Process and apparatus for purifying impure water using microfiltration or ultrafiltration in combination with reverse osmosis

• US 8,758,621 B2
• Filed: 03/24/2005
• Issued: 06/24/2014
• Est. Priority Date: 03/26/2004
• Status: Expired due to Fees

• Current Assignee: Evoqua Water Technologies LLC
• Original Assignee: Evoqua Water Technologies LLC
• Inventors: Zuback, Joseph Edward
• Primary Examiner(s): Jarrett, Lore
• Assistant Examiner(s): Behrendt, Benjamin J
• Application Number:
  US10/599,350
• Publication Number:
  US 20070181496A1
• Time in Patent Office: 3,379 Days
• Field of Search: 210/636, 210/641, 210/806, 210/321.69, 210/333.01, 210649-652, 210/106, 210/108, 210/332, 210/407, 210/409, 210/411, 210/416.1, 210/416.3
• US Class Current: 210/636
• CPC Class Codes: B01D 2321/04 Backflushing
• CPC Class Codes: B01D 2321/168 Use of other chemical agents
• CPC Class Codes: B01D 61/025 Reverse osmosis; Hyperfiltration
• CPC Class Codes: B01D 61/145 Ultrafiltration
• CPC Class Codes: B01D 61/147 Microfiltration
• CPC Class Codes: B01D 61/58 Multistep processes
• CPC Class Codes: B01D 65/02 Membrane cleaning or sterilisation ; Membrane regeneration
• CPC Class Codes: C02F 1/441 by reverse osmosis
• CPC Class Codes: C02F 1/444 by ultrafiltration or microfiltration
• CPC Class Codes: Y02A 20/131 Reverse-osmosis

Abstract

A method of purifying impure water contaminated with a filterable impurity and a dissolved impurity, such as seawater, comprising the steps of: providing impure water to a primary microfiltration or ultrafiltration unit to remove the filterable impurity and produce impure filtered water contaminated with a dissolved impurity; providing the impure filtered water contaminated with a dissolved impurity to a reverse osmosis unit to produce a potable water stream and a residual reverse osmosis stream; and treating the residual reverse osmosis stream prior to reuse. The treatment may be in the form of passing through a secondary filter (such as another microfiltration or ultrafiltration membrane or a cartridge filter, and the subsequently treated reverse osmosis reject may be used to backwash the microfiltration or ultrafiltration unit.

Claims

1. A method of purifying impure water contaminated with a filterable impurity and a dissolved impurity, the method comprising:

filtering the impure water in a primary microfiltration or ultrafiltration unit to remove the filterable impurity and produce impure filtered water contaminated with the dissolved impurity;

directing the impure filtered water through a first fluid line fluidly connecting an impure filtered water outlet of the primary microfiltration or ultrafiltration unit to an inlet of a reverse osmosis unit;

filtering the impure filtered water contaminated with the dissolved impurity in the reverse osmosis unit to produce a potable water stream and a residual reverse osmosis stream;

directing the residual reverse osmosis stream into a second fluid line fluidly connecting a residual reverse osmosis stream outlet of the reverse osmosis unit to an inlet of a secondary microfiltration or ultrafiltration membrane filter;

filtering the residual reverse osmosis stream by passing the stream through the secondary microfiltration or ultrafiltration membrane filter to produce a filtered saline solution;

directing the filtered saline solution into a third fluid line fluidly connecting an outlet of the secondary microfiltration or ultrafiltration membrane filter to the impure filtered water outlet of the primary microfiltration or ultrafiltration unit;

blocking flow of the filtered saline solution from the outlet of the secondary microfiltration or ultrafiltration membrane filter to the inlet of the reverse osmosis unit during backwashing of the primary microfiltration or ultrafiltration unit with the filtered saline solution by closing a valve in the first fluid line during backwashing of the primary microfiltration or ultrafiltration unit; and

backwashing the primary microfiltration or ultrafiltration unit with the filtered saline solution.

2. The method according to claim 1 wherein the secondary microfiltration or ultrafiltration membrane filter is backwashed.

3. The method according to claim 1 wherein the secondary microfiltration or ultrafiltration membrane filter is a cartridge filter.

4. The method according to claim 3 wherein the secondary microfiltration or ultrafiltration membrane filter is backwashed.

5. The method according to claim 1 wherein the impure water is sea water.

6. The method according to claim 1 wherein the filterable impurity includes those typically found in sea water.

7. The method according to claim 1 wherein the dissolved impurity includes sodium ions and chloride ions.

8. The method according to claim 1 further comprising treating the residual reverse osmosis stream prior to backwashing by one or more of a chemical treatment, a radiation treatment or a physical treatment.

9. The method according claim 8 wherein the chemical treatment is selected from the group consisting of chlorination, fluorination, disinfection, scale control treatment, water softening, peroxide, sulfite/bisulfite, ozone and combinations thereof.

10. The method according to claim 8 wherein the radiation treatment is selected from the group consisting of UV, IR, microwave and combinations thereof.

11. The method according to claim 8 wherein the physical treatment is selected from the group consisting of ultrasonication, vortexing, and combinations thereof.

12. The method according to claim 8 wherein the treatment is selected from the group consisting of heat, electroprecipitation, magnetic treatment and combinations thereof.

13. The method according to claim 1 wherein filtering the residual reverse osmosis stream comprises filtering using multiple stages of filtration.

14. The method according to claim 13 wherein filtering the residual reverse osmosis stream comprises filtering through a coarse filter prior to filtering through the secondary microfiltration or ultrafiltration membrane filter.

15. The method according to claim 14 wherein the residual reverse osmosis stream is in controllable fluid communication with a coarse backwashable filter selected from the group consisting of a single or multimedia filter, a disc filter, a diatomaceous earth filter, a membrane filter, a strainer, a screen and combinations thereof.

23. The method according to claim 1 wherein the secondary microfiltration or ultrafiltration membrane filter is fluidly connected downstream of the residual reverse osmosis stream outlet of the reverse osmosis unit but not fluidly connected upstream of the inlet of the reverse osmosis unit.

16. A method of facilitating the purification of impure water, the method comprising:

providing a primary microfiltration or ultrafiltration unit to produce impure filtered water;

providing a first fluid circuit configured to direct the impure filtered water to an inlet of a reverse osmosis unit in downstream fluid communication from said primary microfiltration or ultrafiltration unit;

providing a second fluid circuit fluidly connecting a residual reverse osmosis stream outlet of the reverse osmosis unit to an inlet of a secondary microfiltration or ultrafiltration membrane filter, the second fluid circuit configured to direct a residual reverse osmosis stream from the reverse osmosis unit to the secondary microfiltration or ultrafiltration membrane filter to produce a filtered saline solution; and

providing a controllable fluid pathway configured to direct the filtered saline solution from the secondary microfiltration or ultrafiltration membrane filter to the primary microfiltration or ultrafiltration unit to backwash the primary microfiltration or ultrafiltration unit, the first fluid circuit including a valve which prevents flow of the filtered saline solution from the secondary microfiltration or ultrafiltration membrane filter to the inlet of the reverse osmosis unit during backwashing of the primary microfiltration or ultrafiltration unit with the filtered saline solution.

24. The method according to claim 16 wherein the secondary microfiltration or ultrafiltration membrane filter is fluidly connected downstream of the residual reverse osmosis stream outlet of the reverse osmosis unit but not fluidly connected upstream of the inlet of the reverse osmosis unit.

17. A system for purifying impure water contaminated with a filterable impurity and a dissolved impurity, the system comprising:

a filtration system including;

a primary microfiltration or ultrafiltration unit configured to remove the filterable impurity;

a reverse osmosis unit configured to produce a potable water stream and a residual reverse osmosis stream, the reverse osmosis unit including an inlet in downstream fluid communication from the primary microfiltration or ultrafiltration unit; and

a first controllable fluid pathway configured to transfer a stream of impure filtered water contaminated with a dissolved impurity from the primary microfiltration or ultrafiltration unit to the reverse osmosis unit; and

a backwash system in fluid communication with a residual reverse osmosis stream outlet of the reverse osmosis unit and a permeate outlet of the primary microfiltration or ultrafiltration unit, and including;

a fluid line fluidly connecting the residual reverse osmosis stream outlet of the reverse osmosis unit to an inlet of a secondary microfiltration or ultrafiltration membrane filter, the secondary microfiltration or ultrafiltration membrane filter configured to filter the residual reverse osmosis stream to produce a filtered saline solution;

a second controllable fluid pathway configured to direct the filtered saline solution to backwash the primary microfiltration or ultrafiltration unit; and

a valve disposed in the first controllable fluid pathway which blocks flow of the filtered saline solution from the secondary microfiltration or ultrafiltration membrane filter to the inlet of the reverse osmosis unit during backwashing of the primary microfiltration or ultrafiltration unit.

18. The system according to claim 17 further comprising one or any combination of ports for the introduction of chemical agents, irradiation means, ultrasonic generators, vortexing devices, heating elements, electroprecipitators and magnets.

19. The system according to claim 17 wherein the secondary microfiltration or ultrafiltration unit is a backwashable or disposable cartridge microfiltration or ultrafiltration system.

20. The system according to claim 17 wherein the secondary microfiltration or ultrafiltration unit comprises multiple stages of filtration.

21. The system according to claim 20 wherein the multiple stages of filtration include a first filtration through a coarse filter prior to filtration through the secondary microfiltration or ultrafiltration membrane filter.

22. The system according to claim 17 wherein the residual reverse osmosis stream is in controllable fluid communication with coarse backwashable filters selected from the group consisting of single or multimedia filters, disc filters, diatomaceous earth filters, membrane filters, strainers, and screens.

25. The system according to claim 17 wherein the secondary microfiltration or ultrafiltration membrane filter is fluidly connected downstream of the residual reverse osmosis stream outlet of the reverse osmosis unit but not fluidly connected upstream of the inlet of the reverse osmosis unit.