Automated soil measurement device

• US 9,146,223 B1
• Filed: 03/11/2013
• Issued: 09/29/2015
• Est. Priority Date: 08/03/2012
• Status: Active Grant

• Current Assignee: Winfield Solutions LLC (Land O'Lakes Incorporated)
• Original Assignee: Monsanto Technology LLC (Bayer AG)
• Inventors: Gerber-Siff, Bevan, White, Justin Stewart, Preiner, Michael John, Koshnick, Nicholas Carleton, Prouty, Stephen, Tirrell, Robert
• Primary Examiner(s): Rogers, David A
• Application Number:
  US13/794,331
• Time in Patent Office: 932 Days
• US Class Current: 1/1
• CPC Class Codes: B01D 29/00 Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
• CPC Class Codes: G01N 1/4077 by other techniques involving separation of suspended solids
• CPC Class Codes: G01N 2001/4088 filtration
• CPC Class Codes: G01N 2033/245 for agricultural purposes
• CPC Class Codes: G01N 2035/00475 Filters
• CPC Class Codes: G01N 33/24 Earth materials G01N33/42 takes precedence
• CPC Class Codes: G01N 35/1095 for supplying the samples to flow-through analysers for a specific analyser see relevant groups, e.g. under G01N15/00, G01N21/00, G01N27/00, G01N30/00, H01J49/00

Abstract

A filtration system for a soil analysis device and methods of pressure filtration and automated cleaning are disclosed for generating filtrate used in measuring characteristics of a soil sample and preparing the filtration system for repeated measurements. A mixing chamber combines a soil sample and an extractant into a liquid mixture. The filtration system receives and pressure filters the liquid mixture to quickly generate filtrate used to measure characteristics of the sample. The filtrate is passed to a measurement cell for analysis. Once the analysis is complete, the filtration system performs a cleaning process in preparation to receive a subsequent liquid mixture from another soil sample.

Claims

1. A filtration system of a soil analysis device comprising:

a first chamber coupled to a mixing chamber and receiving a liquid mixture from the mixing chamber, the first chamber coupled to an air source for pressurizing the first chamber;

a second chamber coupled to the first chamber and receiving filtered liquid mixture, the second chamber comprising a drain coupled to a measurement cell for analyzing the filtered liquid mixture, the drain configured to control flow of filtered liquid mixture into the measurement cell; and

a filter disposed between the first chamber and the second chamber to generate filtered liquid mixture by removing particulate from liquid mixture passing through the filter, the filter comprising perforations, the filtration system further configured such that when the perforations are covered by liquid mixture received in the first chamber, the first chamber is capable of being pressurized relative to the second chamber.

2. The device of claim 1, wherein a volume of liquid mixture received in the first chamber at least covers a slurry fill line of the first chamber, the slurry fill line indicating the volume of liquid mixture sufficient to cover the perforations and enable pressurization of the first chamber when the filtration system.

3. The device of claim 1, wherein the second chamber is coupled to a vacuum generator for evacuating air from the second chamber, the second chamber further coupled to a vent line configured to vent the second chamber to atmospheric pressure.

4. The device of claim 1, wherein filtrate is collected in the second chamber for a duration sufficient to generate a volume of filtered liquid mixture at least up to a filtrate fill line, the filtrate fill line indicating the volume of filtered liquid mixture sufficient to analyze the filtrate.

5. The device of claim 1, the first chamber further comprising a second drain for releasing unfiltered liquid mixture from a bottom of the first chamber.

6. The device of claim 1, wherein the filtration system is oriented in a substantially vertical position and includes a first trough shaped bottom section forming a portion of the first chamber and a second trough shaped bottom section forming a portion of the second chamber.

7. The device of claim 1, wherein the measurement cell coupled to the filtration system receives the filtered liquid mixture, the measurement cell coupled to a light source so that light propagating from the light source is attenuated by the filtered liquid mixture and is measured by an optical detector coupled to the measurement cell, the optical detector generating an attenuation spectrum indicating light received by the detector at different wavelengths.

8. The device of claim 1, wherein the filtration system is approximately between 9-21 inches high and about 1-7 inches wide, the filter configured to substantially extend a width of the filtration system to maximize surface area.

9. The device of claim 1, further comprising a computer control system configured to:

control flow of liquid mixture from the mixing chamber into the first chamber;

pressurize the liquid mixture in the first chamber; and

control flow of the filtered liquid mixture through the measurement cell.

10. A soil analysis device comprising:

a first chamber coupled to a mixing chamber and configured to receive a liquid mixture from the mixing chamber for filtration, the first chamber comprising a first drain configured to release substances present in the first chamber;

a second chamber coupled to the first chamber configured to receive a volume of filtered liquid mixture for analysis, the second chamber further comprising an inlet configured to receive a volume of cleaning fluid;

a measurement cell configured to analyze the filtered liquid mixture, the measurement cell comprising a second drain configured to release substances present in the second chamber and the measurement cell; and

a filter comprising perforations disposed between the first chamber and the second chamber, the device configured to

generate the volume of filtered liquid mixture for analysis by passing the liquid mixture through the filter in a forward direction to remove particulate, and

dislodge particulate stuck in the filter during filtration by passing the volume of cleaning fluid through the filter in a reverse direction.

11. The device of claim 10, the device further configured such that when the perforations of the filter are covered by the volume of cleaning fluid, the second chamber is capable of being pressurized relative to the first chamber.

12. The device of claim 11, wherein the second chamber is coupled to an air source configured to pressurize the second chamber to force cleaning fluid through the filter in the reverse direction to dislodge the particulate.

13. The device of claim 10, the device further configured such that when the perforations of the filter are covered by the volume of liquid mixture, the first chamber is capable of being pressurized relative to the second chamber and the first chamber is coupled to an air source configured to pressurize the first chamber to force the liquid mixture through the filter in the forward direction during filtration.

14. The device of claim 10, the device further configured such that when the perforations of the filter are covered by a second volume of cleaning fluid received in the first chamber, the first chamber is capable of being pressurized relative to the second chamber and the first chamber is coupled to an air source configured to pressurize the first chamber to force the second volume of cleaning fluid through the filter in the forward direction.

15. The device of claim 10, the first chamber further coupled to a vacuum generator for evacuating air from first chamber.

16. The device of claim 10, wherein the device is oriented in a substantially vertical position and includes a first trough shaped bottom section forming a portion of the first chamber and a second trough shaped bottom section forming a portion of the second chamber.

17. The device of claim 10, the device further configured to alternately couple the first chamber and the second chamber to an air source to dry the first chamber and the second chamber, the first drain open when pressurizing the second chamber to pass air through the filter in the reverse direction and the second drain open when pressurizing the first chamber to pass air through the filter in the forward direction.

18. A method for generating filtrate from a liquid mixture comprising a portion of a soil sample mixed with an extractant, the method comprising:

receiving, in a first chamber, a volume of the liquid mixture sufficient to cover perforations of a filter when disposed in a substantially vertical orientation between the first chamber and a second chamber, the filter impeding flow of the liquid mixture from the first chamber into a second chamber and removing particulate from the liquid mixture;

generating a pressure differential between the first chamber and the second chamber, the pressure differential forcing the liquid mixture in the first chamber through the filter to accelerate generation of filtered liquid mixture;

collecting a volume of filtered liquid mixture in the second chamber; and

draining filtrate collected in the second chamber into a measurement cell for soil analysis.

19. The method of claim 18, wherein generating the pressure differential between the first chamber and the second chamber comprises pressurizing the first chamber.

20. The method of claim 18, further comprising:

closing a drain of the second chamber when the volume of liquid mixture persists in the first chamber; and

generating a vacuum in the second chamber, the vacuum creating the pressure differential between the first chamber and the second chamber for accelerating the generation of filtered liquid mixture.

21. The method of claim 20, further comprising, in response to collecting the volume of filtered liquid mixture in the second chamber:

venting the second chamber; and

opening the drain of the second chamber to pass filtrate into the measurement cell.

22. The method of claim 18, further comprising regulating flow of the filtered liquid mixture into the measurement cell.

23. The method of claim 18, further comprising initiating a cleaning sequence in response to sensing completion of filtration.

24. A method for cleaning a filtration system, the method comprising:

draining excess liquid mixture from a first chamber through a first drain;

draining excess filtrate from a second chamber through a measurement cell and out through a second drain, the first and second chambers separated by a filter, the filter comprising perforations impeding flow of the liquid mixture from the first chamber into the second chamber;

opening a cleaner inlet for a duration to receive, in the second chamber, a volume of cleaning fluid sufficient to cover the perforations in the filter;

passing cleaning fluid backwards through the filter, from the second chamber into the first chamber, to dislodge particulate caught in the filter during filtration; and

draining excess cleaning fluid from the first and second chambers through the first and second drains, respectively.

25. The method of claim 24, wherein passing cleaning fluid backwards through the filter comprises generating a pressure differential between the first chamber and the second chamber, the pressure differential forcing the cleaning fluid in the second chamber through the filter to dislodge stuck particulate.

26. The method of claim 24, further comprising:

opening an inlet valve to receive, in the first chamber, a second volume of cleaning fluid to pass forwards through the filter into the second chamber; and

draining excess cleaning fluid from the first chamber and excess cleaning fluid from the second chamber.

27. The method of claim 26, wherein passing cleaning fluid forwards though the filter comprises generating a pressure differential between the first chamber and the second chamber, the pressure differential forcing the cleaning fluid in the first chamber through the filter.

28. The method of claim 24, wherein draining excess cleaning fluid from the first and second chambers comprises alternately coupling the first chamber and the second chamber to an air source to dry the first chamber and the second chamber, the first drain open when pressurizing the second chamber to pass air through the filter in a reverse direction and the second drain open when pressurizing the first chamber to pass air through the filter in a forward direction.

29. The method of claim 24, further comprising in response to draining excess cleaning fluid:

opening an inlet valve to receive, in the first chamber, a second volume of cleaning fluid;

generating a pressure differential between the first chamber and the second chamber, the pressure differential forcing the cleaning fluid in the first chamber through the filter; and

draining excess cleaning fluid from the first chamber and excess cleaning fluid from the second chamber.

30. The method of claim 29, wherein draining excess cleaning fluid and excess cleaning fluid from the second chamber comprises alternately coupling the first chamber and the second chamber to an air source to dry the first chamber and the second chamber, the first drain open when pressurizing the second chamber to pass air through the filter in a reverse direction and the second drain open when pressurizing the first chamber to pass air through the filter in a forward direction.