Automated soil measurement device

• US 8,767,194 B2
• Filed: 05/28/2013
• Issued: 07/01/2014
• Est. Priority Date: 05/07/2009
• Status: Expired due to Fees

• Current Assignee: Winfield Solutions LLC (Land O'Lakes Incorporated)
• Original Assignee: Monsanto Technology LLC (Bayer AG)
• Inventors: Preiner, Michael John, Koshnick, Nicholas Carleton, White, Justin Stewart, Gerber-Siff, Bevan
• Primary Examiner(s): STAFIRA, MICHAEL PATRICK
• Application Number:
  US13/903,478
• Publication Number:
  US 20130247655A1
• Time in Patent Office: 399 Days
• Field of Search: 356/51, 356/432, 356/436, 356244-246
• US Class Current: 356/51
• CPC Class Codes: G01N 2021/3155 Measuring in two spectral ranges, e.g. UV and visible
• CPC Class Codes: G01N 21/03 Cuvette constructions
• CPC Class Codes: G01N 21/25 Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
• CPC Class Codes: G01N 21/276 with alternation of sample and standard in optical path
• CPC Class Codes: G01N 21/31 Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry G01N21/72 takes precedence
• CPC Class Codes: G01N 21/314 with comparison of measurements at specific and non-specific wavelengths dual wavelength spectrometry G01J3/427
• CPC Class Codes: G01N 21/33 using ultraviolet light G01N21/39 takes precedence
• CPC Class Codes: G01N 21/35 using infrared light G01N21/39 takes precedence
• CPC Class Codes: G01N 21/3563 for analysing solids; Preparation of samples therefor
• CPC Class Codes: G01N 21/3577 for analysing liquids, e.g. polluted water
• CPC Class Codes: G01N 21/359 using near infrared light
• CPC Class Codes: G01N 33/24 Earth materials G01N33/42 takes precedence
• CPC Class Codes: G01N 33/245 for agricultural purposes

Abstract

A soil analysis device and a method are disclosed for measuring characteristics of a soil sample. A mixing chamber combines a soil sample and an extractant into a liquid mixture. A filtration system receives and filters the liquid mixture. The filtered liquid mixture is transmitted to a measurement cell. The measurement cell is coupled to a light source so that light propagating from the light source is attenuated and/or reflected by the liquid mixture and is measured by one or more optical detectors that are also coupled to the measurement cell. The optical detector generates an attenuation spectrum and/or a reflection spectrum indicating light received by the one or more detectors at different wavelengths. The attenuation and/or reflection spectrum is used to determine the characteristics of the soil sample.

Claims

1. A soil analysis device comprising:

a mixing chamber configured to receive a soil sample and to receive an extractant, the mixing chamber configured to produce a liquid mixture by mixing the soil sample and the extractant;

a filtration system coupled to the mixing chamber and configured to receive the liquid mixture from the mixing chamber and configured to filter a portion of the received liquid mixture; and

a measurement cell coupled to the filtration system and configured to receive the filtered liquid mixture;

at least one optical detector optically coupled to the measurement cell, the optical detector configured to receive light propagating from a light source that has been at least one of;

attenuated by the filtered liquid mixture and

reflected by the filtered liquid mixture,

the at least one optical detector configured to receive light of different wavelengths, and to generate at least one of an attenuation spectrum and a reflection spectrum.

2. The device of claim 1, comprising a pipe transmitting the filtered liquid mixture from the filtration system to the measurement cell, the pipe comprising a sloped portion configured to mitigate the kinetic energy of the filtered liquid mixture thereby preventing the formation of surface effects in the measurement cell.

3. The device of claim 1 wherein the filtration system comprises a filter sufficiently porous to transmit a particulate if a salt is not present in the liquid mixture and to block transmission of the particulate if the salt is present in the liquid mixture.

4. The device of claim 1, wherein the filtration system comprises a reusable filter and an additional pipe section configured to outlet cleaning fluid.

5. The device of claim 4, wherein the filtration system comprises a pressurization system configured to clean the reusable filter by passing a cleaning fluid in an opposite direction from a direction of travel of the filtered liquid mixture.

6. The device of claim 1, wherein the measurement cell receives light from the light source through a first window and the optical detector receives attenuated light through a second window.

7. The device of claim 6, wherein the measurement cell receives light from the light source through a first window and the optical detector receives reflecting light through the first window.

8. The device of claim 6, wherein the first window and the second window allow transmission of ultraviolet, visible and near-infrared light.

9. The device of claim 6, wherein the first window and the second window include at least one of a hydrophilic film and a Teflon coating.

10. The device of claim 1, wherein the mixing chamber produces the liquid mixture using at least one of:

sonication, heating or chemical addition.

11. The device of claim 1, comprising a pre-fill chamber coupled to the mixing chamber, the pre-fill chamber providing extractant to the mixing chamber.

12. The device of claim 1, wherein the mixing chamber comprises one or more additional measurement devices coupled to the mixing chamber, the measurement devices configured to determine additional data associated with the soil sample.

13. The device of claim 1, comprising a plurality of optical detectors, wherein one of the optical detectors is configured to generate the reflection spectrum, and another of the optical detectors is configured to generate the attenuation spectrum.

14. The device of claim 1 comprising an overflow line coupled between the output of the filtration system and the measurement cell, the overflow line configured to output excess air and excess filtered liquid mixture.

15. A method for measuring characteristics of a soil sample comprising:

producing a liquid mixture by combining the soil sample and an extractant in a mixing chamber;

filtering the liquid mixture using a filtration system to produce a filtered liquid mixture;

directing at least a portion of the filtered liquid mixture into a measurement cell;

transmitting at least one of ultraviolet, visible and near-infrared light from a light source into the measurement cell;

detecting light propagating from the light source that has been at least one of;

attenuated by the filtered liquid mixture and

reflected by the filtered liquid mixture,

generating at least one of an attenuation spectrum and a reflection spectrum based on the propagated light; and

determining characteristics of the soil sample from at least one of the attenuation spectrum and the reflection spectrum.

16. The method of claim 15, further comprising:

measuring characteristics of the soil sample using at least one measurement device coupled to the mixing chamber.

17. The method of claim 16, wherein the characteristics of the soil sample comprise one or more of a moisture content of a soil sample, a viscosity of the liquid mixture, a conductivity of the soil sample, a reflection spectrum of the soil sample, a pH of the soil sample and a temperature of the liquid mixture.

18. A method comprising:

producing a liquid mixture by combining the soil sample and an extractant in a mixing chamber;

transmitting the liquid mixture into a filtration system in a first direction;

filtering the liquid mixture using the filtration system to produce a filtered liquid mixture;

directing at least a portion of the filtered liquid mixture into a measurement cell;

transmitting light from a light source into the measurement cell;

detecting light propagated from the light source through the measurement cell; and

directing a cleaning fluid through the filtration system to clean the filtration system, the cleaning fluid passing through the filtration system in a second direction opposite the first direction.