Methods and compositions comprising cement kiln dust having an altered particle size

• US 8,895,486 B2
• Filed: 09/14/2012
• Issued: 11/25/2014
• Est. Priority Date: 09/09/2005
• Status: Active Grant

• Current Assignee: Halliburton Energy Services Incorporated (Halliburton Company)
• Original Assignee: Halliburton Energy Services Incorporated (Halliburton Company)
• Inventors: Roddy, Craig W., Chatterji, Jiten, Brenneis, Chad, Jarratt, Callie R.
• Primary Examiner(s): Figueroa, John J
• Application Number:
  US13/620,013
• Publication Number:
  US 20130008352A1
• Time in Patent Office: 802 Days
• Field of Search: None
• US Class Current: 507/269
• CPC Class Codes: C04B 18/162 Cement kiln dust; Lime kiln dust
• CPC Class Codes: C04B 20/008 Micro- or nanosized fillers, e.g. micronised fillers with particle size smaller than that of the hydraulic binder colloidal silica C04B14/062 ; silica fume C04B18/146
• CPC Class Codes: C04B 28/02 containing hydraulic cements other than calcium sulfates
• CPC Class Codes: C09K 8/032 Inorganic additives
• CPC Class Codes: C09K 8/467 containing additives for specific purposes
• CPC Class Codes: E21B 33/13 Methods or devices for cementing, for plugging holes, crevices or the like
• CPC Class Codes: Y02W 30/91 Use of waste materials as fillers for mortars or concrete
• CPC Class Codes: Y10T 428/2982 Particulate matter [e.g., sphere, flake, etc.]

Abstract

Methods and compositions are disclosed that comprise cement kiln dust having a mean particle size that has been altered. An embodiment discloses a method of preparing cement kiln dust comprising: providing cement kiln dust having an original particle size; and altering the mean particle size of the cement kiln dust from the original size by grinding, separating, or a combination thereof. Another embodiment discloses a well treatment fluid comprising: cement kiln dust having a mean particle size that has been altered from its original size by grinding, separating, or a combination thereof; and water.

Claims

1. A method comprising:

individually grinding a cementitious component consisting essentially of a partially calcined kiln feed removed from a gas stream, wherein the partially calcined kiln feed has an original mean particle size, wherein the cementitious component was ground to reduce the original mean particle size of the partially calcined kiln feed to a size of about 15 microns or less, wherein the original mean particle size of the partially calcined kiln feed was reduced by about 25% or more by the grinding, and wherein the partially calcined kiln feed comprises SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, Na2O, and K2O; and

mixing the ground partially calcined kiln feed with a hydraulic cement.

2. The method of claim 1, wherein the original mean particle size of the partially calcined kiln feed is reduced by about 50% or more by the grinding.

3. The method of claim 1, wherein the original mean particle size of the partially calcined kiln feed is reduced to a range of from about 1 micron to about 10 microns.

4. The method of claim 1, wherein the settable composition further comprises an additive selected from the group consisting of fly ash, slag, shale, zeolite, metakaolin, pumice, perlite, lime, silica, rice-hull ash, micro-fine cement, and any combination thereof.

5. The method of claim 1, further comprising using the partially calcined kiln feed in a settable composition comprising an additive selected from the group consisting of a set retarding additive, a strength-retrogression additive, a set accelerator, a weighting agent, a lightweight additive, a gas-generating additive, a mechanical-property-enhancing additive, a lost-circulation material, a filtration-control additive, a dispersant, a fluid-loss-control additive, a defoaming agent, a foaming agent, an oil-swellable particle, a water-swellable particle, a thixotropic additive, and any combination thereof.

6. The method of claim 1, further comprising introducing a settable composition comprising the partially calcined kiln feed into a subterranean formation.

7. The method of claim 6, wherein the settable composition is used in primary cementing.

8. The method of claim 6, wherein the settable composition is used in remedial cementing.

9. The method of claim 6, wherein the partially calcined kiln feed comprises cement kiln dust and is present in the settable composition in an amount in a range of from about 1% to about 100% by weight of the total amount of cementitious components present in the settable composition.

10. The method of claim 6, wherein the partially calcined kiln feed comprises cement kiln dust and is present in the settable composition in an amount in a range of from about 80% to about 100% by weight of the total amount of cementitious components present in the settable composition.

11. The method of claim 1, wherein the mean particle size of the partially calcined kiln feed has been reduced in an amount sufficient to provide an increase in 24-hour compressive strength of at least about 5% for a settable composition comprising the partially calcined kiln feed, the 24-hour compressive strength being measured using an Ultrasonic Cement Analyzer while maintained at 140°

F. and 3,000 psi.

12. The method of claim 1, wherein the mean particle size of the partially calcined kiln feed has been reduced in an amount sufficient to provide an increase in 24-hour compressive strength of at least about 20% for a settable composition comprising the partially calcined kiln feed, the 24-hour compressive strength being measured using an Ultrasonic Cement Analyzer while maintained at 140°

F. and 3,000 psi.

13. The method of claim 1, wherein the mean particle size of the partially calcined kiln feed has been reduced in an amount sufficient to provide an increase in 24-hour compressive strength of at least about 100% for a settable composition comprising the partially calcined kiln feed, the 24-hour compressive strength being measured using an Ultrasonic Cement Analyzer while maintained at 140°

F. and 3,000 psi.

14. A method of preparing a partially calcined kiln feed removed from a gas stream comprising:

providing the partially calcined kiln feed removed from a gas stream, wherein the partially calcined kiln feed has an original mean particle size and comprises SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, Na2O, and K2O; and

intergrinding the partially calcined kiln feed with one or more additives to reduce the original mean particle size of the partially calcined kiln feed to a size of about 15 microns or less, wherein the original mean particle size of the partially calcined kiln feed was reduced by at least about 25% by the grinding, wherein the partially calcined kiln feed is present in an amount of about 55% or more by weight of a total amount of the partially calcined kiln feed and the one or more additives.

15. The method of claim 14, wherein the reduced mean particle size of the partially calcined kiln feed is in a range of from about 1 micron to about 10 microns.

16. The method of claim 14, wherein the partially calcined kiln feed is from the manufacture of cement.

17. The method of claim 14, further comprising using the partially calcined kiln feed in a settable composition comprising an additive selected from the group consisting of hydraulic cement, fly ash, slag, shale, zeolite, metakaolin, pumice, perlite, lime, silica, rice-hull ash, micro-fine cement, and any combination thereof.

18. The method of claim 14, further comprising using the partially calcined kiln feed in a settable composition comprising an additive selected from the group consisting of a set retarding additive, a strength-retrogression additive, a set accelerator, a weighting agent, a lightweight additive, a gas-generating additive, a mechanical-property-enhancing additive, a lost-circulation material, a filtration-control additive, a dispersant, a fluid-loss-control additive, a defoaming agent, a foaming agent, an oil-swellable particle, a water-swellable particle, a thixotropic additive, and any combination thereof.

19. The method of claim 14, further comprising introducing a settable composition comprising the partially calcined kiln feed into a subterranean formation.

20. The method of claim 19, wherein the settable composition is used in primary cementing.

21. The method of claim 19, wherein the settable composition is used in remedial cementing.

22. The method of claim 19, wherein the partially calcined kiln feed comprises cement kiln dust.

23. The method of claim 19 wherein the partially calcined kiln feed comprises cement kiln dust and is present in the settable composition in an amount in a range of from about 80% to about 100% by weight of the total amount of cementitious components present in the settable composition.

24. The method of claim 14, wherein the mean particle size of the partially calcined kiln feed has been reduced in an amount sufficient to provide an increase in 24-hour compressive strength of at least about5% for a settable composition comprising the partially calcined kiln feed, the 24-hour compressive strength being measured using an Ultrasonic Cement Analyzer while maintained at 140°

F. and 3,000 psi.

25. The method of claim 14, wherein the mean particle size of the partially calcined kiln feed has been reduced in an amount sufficient to provide an increase in 24-hour compressive strength of at least about 20% for a settable composition comprising the partially calcined kiln feed, the 24-hour compressive strength being measured using an Ultrasonic Cement Analyzer while maintained at 140°

F. and 3,000 psi.

26. The method of claim 14, wherein the mean particle size of the cement kiln dust has been reduced in an amount sufficient to provide an increase in 24-hour compressive strength of at least about 100% for a settable composition comprising the partially calcined kiln feed, the 24-hour compressive strength being measured using an Ultrasonic Cement Analyzer while maintained at 140°

F. and 3,000 psi.

27. A method of preparing a partially calcined kiln feed removed from a gas stream comprising:

providing the partially calcined kiln feed removed from a gas stream, wherein the partially calcined kiln feed has an original mean particle size and comprises SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, Na2O, and K2O; and

intergrinding the partially calcined kiln feed with at least one additive selected from the group consisting of pumice, perlite, and a combination thereof to reduce the original mean particle size of the partially calcined kiln feed to a size of about 15 microns or less, wherein the original mean particle size of the partially calcined kiln feed was reduced by about 25% or more by the grinding, wherein the partially calcined kiln feed is present in an amount of about 55% or more by weight of a total amount of the partially calcined kiln feed and the one or more additives.

28. The method of claim 27, wherein the original mean particle size of the partially calcined kiln feed is reduced by about 50% or more by the grinding.

29. The method of claim 27, wherein the original mean particle size of the partially calcined kiln feed is reduced to a range of from about 1 micron to about 10 microns.

30. The method of claim 27, further comprising using the partially calcined kiln feed in a settable composition comprising an additive selected from the group consisting of a set retarding additive, a strength-retrogression additive, a set accelerator, a weighting agent, a lightweight additive, a gas-generating additive, a mechanical-property-enhancing additive, a lost-circulation material, a filtration-control additive, a dispersant, a fluid-loss-control additive, a defoaming agent, a foaming agent, an oil-swellable particle, a water-swellable particle, a thixotropic additive, and any combination thereof.