Method and apparatus for transforming waste into fuel ethanol

• US 9,062,333 B2
• Filed: 08/16/2010
• Issued: 06/23/2015
• Est. Priority Date: 08/14/2009
• Status: Active Grant

• Current Assignee: Environmental Quality Management Associates
• Original Assignee: Environmental Quality Management Associates
• Inventors: Lehr, Larry L.
• Primary Examiner(s): Tate, Chris R
• Assistant Examiner(s): White, Douglas F
• Application Number:
  US12/856,920
• Publication Number:
  US 20110039318A1
• Time in Patent Office: 1,772 Days
• Field of Search: None
• US Class Current: 1/1
• CPC Class Codes: C12M 43/02 Bioreactors or fermenters combined with devices for liquid fuel extraction; Biorefineries
• CPC Class Codes: C12M 45/04 Phase separators; Separation of non fermentable material; Fractionation
• CPC Class Codes: C12M 45/20 Heating; Cooling heating or cooling apparatus for laboratory uses B01L7/00
• CPC Class Codes: C12P 19/02 Monosaccharides 2-ketogulonic acid C12P7/60
• CPC Class Codes: C12P 19/14 produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase , e.g. by cellulase, hemicellulase
• CPC Class Codes: C12P 2201/00 Pretreatment of cellulosic or lignocellulosic material for subsequent enzymatic treatment or hydrolysis
• CPC Class Codes: C12P 7/10 substrate containing cellulosic material
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel

Abstract

The present invention describes substrates (feedstocks) used in the production of fuel ethanol and describes the process by which the alcohol is produced. The inventors process animal, vegetable, industrial food waste or a mixture of wastes in a process involving saccharification and fermentation reactions to produce a mixture of fuel ethanol water and carbon-dioxide, which is subsequently separated to recover 95 vol. % ethanol.

Claims

1. A method for producing fuel ethanol from wastes comprising the steps of:

providing a heated reactor;

adding a waste mash of one or more animal wastes, one or more vegetable wastes, one or more industrial food wastes or a mixture thereof to the heated reactor;

adding a measured quantity of water to the waste mash contained in the heated reactor;

precooking the waste mash at about 145°

F.;

heating the waste mash to between about 230°

F. and 320°

F.;

cooling the mash to between about 140°

F. and 145°

F. to form starch;

adding one or more beta enzymes selected from a group consisting of α

-amylases, amyloglucosidases, β

-amylase, cellulases, and lignases to the waste mash;

cooling the waste mash to about 85°

F.;

liquefying the waste;

converting the one or more carbohydrates to one or more fermentable sugars comprising one or more disaccharides and one or more oligomer;

adding of one or more yeast species to the cooled reactor;

maintaining a temperature of between about 85-95 °

F.;

forming fuel ethanol and carbon dioxide by anaerobic fermentation of the one or more fermentable sugars by the one or more yeast species;

forming a mixture of the fuel ethanol and water;

transferring the mixture to a distillation column;

distilling the mixture to separate the fuel ethanol and the water to form a distilled fuel ethanol; and

contacting the distilled fuel ethanol with one or more molecular sieves to remove residual water.

2. The method of claim 1, wherein the one or more animal wastes are selected from a group consisting of cow wastes, poultry wastes, hog wastes, turkey waste, chicken waste, dairy waste, human wastes, animal manure, algal biomass and fungal biomass.

3. The method of claim 1, wherein the measured quantity of water is determined by one or more physical properties of the animal wastes, the vegetable wastes, the industrial food wastes, or the mixture.

4. The method of claim 1, wherein the one or more molecular sieves are selected from a group consisting of activated carbon, desiccants, lime, silica gel, and zeolites.

5. The method of claim 1, wherein the disaccharide is maltose and the oligomer comprises of one or more glucose units.

6. The method of claim 1, wherein the one or more vegetable wastes are selected from a group consisting of fruit wastes, potatoes, sugar crops, cane, beets, bagasse, wood, and wood by-products.

7. The method of claim 1, wherein the one or more industrial food wastes are selected from a group consisting of candy waste, bakery waste, rice bran, bean curd refuse, soybean meals, bread, and steamed rice fodder.

8. A method for producing fuel ethanol from wastes comprising the steps of:

providing a heated reactor;

adding a waste mash of one or more animal wastes, one or more vegetable wastes, one or more industrial food wastes or a mixture thereof to the heated reactor;

adding a measured quantity of water to the waste mash contained in the heated reactor;

precooking the waste mash at about 145°

F.;

heating the waste mash to between about 230°

F. and 320°

F.;

cooling the mash to between about 140°

F. and 145°

F. to form starch;

adding one or more beta enzymes selected from a group consisting of α

-amylases, amyloglucosidases, β

-amylase, cellulases, and lignases to the waste mash;

liquefying the waste;

converting the one or more carbohydrates to one or more fermentable sugars comprising one or more disaccharides and one or more oligomer;

cooling the waste mash to about 85°

F.;

adding of one or more yeast species to the cooled reactor;

maintaining a temperature of between about 85-95 °

F.;

forming fuel ethanol and carbon dioxide by anaerobic fermentation of the one or more fermentable sugars by the one or more yeast species;

forming a mixture of the fuel ethanol and water;

transferring the mixture to a distillation column;

distilling the mixture to separate the fuel ethanol and the water to form a distilled fuel ethanol; and

contacting the distilled fuel ethanol with one or more molecular sieves to remove residual water.