil extraction system of claim 2 wherein said ratio comprises about 2:

1 to about 5;

1 (wt/wt).

4. The corn oil extraction system of claim 3 further comprising a duration of time of between about 10 and about 30 minutes.

5. The corn oil extraction system of claim 1, further comprising a comminutor which reduces particle size of said amount of corn germ fluidically engaged to said amount of supercritical carbon dioxide in said corn germ extraction zone to less than about 30 mesh.

6. The corn oil extraction system of claim 1, further comprising a water removal element coupled to said amount of supercritical carbon dioxide which reduces an amount of water in said amount of supercritical carbon dioxide which fluidically engages said amount of corn germ inside of said corn germ extraction zone to between about one percent by weight to about seven percent by weight.

7. The corn oil extraction system of claim 6, wherein said amount of corn germ located inside said corn germ extraction zone contains an amount of water in the range of about ten percent by weight to about fourteen percent by weight prior to fluidic engagement with said amount of supercritical carbon dioxide inside said corn germ extraction zone.

8. The corn oil extraction system of claim 7, further comprising an amount of extracted corn germ generated by fluidic engagement with said amount of supercritical carbon dioxide inside said corn germ extraction zone, wherein said amount of extracted corn germ contains an amount of water in the range of about one percent by weight to about seven percent by weight.

9. The corn oil extraction system of claim 8, further comprising an amount of distillation soluble having an amount of solids in the range of about 20 percent by weight to about 60 percent by weight mixed with said amount of extracted corn germ containing an amount of water in the range of about one percent by weight to about seven percent by weight sufficient to increase said amount of water contained by said amount of extracted corn germ to between eight percent by weight to about fourteen percent by weight.

10. The corn oil extraction system of claim 9, further comprising an amount of distillation soluble having an amount of solids in the range of about 20 percent by weight to about 60 percent by weight mixed with said amount of extracted corn germ containing an amount of water in the range of about one percent by weight to about seven percent by weight sufficient to increase said amount of water contained by said amount of extracted corn germ to greater than fourteen percent by weight, and further comprising a dryer capable of reducing the amount of water contained by said amount of corn germ mixed with said amount of distillation soluble having said amount of solids in the range of about 30 percent by weight to about 60 percent by weight to between about eight percent by weight to about fourteen percent by weight.