Pressure swing adsorption system with indexed rotatable multi-port valves

• US 9,101,872 B2
• Filed: 07/17/2013
• Issued: 08/11/2015
• Est. Priority Date: 06/30/2006
• Status: Expired due to Fees

• Current Assignee: Air Products and Chemicals Incorporated (Linde Plc)
• Original Assignee: Air Products and Chemicals Incorporated (Linde Plc)
• Inventors: Rarig, David Lester, Whitley, Roger Dean, Labuda, Matthew James
• Primary Examiner(s): Hopkins, Robert A
• Application Number:
  US13/944,418
• Publication Number:
  US 20130299023A1
• Time in Patent Office: 755 Days
• Field of Search: 95/96, 951/30, 951/48, 137/625, 137/624.13, 137/625.4, 137/625.41, 137/625.46
• US Class Current: 1/1
• CPC Class Codes: B01D 2253/108 Zeolites
• CPC Class Codes: B01D 2259/40005 using rotary valves
• CPC Class Codes: B01D 2259/40015 with two sub-steps
• CPC Class Codes: B01D 2259/40032 with three sub-steps
• CPC Class Codes: B01D 2259/40052 Recycled product or process gas
• CPC Class Codes: B01D 2259/40069 Eight
• CPC Class Codes: B01D 2259/40079 Co-current
• CPC Class Codes: B01D 2259/40081 Counter-current
• CPC Class Codes: B01D 2259/404 using four beds
• CPC Class Codes: B01D 53/02 by adsorption, e.g. preparative gas chromatography solid sorbent compositions B01J20/00, preparation of inorganic compounds or elements C01
• CPC Class Codes: B01D 53/0446 Means for feeding or distributing gases
• CPC Class Codes: B01D 53/047 Pressure swing adsorption
• CPC Class Codes: F16K 11/0716 with fluid passages through the valve member F16K11/0704, F16K11/0708, F16K11/0712 take precedence
• CPC Class Codes: F16K 11/085 with cylindrical plug
• CPC Class Codes: F16K 11/087 with spherical plug
• CPC Class Codes: Y10T 137/86863 Rotary valve unit
• CPC Class Codes: Y10T 137/86871 Plug

Abstract

Pressure swing adsorption system comprising two or more vessels, each having a feed end, a product end, and adsorbent material adapted to adsorb one or more components from a multi-component feed gas mixture; piping adapted to (1) introduce the feed gas mixture into the feed ends, withdraw a product gas from the product ends, and withdraw a waste gas from the feed ends of the vessels, and (2) place the product ends of any pair of vessels in flow communication; a feed pipe adapted to supply the feed gas mixture to the system; a product pipe adapted to withdraw the product gas from the system; and a waste gas pipe adapted to withdraw the waste gas from the system. An indexed rotatable multi-port valve is adapted to place the product end of each vessel in sequential flow communication with the product end of each of the other vessels.

Claims

1. An indexed rotatable multi-port valve assembly comprising

(a) a rotatable member adapted for rotation about an axis and having a first circular cross-section perpendicular to the axis, wherein the rotatable member comprises a first, a second, and a third passage through the rotatable member;

(b) a valve body surrounding the rotatable member, wherein the valve body is coaxial with the rotatable member and has an inner surface and an outer surface, and wherein the valve body comprises first, second, third, and fourth passages between the inner surface and the outer surface; and

(c) an indexing valve drive motor adapted to rotate the rotatable member intermittently in a single rotary direction to place the rotatable member sequentially in each of eight different circumferential positions about the periphery of the circular cross-section relative to the valve body to align selected passages in the rotatable member with selected passages in the valve body.

2. The indexed rotatable multi-port valve assembly of claim 1 wherein any one of the first, second, and third passages has a different cross-sectional flow area than either of the other two passages.

3. The indexed rotatable multi-port valve assembly of claim 1 wherein the rotatable member is adapted for intermittent rotation within the inner surface of the valve body such that

(1) the first passage in the rotatable member is in flow communication with the first and second passages in the valve body while the second and third passages in the rotatable member are not in flow communication with any passage in the valve body, and

(2) the first passage in the rotatable member is in flow communication with the third and fourth passages in the valve body while the second and third passages in the rotatable member are not in flow communication with any passage in the valve body, and

(3) one of the second or third passages in the rotatable member is in flow communication with the first and fourth passages in the valve body while the first passage in the rotatable member is not in flow communication with any passage in the valve body, and

(4) one of the second or third passages in the rotatable member is in flow communication with the second and third passages in the valve body while the first passage in the rotatable member is not in flow communication with any passage in the valve body.

4. An indexed rotatable multi-port valve assembly comprising

(a) a rotatable member adapted for rotation about an axis and having a first circular cross-section perpendicular to the axis, wherein the rotatable member has an outer surface, and wherein the rotatable member comprises

(1) first, second, third, fourth, fifth, and sixth openings at the outer surface that are disposed about the periphery of the first circular cross-section, wherein

the first opening and the second opening are separated by two equal arcs of 180 degrees around the periphery of the first circular cross-section,

the third and fourth openings are disposed along one of the two equal arcs separating the first and second openings, the third opening is separated from the fourth opening by an arc of 90 degrees on the periphery, the third opening is separated from the first opening by an arc of 45 degrees on the periphery, and the fourth opening is separated from the second opening by an arc of 45 degrees on the periphery, and

the fifth and sixth openings are disposed along the other of the two equal arcs separating the first and second openings, the fifth opening is separated from the sixth opening by an arc of 90 degrees on the periphery, the fifth opening is separated from the first opening by an arc of 45 degrees on the periphery, and the sixth opening is separated from the second opening by an arc of 45 degrees on the periphery, and

(2) a first passage through the rotatable member connecting the first opening with the second opening, a second passage through the rotatable member connecting the third opening with the fourth opening, and a third passage through the rotatable member connecting the fifth opening with the sixth opening;

(b) a valve body surrounding the rotatable member, wherein the valve body is coaxial with the rotatable member and has a second circular cross-section that is perpendicular to the axis of the rotatable member, a periphery of the second circular cross-section that is co-planar with the periphery of the first circular cross-section of the rotatable member, an inner surface, and an outer surface, and wherein the valve body comprises

(1) first, second, third, and fourth openings at the inner surface that are disposed about the periphery of the second circular cross-section, wherein each opening is separated from each adjacent opening by an arc of 90 degrees on this periphery;

(2) first, second, third, and fourth openings at the outer surface of the housing, and

(3) a first passage through the valve body connecting the first opening at the inner surface with the first opening at the outer surface, a second passage through the valve body connecting the second opening at the inner surface with the second opening at the outer surface, a third passage through the valve body connecting the third opening at the inner surface with the third opening at the outer surface, and a fourth passage through the valve body connecting the fourth opening at the inner surface with the fourth opening at the outer surface; and

(c) an indexing valve drive motor adapted to rotate the rotatable member intermittently in a single rotary direction to place the rotatable member sequentially in each of eight different circumferential positions about the periphery of the circular cross-section relative to the valve body to align selected passages in the rotatable member with selected passages in the valve body.