Method and apparatus for the weatherability testing of a material

• US 9,234,832 B2
• Filed: 05/21/2013
• Issued: 01/12/2016
• Est. Priority Date: 05/22/2012
• Status: Active Grant

• Current Assignee: Maschinenfabrik Reinhausen GmbH (Richard Scheubeck Beteiligungs-Gmbh & Co. KG)
• Original Assignee: Maschinenfabrik Reinhausen GmbH (Richard Scheubeck Beteiligungs-Gmbh & Co. KG)
• Inventors: Nettesheim, Stefan
• Primary Examiner(s): Soderquist, Arlen
• Application Number:
  US13/899,255
• Publication Number:
  US 20130316459A1
• Time in Patent Office: 966 Days
• Field of Search: 422/53, 422/68.1, 436/2, 436/6
• US Class Current: 1/1
• CPC Class Codes: G01N 17/00 Investigating resistance of materials to the weather, to corrosion, or to light
• CPC Class Codes: G01N 17/002 Test chambers

Abstract

A method and an apparatus (1) for weatherability testing of a material sample (3) are disclosed. The material sample (3) is exposed to a testing atmosphere (12) in a testing chamber (2). The testing atmosphere (12) is formed by a plasma (10). Testing atmosphere (12) is withdrawn from the testing chamber (2) and resupplied to the plasma generation as a process gas (5G), after filtering and/or conditioning. At least one further substance (8S) may be added to a process gas (5G) for plasma generation, in order to obtain a desired chemical composition of the testing atmosphere (12). Parameters of the testing atmosphere (12) like temperature and chemical composition may be controlled. The material sample (3) may furthermore be exposed to UV light (25), which preferably is generated by an electric arc.

Claims

1. A method for weatherability testing of at least one material sample, comprising the following steps:

a) placing a material sample in a testing chamber;

b) generating a plasma in a plasma generator and releasing a plasma jet into said testing chamber, wherein the plasma jet is not directed at the material sample;

c) forming a defined testing atmosphere in said testing chamber by means of said plasma jet, for said testing atmosphere to affect said material sample;

d) withdrawing said testing atmosphere from said testing chamber; and

,

e) supplying at least a portion of said testing atmosphere, withdrawn from said testing chamber, after filtering and/or conditioning, to said plasma generator as a process gas.

2. The method recited in claim 1, wherein said testing atmosphere is formed by conversion of at least one process gas in said plasma and in said plasma jet, and wherein a composition of said testing atmosphere is tested and monitored by a sensor.

3. The method recited in claim 2, wherein said at least one process gas is oxygen.

4. The method recited in claim 2, wherein said at least one process gas is air.

5. The method recited in claim 2, wherein said at least one process gas is of a defined humidity.

6. The method recited in claim 2, wherein at least one substance is added to said at least one process gas in said plasma generator in order to obtain a desired chemical composition of said testing atmosphere.

7. The method recited in claim 6, wherein said at least one substance added to said at least one process gas is an aerosol.

8. The method recited in claim 7, wherein said aerosol contains at least one salt.

9. The method recited in claim 1, wherein within said testing chamber a directed stream and/or a swirling is imparted to said testing atmosphere.

10. The method recited in claim 1, wherein a portion of said testing atmosphere withdrawn from said testing chamber is released into an environment.

11. The method recited in claim 1, wherein said plasma is generated by a continuous dielectric barrier discharge.

12. The method recited in claim 1, wherein said plasma is generated by a pulsed dielectric barrier discharge.

13. The method recited in claim 1, wherein said plasma is generated by a continuous electric arc.

14. The method recited in claim 1, wherein said plasma is generated by a pulsed electric arc.

15. The method recited in claim 1, wherein said material sample is exposed to ultraviolet light.

16. The method recited in claim 15, wherein said ultraviolet light is generated by an electric arc.

17. The method recited in claim 1, wherein said testing atmosphere is exposed to ultraviolet light.

18. The method recited in claim 17, wherein said ultraviolet light is generated by an electric arc.

19. The method recited in claim 1, wherein said material sample and said testing atmosphere are exposed to ultraviolet light.

20. The method recited in claim 19, wherein said ultraviolet light is generated by an electric arc.

21. The method recited in claim 1, wherein at least one parameter of said testing atmosphere is controlled and said at least one parameter is selected from the group consisting of temperature, pressure, humidity, pH value, ozone content and chemical composition of said testing atmosphere.

22. An apparatus for the weatherability testing of at least one material sample, comprising:

a testing chamber for holding a material sample,

a plasma generator with a feed system for at least one process gas for the generation of a plasma and an outlet for a plasma jet into said testing chamber for the formation of a defined testing atmosphere, wherein the plasma jet is not directed at the material sample; and

,

a recycling system wherein said testing atmosphere is withdrawn from said test chamber, conditioned, and resupplied as a process gas to said plasma generator.

23. The apparatus recited in claim 22, wherein a feed system is provided for feeding a further substance to said plasma generator.

24. The apparatus recited in claim 22, wherein a control unit is provided for controlling at least one parameter of said testing atmosphere and said at least one parameter is selected from a group consisting of temperature, pressure, humidity, pH value, ozone content and chemical composition of said testing atmosphere and wherein said testing chamber contains at least one sensor for said at least one parameter.

25. The apparatus recited in claim 24, wherein said control unit is configured to affect at least said feed system for said at least one process gas.

26. The apparatus recited in claim 24, wherein said control unit is configured to affect a feed system for at least one substance.

27. The apparatus recited in claim 24, wherein said control unit is configured to affect a voltage source for said plasma generator.

28. An apparatus for the weatherability testing of at least one material sample, comprising:

a testing chamber for holding the at least one material sample;

a plasma generator including an outlet at least partially disposed within the testing chamber;

at least one process gas supplied to the plasma generator;

a voltage source arranged to convert the at least one supplied process gas into a plasma to be introduced into the testing chamber via the outlet and form a defined testing atmosphere in the testing chamber, wherein the plasma is not directed at the material sample;

;

a first substance suitable to be mixed with the plasma in the plasma generator;

a conditioner arranged to remove a second substance from the defined testing atmosphere; and

,

a pressure generator arranged to pressurize the defined testing atmosphere, wherein;

once the testing chamber is filled with the defined testing atmosphere, the defined testing atmosphere flows from the testing chamber to the conditioner, to the pressure generator and to the testing chamber again.