Evaporative light scattering detector

• US 8,681,330 B2
• Filed: 02/27/2007
• Issued: 03/25/2014
• Est. Priority Date: 03/09/2006
• Status: Expired due to Fees

• Current Assignee: BÜCHI Labortechnik AG
• Original Assignee: Alltech Associates Incorporated (Standard Industries Holdings, Inc.)
• Inventors: Saari-Nordhaus, Raaidah B., Mendoza, Washington J., Anderson, James M., Wicnienski, Michael F., Kuch, Alexandra M.
• Primary Examiner(s): NGUYEN, SANG H
• Application Number:
  US12/224,929
• Publication Number:
  US 20110181880A1
• Time in Patent Office: 2,583 Days
• Field of Search: 356335-338, 356432-437, 356/244, 428/36.3, 428/36.6, 428/36.7, 428/36.8, 428/36.9, 428/36.91, 425/35.9, 301/124.1, 301/137, 301/125, 138/140
• US Class Current: 356/337
• CPC Class Codes: G01N 2030/847 by pneumatic means
• CPC Class Codes: G01N 30/74 Optical detectors measurement of intensity, velocity, spectral content, polarisation, or phase of infrared, visible or ultraviolet light G01J

Abstract

Components suitable for use in an evaporative light scattering detector and other devices are disclosed. Methods of making and using components suitable for use in an evaporative light scattering detector and other devices are also disclosed.

Claims

1. A composite tubular member comprising a tubular wall structure having a first end, a second end, an inner wall surface facing an interior of the tubular wall structure, and an outer wall surface, said tubular wall structure comprising an inner layer of a first metal and an outer layer of a second metal, said second metal having a higher coefficient of heat transfer compared to said first metal.

2. The composite tubular member of claim 1, wherein an outer surface of said inner layer is in contact with an inner surface of said outer layer.

3. The composite tubular member of claim 1, wherein the tubular wall structure comprises an outer sleeve of said second metal and an inner sleeve of said first metal, wherein an inner surface of said inner sleeve forms the inner wall surface.

4. The composite tubular member of claim 1, wherein the inner sleeve comprises flange portions on opposite ends of the inner sleeve, said flange portions forming the first end and second end of the tubular wall structure.

5. The composite tubular member of claim 1, wherein the outer wall surface of the tubular wall structure is a continuous surface that extends around a majority of an outer periphery of the tubular wall structure.

6. The composite tubular member of claim 1, wherein the first end of the tubular wall structure has an inlet cross-sectional flow area, the second end of the tubular wall structure has an outlet cross-sectional flow area, and the tubular wall structure has a tubular cross-sectional flow area between the first end and the second end, said tubular cross-sectional flow area being substantially equal to the inlet cross-sectional flow area, the outlet cross-sectional flow area, or both.

7. The composite tubular member of claim 6, wherein the tubular cross-sectional flow area is substantially equal to both the inlet cross-sectional flow area and the outlet cross-sectional flow area.

8. The composite tubular member of claim 7, wherein each of the tubular cross-sectional flow area, the inlet cross-sectional flow area, and the outlet cross-sectional flow area has a circular cross-sectional flow area.

9. The composite tubular member of claim 1, wherein the tubular wall structure has a wall thickness of at least about 2.54 mm (0.10 in).

10. The composite tubular member of claim 1, wherein the inner layer has a wall thickness of from about 2.54 mm (0.10 in) to about 5.08 mm (0.20 in), and the outer layer has a wall thickness of from about 2.54 mm (0.10 in) to about 7.62 mm (0.30 in).

11. The composite tubular member of claim 1, wherein said first metal comprises stainless steel, and said second metal comprises copper.

12. The composite tubular member of claim 1, further comprising one or more temperature sensors positioned along a length of said tubular wall structure.

13. The composite tubular member of claim 12, wherein said one or more temperature sensors are positioned along said outer wall surface of said tubular wall structure.

14. The composite tubular member of claim 12, wherein said one or more temperature sensors comprises at least two separate temperature sensors positioned along said tubular wall structure.

15. The composite tubular member of claim 14, wherein said tubular wall structure has a tubular midsection having a midsection length L, and wherein said at least two of said separate temperature sensors are positioned a distance of at least L/2 from one another along said tubular wall structure.

16. The composite tubular member of claim 1, further comprising a heating element positioned over said outer wall surface along a length of said tubular wall structure.

17. The composite tubular member of claim 16, wherein said heating element substantially covers all of said outer wall surface.

18. An evaporative light scattering detector comprising the composite tubular member of claim 1.

19. A method of analyzing a test sample that potentially contains at least one analyte, said method comprising the steps of:

introducing the test sample into the composite tubular member of the evaporative light scattering detector of claim 18.