Techniques for pitch densification

• US 8,721,954 B2
• Filed: 03/13/2013
• Issued: 05/13/2014
• Est. Priority Date: 11/02/2010
• Status: Expired due to Fees

• Current Assignee: Honeywell International Inc.
• Original Assignee: Honeywell International Inc.
• Inventors: La Forest, Mark L., Klinedinst, Roger L., Wright, David M.
• Primary Examiner(s): Del Sole, Joseph S
• Assistant Examiner(s): Hohenbrink, Jr., Lawrence D
• Application Number:
  US13/801,229
• Publication Number:
  US 20130193606A1
• Time in Patent Office: 426 Days
• Field of Search: 264/553, 264/570, 264/571, 264/29.1, 264/29.5, 264/259.279, 264/328.4, 264/328.5, 425/503, 425/504, 425/544, 425/546, 425/DIG.228
• US Class Current: 264/328.5
• CPC Class Codes: B29C 43/003 characterised by the choice of material
• CPC Class Codes: B29C 70/48 and impregnating the reinforcements in the closed mould, e.g. resin transfer moulding [RTM] , e.g. by vacuum
• CPC Class Codes: B29K 2307/04 Carbon
• CPC Class Codes: B29L 2031/7482 Brakes
• CPC Class Codes: C04B 2235/616 Liquid infiltration of green bodies or pre-forms
• CPC Class Codes: C04B 35/6269 Curing of mixtures
• CPC Class Codes: C04B 35/83 Carbon fibres in a carbon matrix
• CPC Class Codes: F16D 69/023 Composite materials containing carbon and carbon fibres or fibres made of carbonizable material

Abstract

In some examples, a method for densifying a material via pitch comprises inserting the material to be densified into a mold, wherein the mold is part of an apparatus. The apparatus may include a ram configured to apply a ram pressure sufficient to force a pitch into the mold to densify the material, a gas source configured to apply a gas pressure sufficient to force the pitch into the mold to densify the material, and a vacuum source operable to create a vacuum pressure in the mold at least prior to application of either the ram pressure or the gas pressure. The method may further comprise densifying the material in the mold via pitch using a selectable one of the ram, the gas source, the ram and the vacuum source, or the gas source and the vacuum source.

Claims

1. A method comprising:

inserting a material to be densified into a mold, wherein the mold is part of an apparatus including;

a ram configured to apply a ram pressure sufficient to force a pitch into the mold to densify the material,

a gas source configured to apply a gas pressure sufficient to force the pitch into the mold to densify the material, and

a vacuum source operable to create a vacuum pressure in the mold at least prior to application of either the ram pressure or the gas pressure; and

densifying the material in the mold via pitch using a selectable one of the ram, the gas source, the ram and the vacuum source, or the gas source and the vacuum source.

2. The method of claim 1, wherein the material comprises a carbon fiber material preformed into a shape of a brake disc.

3. The method of claim 1, wherein densifying the material in the mold via pitch comprises applying a ram pressure, via the ram, between approximately 500 pounds per square inch (psi) and approximately 5000 psi to force the pitch into the mold.

4. The method of claim 1, wherein the ram comprises at least one of a hydraulic ram, a pneumatic ram, or a screw ram.

5. The method of claim 1, wherein the vacuum source is configured to apply the vacuum pressure between approximately 5 torr and approximately 100 torr.

6. The method of claim 1, wherein densifying the material in the mold via pitch comprises applying, via the gas source, the gas pressure between approximately 10 pounds per square inch (psi) and approximately 1000 psi to force the pitch into the mold.

7. The method of claim 6, wherein the gas source comprises nitrogen.

8. The method of claim 6, wherein the vacuum source is configured to apply the vacuum pressure between approximately 10 torr and approximately 20 torr.

9. The method of claim 1, further comprising determining an initial density of the material, wherein the apparatus is configured to select one of the ram, the gas source, the ram and the vacuum source, or the gas source and the vacuum source to densify the material based on the determined initial density.

10. The method of claim 9, wherein the apparatus is configured to select at least one of the gas source or the gas source and the vacuum source to densify the material to be densified if the initial density is less than or equal to approximately 0.8 grams per cubic centimeter.

11. The method of claim 9, wherein the apparatus is configured to select at least one of the ram or the ram and the vacuum source to densify the material to be densified if the initial density is greater than or equal to approximately 0.8 grams per cubic centimeter.

12. A method comprising:

inserting a material to be densified into a mold, wherein the mold is part of an apparatus including;

a ram configured to apply a ram pressure to force a melted pitch into the mold to densify the material during at least one of a resin transfer molding cycle or a vacuum-assisted resin transfer molding cycle,

an inert gas source configured to apply a gas pressure to force the melted pitch into the mold to densify the material during a vacuum pressure infiltration cycle, and

a vacuum source configured to create a vacuum pressure in the mold during at least one of the vacuum-assisted resin transfer molding cycle or the vacuum pressure infiltration cycle; and

densifying the material in the mold via pitch using a selectable one of the resin transfer molding cycle, the vacuum-assisted resin transfer molding cycle, or the vacuum pressure infiltration cycle.

13. The method of claim 12, wherein the ram comprises at least one of a hydraulic ram, a pneumatic ram, or a screw ram, and the ram pressure is between approximately 500 pounds per square inch (psi) and approximately 5000 psi.

14. The method of claim 12, wherein the inert gas source is configured to apply the vacuum pressure between approximately 5 torr and approximately 100 torr.

15. The method of claim 12, further comprising determining an initial density of the material, wherein the apparatus is configured to select one of the resin transfer molding cycle, the vacuum-assisted resin transfer molding cycle, or the vacuum pressure infiltration cycle to densify the preform based on the determined initial density.

16. The method of claim 15, wherein the apparatus is configured to select the vacuum pressure infiltration cycle if the initial density is less than approximately 0.8 grams per cubic centimeter (g/cc), the vacuum-assisted resin transfer molding cycle if the initial density is between approximately 0.8 g/cc and approximately 1.0 g/cc, and the resin transfer molding cycle if the initial density is greater than approximately 1.0 g/cc.

17. A method comprising:

inserting a material to be densified into a mold, wherein the mold is part of an apparatus configured to densify the material using a selectable one of a resin transfer molding cycle, a vacuum-assisted resin transfer molding cycle, or a vacuum pressure infiltration cycle;

selecting one of the resin transfer molding cycle, the vacuum-assisted resin transfer molding cycle, or the vacuum pressure infiltration cycle to densify the material in the mold; and

densifying the material in the mold using the selected one of the resin transfer molding cycle, the vacuum-assisted resin transfer molding cycle, or the vacuum pressure infiltration cycle to densify the material to be densified.

18. The method of claim 17, further comprising determining an initial dens of the material to be densified, wherein selecting one of a resin transfer molding cycle, a vacuum-assisted resin transfer molding cycle, or a vacuum pressure infiltration cycle to densify the material to be densified comprises selecting the one of the resin transfer molding cycle, the vacuum-assisted resin transfer molding cycle, or the vacuum pressure infiltration cycle based on the determined initial density.

19. The method of claim 17, wherein the material to be densified comprises a brake disc preform, and wherein densifying the material in the mold comprises pitch densifying the material in the mold.

20. The method of claim 19, wherein pitch densifying the material in the mold comprises applying at least one of a ram pressure or an inert gas pressure to the pitch.