Mobile water analysis arrangement and method for determining an analyte in a water sample

• US 9,012,234 B2
• Filed: 09/28/2009
• Issued: 04/21/2015
• Est. Priority Date: 10/06/2008
• Status: Active Grant

• Current Assignee: Hach Lange GmbH (Danaher Corporation)
• Original Assignee: Hach Lange GmbH (Danaher Corporation)
• Inventors: Lundgreen, Ulrich, Farjam, Aria, Uthemann, Rolf, Mitreiter, Andreas, Huenig, Isabel, Lenhard, Markus, Froemel, Rainer, Kumpch, Hans-Joachim
• Primary Examiner(s): SIEFKE, SAMUEL P
• Application Number:
  US13/122,560
• Publication Number:
  US 20110223681A1
• Time in Patent Office: 2,031 Days
• Field of Search: 422/50, 422400-402, 436/165, 436/166, 436/169, 436/172
• US Class Current: 436/165
• CPC Class Codes: B01L 2300/0645 Electrodes
• CPC Class Codes: B01L 2300/0654 Lenses; Optical fibres
• CPC Class Codes: B01L 2300/0681 Filter
• CPC Class Codes: B01L 2300/0838 Capillaries
• CPC Class Codes: B01L 2400/0475 specific mechanical means and fluid pressure
• CPC Class Codes: B01L 3/5027 by integrated microfluidic structures, i.e. dimensions of channels and chambers are such that surface tension forces are important, e.g. lab-on-a-chip B01L3/5023 takes precedence; micromixers B01F33/30; microreactors for synthesis B01J19/0093; microcapillary devices in general B81B1/00
• CPC Class Codes: B01L 3/502715 characterised by interfacing components, e.g. fluidic, electrical, optical or mechanical interfaces
• CPC Class Codes: B01L 3/50273 characterised by the means or forces applied to move the fluids micropumps F04B19/006, of the membrane type F04B43/043
• CPC Class Codes: G01N 21/31 Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry G01N21/72 takes precedence
• CPC Class Codes: G01N 21/3151 using two sources of radiation of different wavelengths G01N21/33 - G01N21/39 take precedence
• CPC Class Codes: G01N 21/59 Transmissivity G01N21/25 takes precedence
• CPC Class Codes: G01N 21/78 producing a change of colour
• CPC Class Codes: G01N 2201/0245 with insertable-removable part
• CPC Class Codes: G01N 2201/061 Sources
• CPC Class Codes: G01N 27/30 Electrodes, e.g. test electrodes; Half-cells G01N27/414 takes precedence
• CPC Class Codes: G01N 27/4167 pH electrodes therefor G01N27/302, G01N27/36
• CPC Class Codes: G01N 27/4168 Oxidation-reduction potential, e.g. for chlorination of water water analysis G01N33/18
• CPC Class Codes: G01N 33/1886 using probes, e.g. submersible probes, buoys
• CPC Class Codes: G01N 33/1893 using flow cells

Abstract

A mobile water analyzing system for determining an analyte in a water sample includes a basic unit and a test element configured to be inserted into the basic unit. The test element includes a sample line with an inlet opening configured to receive the water sample, a measuring section forming a measuring track and configured to allow the determination of an analyte, a pump opening, and a key reagent disposed inside the sample line. The basic unit includes a test element receptacle configured to hold the inserted test element, an analyzer with an analyzer measuring track formed by the measuring section, and a pump actuator cooperatively connected with the pump opening.

Claims

1. A mobile water analyzing system for determining an analyte in a water sample, the mobile water analyzing system comprising:

a basic unit and a test element configured to be inserted into the basic unit, whereby the test element comprises;

a microfluidic sample line comprising;

an inlet opening disposed at a first end, the inlet opening being configured to receive the water sample,

a pump port disposed at a second end of the sample line,

an inlet section disposed between the inlet opening and the pump port,

a measuring section comprising at least one window arranged at an end of the measuring section, the measuring section being arranged between the inlet section and the pump port and being coincident with a sample pathway, and

a key reagent disposed in the sample line; and

whereby the basic unit comprises;

a photometer comprising a light source configured to generate a measurement beam and a light detector configured to receive the measurement beam,

a test element receptacle configured so as to allow the test element to be inserted into the test element receptacle,

a photometric measuring track, the photometric measuring track being defined by the measuring section when the test element is inserted into the test element receptacle, the measurement beam and the photometric measuring track being aligned during a photometric measurement so that a photometric measurement occurs along a length of each of the photometric measuring track and the measuring section, and not in a cross direction thereto, and

a pump actuator cooperatively connected with the pump port.

2. The mobile water analyzing system as recited in claim 1, wherein the test element further comprises a bottom part and a separate cover part, whereby the bottom part and the separate cover part are arranged so as to form the sample line therebetween.

3. The mobile water analyzing system as recited in claim 1, wherein the analyzer is an electrochemical analyzer configured to determine an electrical parameter in the measuring section, and wherein the basic unit and the test element each further comprise at least one contact and the measuring section includes at least one electrode, wherein the at least one electrode is connected with the analyzer through the at least one contact of the basic unit and the test element.

4. The mobile water analyzing system as recited by claim 1, wherein each of the photometric measuring track and the measuring section are formed by a longitudinal section of the sample line.

5. The mobile water analyzing system as recited in claim 1, wherein the test element further comprises a pump membrane and the pump actuator is configured to control the pump membrane.

6. The mobile water analyzing system as recited in claim 5, wherein the pump actuator is a part of a sample pump of the basic unit, the sample pump being connected with the pump port.

7. The mobile water analyzing system as recited in claim 1, wherein the test element further comprises an auxiliary reagent disposed in the sample line, the auxiliary reagent being disposed between the key reagent and the pump port.

8. The mobile water-analyzing system as recited in claim 1, wherein the test element further comprises an absorption body disposed between the measuring section and the pump port.

9. The mobile water-analyzing system as recited in claim 1, wherein the test element further comprises a sample filter disposed in the inlet section.

10. The mobile water analyzing system as recited in claim 1, wherein the basic unit further comprises a heating and/or cooling element configured to at least one of heat and cool the test element.

11. The mobile water analyzing system as recited in claim 1, wherein the test element further comprises a hydrophobic stopper capillary disposed in the sample line.

12. The mobile water analyzing system as recited in claim 1, wherein the test element further comprises a dose capillary disposed in the sample line.

13. A method for determining an analyte in a water sample with a mobile water analyzing system as recited in claim 1, the method comprising:

inserting the test element into the basic unit;

immersing the inlet opening into the water to be analyzed;

activating the pump actuator so as to suck a sample of the water to be analyzed through the inlet opening toward the measuring section;

segregating a defined portion of the sample inside the sample line;

mixing the sample with the key reagent by transporting the sample;

transporting the sample to the measuring section;

analyzing the sample in the measuring section with the analyzer; and

removing the test element from the basic unit.

14. The mobile water analyzing system as recited in claim 1,

wherein the test element is prefabricated.