Method in connection with the washing of pulp at a chemical pulp mill

• US 8,632,655 B2
• Filed: 06/12/2008
• Issued: 01/21/2014
• Est. Priority Date: 06/15/2007
• Status: Active Grant

• Current Assignee: Andritz Oy (Andritz AG)
• Original Assignee: Andritz Oy (Andritz AG)
• Inventors: Vehmaa, Janne, Pikka, Olavi, Tervola, Pekka
• Primary Examiner(s): Calandra, Anthony J
• Application Number:
  US12/664,425
• Publication Number:
  US 20100243183A1
• Time in Patent Office: 2,049 Days
• Field of Search: 162/29
• US Class Current: 162/29
• CPC Class Codes: D21C 11/0028 Effluents derived from the washing or bleaching plants
• CPC Class Codes: D21C 3/02 with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
• CPC Class Codes: D21C 9/02 Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
• CPC Class Codes: D21C 9/14 with ClO2 or chlorites
• CPC Class Codes: D21C 9/147 with oxygen or its allotropic modifications D21C9/16 takes precedence
• CPC Class Codes: D21C 9/153 with ozone
• CPC Class Codes: D21C 9/166 with peracids
• CPC Class Codes: D21C 9/18 De-watering de-watering in general F26B; Elimination of cooking or pulp-treating liquors from the pulpD21C9/002, D21C9/02 take precedence; paper-making machines D21F; strainers in digesters D21C7/00; presses in general B30B

Abstract

A method in connection with washing of pulp at a chemical pulp mill including at least an alkaline cooking process utilizing cooking liquor for producing pulp, brown stock treatment with essentially closed liquid cycles, in which the last washing device is a washing device based on pressing of pulp, a press or a washing press, a pulp bleaching plant using ECF-bleaching, wherein chloride-containing effluents are formed, a chemical recovery plant and effluent purification. The liquid flows generated at a chemical pulp mill are efficiently circulated without disturbing the main process and minimizing the emissions from the mill. Purified effluent in the amount of at least 1 m3/adt pulp is introduced into the dilution after the press or washing press, whereby the effluent is passed from the dilution into the first process stage of the bleaching.

Claims

1. A method in the connection of pulp washing at a chemical pulp mill comprising:

alkaline cooking of cellulosic material utilizing cooking liquor for producing brown stock pulp,

washing the brown stock pulp in essentially closed successive liquid wash cycles, wherein a washing device in a last of the liquid wash cycles includes at least one of a washing device based on pressing of pulp, a press and a washing press,

beaching the washed brown stock using ECF-bleaching, wherein the bleaching includes a first bleaching stage and a discharge for chloride-containing effluents formed during the bleaching, and

purifying the chloride-containing effluents with a biological agent,

introducing at least 1 m³/adt of the purified chloride-containing effluents as a dilution liquid into the washed brown stock pulp downstream of the last washing device, press or washing press, and the purified chloride-containing effluents flow with the washed brown stock pulp to the first bleaching stage.

2. The method according to claim 1, wherein the first bleaching stage includes at least one of an acid treatment, a D-stage, an ozone stage, an alkaline extraction stage and a peracetic acid stage.

3. The method according to claim 1 wherein the chloride-containing effluents are purified to decrease lignin-content of the effluents.

4. The method according to claim 3 wherein the purification of the chloride-containing effluents comprises a chemical treatment.

5. The method according to claim 1, wherein a washing liquid for washing the brown stock pulp includes at least one of fresh water, evaporation plant condensate and drying machine circulation water.

6. The method according to claim 1, wherein the washing includes oxygen-delignification of the brown stock pulp.

7. The method according to claim 1 wherein a condensate originating from an evaporation plant is used in bleaching as a source of fresh water for the washing of the brown stock.

8. The method according to claim 7, wherein the condensate from the evaporation plant is also used in a pulp drying machine.

9. The method according to claim 1, wherein the chloride-containing effluents are treated in separate fractions, and one of the fractions is treated with the biological agent and another of the fractions is treated with a chemical.

10. The method according to claim 1, wherein oxidized white liquor is used as an alkali source for the bleaching and to neutralize the chloride-containing effluents.

11. The method according to as in claim 1, wherein the chloride-containing effluents upstream of the purification are cooled by the purified chloride-containing effluents.

12. The method according to claim 11, wherein the cooling occurs in a cross-flow heat exchanger through which flows the chloride-containing effluents and the purified chloride-containing effluents.

13. A method for washing pulp at a chemical pulp mill comprising:

alkaline cooking cellulosic material using a cooking liquor and producing a brown stock pulp from the cooking;

washing the brown stock pulp in a series of washing stages, wherein a last of the washing stages includes pressing the brown stock pulp;

bleaching the washed and pressed brown stock pulp with ECF-bleaching and discharging chloride-containing effluents from the bleaching, and

purifying the chloride-containing effluents using a biological agent to consume lignin in the effluents;

diluting the washed an pressed brown stock pulp with at least one cubic meter of purified chloride-containing effluents per one ton of air dried pulp (1 m³/adt), wherein the diluted, washed and pressed brown stock pulp with the purified chloride-containing effluents flow to a first process stage of the bleaching step.

14. A method to wash pulp produced in a chemical pulp mill comprising:

producing brown stock pulp in an alkaline cooking process using a cooking liquor;

washing the brown stock pulp in a succession of washing stages;

pressing the washed brown stock pulp in at least a last washing stage of the succession of washing stages;

bleaching the washed brown stock pulp in a ECF-bleaching process which produces bleached pulp and chloride-containing effluents;

purifying the chloride-containing effluents using a biological agent to consume lignin in the chloride-containing effluents, and

introducing as a dilution liquid at least one cubic meter of the chloride-containing purified effluents per one ton of air dried pulp (1 m³/adt) to the washed brown stock pulp downstream, in a pulp flow direction, from the last washing device and upstream of a first bleaching stage in the pulp bleaching step.