Terahertz frequency domain spectrometer with discrete coarse and fine tuning

• US 8,829,440 B2
• Filed: 03/14/2013
• Issued: 09/09/2014
• Est. Priority Date: 05/19/2008
• Status: Active Grant

• Current Assignee: Joseph R. Demers
• Original Assignee: Emcore Corporation
• Inventors: Logan, Ronald T. Jr., Demers, Joseph R.
• Primary Examiner(s): Bryant, Casey
• Application Number:
  US13/831,438
• Publication Number:
  US 20130200263A1
• Time in Patent Office: 544 Days
• Field of Search: 250/339.07, 356/300
• US Class Current: 250/339.07
• CPC Class Codes: A61B 5/0507 using microwaves or terahertz waves
• CPC Class Codes: G01J 3/10 Arrangements of light sources specially adapted for spectrometry or colorimetry
• CPC Class Codes: G01J 3/42 Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry beam switching arrangements G01J3/08
• CPC Class Codes: G01J 3/427 Dual wavelengths spectrometry
• CPC Class Codes: G01J 3/4531 Devices without moving parts
• CPC Class Codes: G01N 21/3581 using far infrared light; using Terahertz radiation
• CPC Class Codes: G01N 21/3586 by Terahertz time domain spectroscopy [THz-TDS]
• CPC Class Codes: G01N 21/39 using tunable lasers

Abstract

An apparatus for analyzing, identifying or imaging an target including first and second laser beams coupled to a pair of photoconductive switches to produce CW signals in one or more bands in a range of frequencies greater than 100 GHz focused on and transmitted through or reflected from the target; and a detector for acquiring spectral information from signals received from the target and using a multi-spectral heterodyne process to generate an electrical signal representative of some characteristics of the target. The lasers are tuned to different frequencies and a frequency shifter in the path of one laser beam allows the terahertz beam to be finely adjusted in one or more selected frequency bands.

Claims

1. A method for spectroscopy comprising:

sweeping a CW radiative beam over at least one frequency band in a range of frequencies greater than 100 GHz;

receiving the CW radiative beam with a frequency control element and finely adjusting the frequency of the CW radiative beam using the frequency control element in frequency increments less than 100 MHz for generating electrical signals representative of some characteristic of a target in the at least one frequency band;

directing the finely adjusted radiative beam to a target; and

acquiring spectral information from the target.

2. A method as defined in claim 1, further comprising providing first and second lasers having different tunable frequencies, and wherein sweeping the CW radiative beam includes activating a first photoconductive switch by a first composite optical beam from the first and second lasers, and wherein sweeping a CW radiative beam over at least one frequency band in a range of frequencies greater than 100 GHz comprises sweeping the frequency of one of the first and second lasers.

3. A method as defined in claim 2, further comprising performing a heterodyne down conversion of the acquired spectral information from the target, wherein acquiring spectral information from the target comprises:

activating a second photoconductive switch by a second composite optical beam from the first and second lasers, the second composite beam being different from the first composite beam; and

generating an electrical signal representative of radiation transmitted or reflected from the target to provide spectral information from the target.

4. A method as defined in claim 3, further comprising:

biasing the first photoconductive switch with a modulated bias voltage; and

providing a “

lock-in”

amplifier in a detection system coupled to the second photoconductive switch, wherein the modulated bias voltage is supplied to the detection system.

5. A method as defined in claim 2, further comprising providing first and second thermoelectric coolers coupled to the first and second lasers respectively for independently coarsely tuning each of the lasers over a wavelength range of about 5 nm intervals or step sizes of about 0.01 nm.

6. A method as defined in claim 2, wherein the frequency control element comprises a frequency shifter coupled to a portion of an output beam from the first laser for tuning the frequency of the portion of the output beam from the first laser over at least a portion of a frequency range between 0 and 10 GHz.

7. A method as defined in claim 6, further comprising providing a reference oscillator coupled to the frequency shifter for tuning the frequency of the portion of the output beam from the first laser with a frequency interval or step size less than 1 MHz.

8. A method as defined in claim 6, further comprising providing a reference oscillator coupled to the frequency shifter for tuning the frequency of the portion of the output beam from the first laser.

9. A method as defined in claim 8, wherein the reference oscillator has an adjustable frequency interval or step size between 1 Hz and 100 MHz.

10. A method as defined in claim 8, wherein an intensity of a mixing or difference signal between laser frequencies of the first and second lasers, in combination with the modulation of the conductance in the photoconductive switches as a result of current flow in an antenna from the radiation transmitted or reflected from the target, results in a heterodyning and down conversion of an electrical signal representative of radiation transmitted or reflected from the target to provide spectral information from the target to a baseband frequency equal to the frequency of the reference oscillator.

11. A method as defined in claim 2, wherein the frequency control element comprises frequency shifter coupled to a portion of an output beam from the first laser for tuning the frequency of the portion of the output beam from the first laser with an adjustable frequency interval or step size between 1 Hz and 100 MHz.

12. A method as defined in claim 2, wherein the frequency control element comprises frequency modulator coupled to a portion of an output beam from the first laser for tuning the frequency of the portion of the output beam from the first laser and having an electronically adjustable bias for tuning the frequency of the portion of the output beam from the first laser.

13. A method as defined in claim 12, wherein the frequency modulator performs a frequency shift of the portion of the output beam from the first laser.

14. A method as defined in claim 1, further comprising:

storing a spectral signature of a compound;

sweeping the CW radiative beam over at least one frequency band in the range of frequencies from 100 GHz to 1.5 THz; and

subsequently determining whether the spectral signature of the compound is present in the acquired spectral information by tuning the frequency of the CW radiative beam in frequency increments less than 100 MHz.