Viscosity control in compositions comprising plant fiber materials

• US 8,884,002 B2
• Filed: 12/01/2010
• Issued: 11/11/2014
• Est. Priority Date: 12/01/2010
• Status: Active Grant

• Current Assignee: Fiberstar Incorporated
• Original Assignee: Fiberstar Bio-Ingredient Technologies, Inc.
• Inventors: Lundberg, Brock
• Primary Examiner(s): Fetterolf, Brandon
• Assistant Examiner(s): White, Everett
• Application Number:
  US12/958,118
• Publication Number:
  US 20120142909A1
• Time in Patent Office: 1,441 Days
• Field of Search: 536/80, 536/124
• US Class Current: 536/80
• CPC Class Codes: C08B 15/00 Preparation of other cellulose derivatives or modified cellulose , e.g. complexes
• CPC Class Codes: C08L 1/02 Cellulose; Modified cellulose
• CPC Class Codes: C08L 2205/16 Fibres; Fibrils
• CPC Class Codes: C12P 19/04 Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
• CPC Class Codes: C12Y 301/01011 Pectinesterase (3.1.1.11)
• CPC Class Codes: D21C 9/002 by chemical means; preparation of dewatered pulp, e.g. in sheet or bulk form, containing special additives

Abstract

Pectinases, such as Pectinex™ Ultra SP-L (composed of the enzyme Polygatacturonase, a type of pectinase which is derived from Aspergillus aculeatus) or pectinmethylesterases were used to decrease or increase, respectively, the viscosity of fiber solutions, especially solutions with highly refined cellulosic thickeners, and particularly those made of highly refined cellulosic parenchyma cell wall fiber solutions. The enzyme can reduce the viscosity up to 95% or increase the viscosity 100 fold. At lower concentrations the enzyme requires up to a few days of reacting to reach the full reduction in viscosity. Pectinex™ Ultra SP-L has an optimum pH of 4.5-5 and a temperature optimum of 40° C. By controlling the viscosity available from the dried, treated highly refined cellulosic fiber compositions, tailored powder compositions can be provided that will provide precise viscosities when rehydrated in solutions at a constant concentration.

Claims

1. A method of increasing viscosity-increasing effects of an edible refined cellulose fiber comprising:

providing an aqueous volume;

adding to the aqueous volume from 0.5% to 20% by weight of edible refined cellulose fiber to form a first reagent composition;

adding from 0.025% to 8% by volume of pectinase or pectinmethylesterase to the first reagent composition at a temperature of from 20°

C. to 80°

C.;

allowing the enzyme to modify the refined cellulose fiber for at least 15 minutes to form a final liquid composition; and

removing the modified refined cellulose from the final liquid composition;

and removing liquid from the final liquid composition to produce a viscosity increasing highly refined cellulose mass.

2. The method of claim 1 wherein the refined cellulose is present as from 2% by weight to 8% by weight in the first reagent composition.

3. The method of claim 1 wherein the temperature is maintained between 30°

C. and 50°

C. for between 30 minutes and three hours before removing the modified refined cellulose.

4. The method of claim 1 wherein the refined cellulose comprises highly refined cellulose having a total dietary fiber (TDF) content greater than 30% as measured by AOAC 991.43 and a water holding capacity greater than five parts water per part fiber as measured by AACC 56-30 and comprises less than 90% soluble fiber.

5. The method of claim 1 wherein pH in the first reagent composition is maintained between 3.0 and 9.0 during conversion to the final liquid composition and the refined cellulose is present as from 2% by weight to 8% by weight in the first reagent composition and the temperature in the first reagent composition is maintained between 30°

C. and 65°

C.

6. The method of claim 1 wherein after removing the modified refined cellulose from the final liquid composition, the removed modified refined cellulose is dried to form a dry composition.

7. The method of claim 6 wherein the dry composition is a dry refined cellulose composition comprising an enzymatically-modified cellulose fiber or enzymatically-modified refined cellulose particle, the enzymatic modification of the refined cellulose fiber reducing viscosity enhancing properties of the refined cellulose fiber or refined cellulose particle before modification.

8. The method of claim 7 wherein the dry composition comprises a refined cellulose fiber or refined cellulose particle comprises parenchymal cell wall mass selected from the group consisting of citrus pulp, citrus peel, sugar beet pulp, banana pulp, mango pulp, apple pulp or fiber, passion fruit pulp and tomato pulp.

9. The method of claim 7 wherein the refined cellulose fiber or refined cellulose particle comprises orange pulp mass.

10. The method of claim 7 wherein the enzyme used to modify the fiber or refined cellulose particle comprises a pectinase.

11. The method of claim 7 wherein the enzyme used to modify the fiber or refined cellulose particle comprises a pectinmethylesterase.

12. The method of claim 6 wherein the dry composition is a composition comprising an enzymatically-modified fiber or enzymatically-modified refined cellulose particle displaying at least 5% increased viscosity in centipoise as compared to the fiber or refined cellulose particle before modification at a concentration of 3% by weight of fiber to 97% by weight of deionized water at 25°

C.±

3°

C. after 1 minute.

13. The method of claim 12 wherein the dry composition comprises a refined cellulose fiber or refined cellulose particle comprises parenchymal cell wall mass selected from the group consisting of citrus pulp, citrus peel, sugar beet pulp, banana pulp, mango pulp, apple pulp or fiber, passion fruit pulp and tomato pulp.

14. The method of claim 12 wherein the refined cellulose fiber or refined cellulose particle comprises orange pulp mass.

15. The method of claim 12 wherein the enzyme used to modify the fiber or refined cellulose particle comprises a pectinase.

16. The method of claim 12 wherein the enzyme used to modify the fiber or refined cellulose particle comprises a pectinmethylesterase.

17. The method of claim 6 wherein the dry composition comprises a refined cellulose fiber or refined cellulose particle before enzymatic modification that has a total dietary fiber (TDF) content greater than 30% as measured by AOAC 991.43 comprises less than 90% soluble fiber.

18. The method of claim 6 wherein the dry composition comprises a refined cellulose fiber or refined cellulose particle comprises parenchymal cell wall mass, selected from the group consisting of citrus pulp, sugar beet pulp, banana pulp, mango pulp, apple pulp, passion fruit pulp and tomato pulp.

19. The method of claim 6 wherein the enzyme used to modify the fiber or refined cellulose particle comprises a pectinase.

20. The method of claim 6 wherein the enzyme used to modify the fiber or refined cellulose particle comprises a pectinmethylesterase.