Large volume analyte preconcentrator

• US 8,771,613 B2
• Filed: 07/31/2009
• Issued: 07/08/2014
• Est. Priority Date: 07/31/2008
• Status: Active Grant

• Current Assignee: University of Louisville
• Original Assignee: University of Louisville
• Inventors: Martin, Michael, Keynton, Robert, Roussel, Thomas, Walsh, Kevin M., Jackson, Douglas J., Naber, John, Abersold, Julia W., Hageman, Richard B. III, Alexander, Suraj, Cambron, Scott
• Primary Examiner(s): MERKLING, SALLY ANNE
• Application Number:
  US13/056,091
• Publication Number:
  US 20110214482A1
• Time in Patent Office: 1,803 Days
• Field of Search: 422/527, 422/400, 422/69, 73/234.1, 73/250.5
• US Class Current: 422/527
• CPC Class Codes: B01D 2253/202 Polymeric adsorbents
• CPC Class Codes: B01D 53/02 by adsorption, e.g. preparative gas chromatography solid sorbent compositions B01J20/00, preparation of inorganic compounds or elements C01
• CPC Class Codes: G01N 1/405 by adsorption or absorption

Abstract

A large volume preconcentrator device for concentrating analytes. A housing accepts an analyte vapor flow, and a plurality of collection surfaces are disposed within the housing. A selectively actuatable heater is disposed on each of the plurality of collection surfaces. At least one selectively actuatable damper is disposed within the housing for selectively restricting a collection flow.

Claims

1. A large volume preconcentrator device for concentrating analytes, the device comprising:

a housing that accepts an analyte vapor collection flow;

a plurality of fixed supports disposed within said housing, each of said plurality of supports respectively defining a collection surface, and the plurality of supports collectively defining a collection plane where the collection flow reaches the collection surfaces;

a selectively actuatable heater disposed on the collection surface of each of said plurality of supports;

a sorbent coating disposed on the collection surface of each of said plurality of supports; and

a plurality of selectively actuatable dampers disposed within said housing and being rotatable about a pivot for selectively restricting a collection flow,

wherein the plurality of selectively actuatable dampers are provided within the housing downstream of the collection plane, for selectively allowing and restricting collection flow.

2. The preconcentrator device of claim 1, wherein the collection surface of each of said plurality of supports is disposed to face toward a direction of a collection flow through said housing;

wherein the collection surface of each of said plurality of supports is disposed to face along a direction of a desorption flow through said housing.

3. The preconcentrator device of claim 1, wherein each of said plurality of supports comprises louvers supported within said housing.

4. The preconcentrator device of claim 1, wherein said pivot is positioned at the center of said at least one selectively actuatable damper.

5. The preconcentrator device of claim 3, wherein each of the louvers are fixed.

6. The preconcentrator device of claim 3, wherein, for each of the louvers, said selectively actuatable heater is thermally isolated from the louver.

7. The preconcentrator device of claim 3, wherein each of the louvers comprise a plurality of narrow slots extending through the louvers and defining spaces between the narrow slots along the collection surface.

8. The preconcentrator device of claim 1, wherein each of said plurality of selectively actuatable dampers comprises adjustable louvers that are rotatable between a first position providing gaps between said dampers for allowing collection flow and a second position wherein said dampers overlap for restricting collection flow.

9. The preconcentrator device of claim 1, wherein each of said heaters comprises:

a thermal insulation layer disposed over the collection surface;

a heater trace disposed over said thermal insulation layer; and

a thermal distribution layer disposed over said heater trace.

10. The preconcentrator device of claim 9, wherein each of said heaters further comprises:

a thin dielectric layer disposed between said heater trace and said thermal distribution layer.

11. The preconcentrator device of claim 1, wherein said housing is configured to interface with at least one of a return air duct, a vapor collection hood, and a second stage preconcentrator.

12. The preconcentrator device of claim 1, wherein, for each of said plurality of supports, said selectively actuatable heater is disposed on both the collection surface and an opposing surface of the support.

13. A large volume preconcentrator device for concentrating analytes, the device comprising:

a housing for accepting an analyte vapor collection flow;

means for supporting a plurality of fixed collection surfaces facing a direction of a collection flow, the collection surfaces collectively defining a collection plane where the collection flow reaches the collection surfaces;

means for collecting analyte on the plurality of collection surfaces during the collection flow;

means for selectively restricting the collection flow at a position downstream of the plurality of collection surfaces by actuation of a plurality of selectively actuatable dampers, each of which is rotatable about a pivot; and

means for inducing a desorption flow from the collection surfaces.

14. A large volume preconcentrator device for concentrating analytes, the device comprising:

a housing that accepts an analyte vapor collection flow;

a plurality of collection surfaces fixably disposed within said housing, collectively defining a collection plane where the collection flow reaches the collection surfaces;

a selectively actuatable heater disposed on each of the collection surfaces; and

a plurality of selectively actuatable dampers disposed within said housing and downstream of said plurality of collection surfaces,

wherein said selectively actuatable dampers are rotatable about a pivot and configured to occupy a first position providing gaps between said dampers for selectively allowing collection flow and a second position wherein said dampers overlap for selectively restricting a collection flow.