Reactor for degumming

• US 9,290,717 B1
• Filed: 12/15/2014
• Issued: 03/22/2016
• Est. Priority Date: 12/15/2014
• Status: Active Grant

• Current Assignee: Archer Daniels Midland Company
• Original Assignee: Arisdyne Systems Incorporated
• Inventors: Kozyuk, Oleg, Reimers, Peter, Reinking, Paul A.
• Primary Examiner(s): Young, Natasha
• Application Number:
  US14/570,399
• Time in Patent Office: 463 Days
• US Class Current: 1/1
• CPC Class Codes: B01J 19/2405 provoking a turbulent flow of the reactants, such as in cyclones, or having a high Reynolds-number
• CPC Class Codes: B01J 2219/00164 controlling the flow
• CPC Class Codes: B01J 3/08 Application of shock waves for chemical reactions or for modifying the crystal structure of substances
• CPC Class Codes: C11B 3/16 by mechanical means

Abstract

A reactor is used for degumming vegetable oil to increase yield and reduce phosphatides. The reactor includes an annular obstruction with multiple circumferential spacers that form ring gaps around a center body having a tapered surface. The circumferential spacers and ring gaps form decompression stages for explosively mixing the oil with degumming agents. Impurities are transferred to the degumming agents and further separation of the components can be carried out to produce a refined oil product.

Claims

1. A reactor for degumming oil, the reactor comprising:

a housing having a flow path, the flow path having an a surface and the flow path comprising an upstream portion for receiving oil and a downstream portion for receiving processed oil;

an annular obstruction attached to the surface of the flow path for reducing the cross-sectional area of the flow path, the obstruction having an opening;

a frusto-conical body or a portion thereof positioned in the opening of the annular obstruction, the frusto-conical body having a surface and being positioned along the centerline of the flow path of the housing;

the annular obstruction having two or more circumferential spacers in series positioned around the surface of the frusto-conical body; and

the two or more circumferential spacers in series positioned around the surface of the frusto-conical body form ring gaps around the surface of the frusto-conical body for guiding oil through the flow path, wherein the cross-sectional area of each ring gap (Ax) is less than that of the next downstream ring gap (Ax+1) according to the following equation;

1.2≦

(Ax+1)/Ax≦

1.4, where x=1, 2, 3.

2. The reactor of claim 1, wherein the frusto-conical body having a gradually increasing circumferential diameter along its surface in a direction towards the downstream portion of the flow path.

3. The reactor of claim 1, wherein the two or more circumferential spacers having a surface facing towards the upstream portion of the flow path, wherein the surface facing towards the upstream portion forms an angle between 900 and 1000 with the surface of the frusto-conical body positioned in the opening of the annular obstruction.

4. The reactor of claim 1, wherein the two or more circumferential spacers in series positioned around the surface of the frusto-conical body having a surface facing towards the downstream portion of the flow path, wherein the surface facing towards the downstream portion forms an angle between 500 and 800 with the centerline of the flow path of the housing.

5. The reactor of claim 1, wherein the annular obstruction having three circumferential spacers in series positioned around the surface of the frusto-conical body.

6. The reactor of claim 1, wherein the ring gap having a radial length, the radial length of the ring gap is selected so that the ratio between a ring gap radial length and the next downstream ring gap radial length is in the range from 1.08 to 1.27, the ring gap radial length being the minimal distance between the innermost tip of a circumferential spacer and the surface of the frusto-conical body.

7. The reactor of claim 6, wherein the radial length of the ring gaps being less than 4 mm.

8. The reactor of claim 1, wherein the two or more circumferential spacers having a knife edge that lands less than 1 mm in thickness as measured along the flow direction in the housing.

9. The reactor of claim 1, wherein the frusto-conical body being mounted on shaft for moving the frusto-conical body along the centerline of the flow path of the housing and within the annular obstruction.

10. The reactor of claim 9, further comprising a mechanism for moving the shaft.

11. A reactor for degumming vegetable oil in the absence of cavitation, the reactor comprising:

a tubular housing having a flow path, the flow path having comprising an upstream portion for receiving oil and a downstream portion for receiving processed oil;

the tubular housing having an annular obstruction for reducing the cross-sectional area of the flow path, the annular obstruction comprising a series of two or more circumferential spacers in series, wherein the two or more circumferential spacers each form a circular 13 opening such that the diameter of the opening of each circumferential spacer with each consecutive downstream circumferential spacer;

a body or a portion thereof positioned in the circular openings of the two or more circumferential spacers in series, the body having a tapered surface that forms ring gaps between the two or more circumferential spacers and the tapered surface, wherein the ring gaps provide a flow path for the vegetable oil, wherein the cross-sectional area of each ring gap (Ax) is less than that of the next downstream ring gap (Ax+1) according to the following equation;

1.2≦

(Ax+1)/Ax≦

1.4, where x=1, 2, 3; and

the two or more circumferential spacers having a surface facing towards the upstream portion of the flow path, wherein the surface facing towards the upstream portion forms an angle between 900 and 1000 with the tapered surface of the body positioned in the circular openings of the two or more circumferential spacers in series and the two or more circumferential spacers having an angled surface facing towards the downstream portion of the flow path, wherein the angled surface facing towards the downstream portion forms an angle between 500 and 800 with the centerline of the flow path through the upstream portion of the tubular housing.

12. The reactor of claim 11, wherein the annular obstruction having three circumferential spacers in series positioned around the tapered surface of the body.

13. The reactor of claim 11, wherein the cross-sectional area of each ring gap (Ax) being selected such that no cavitation is induced in the vegetable oil.

14. The reactor of claim 11, wherein the angle of the taper is constant along the tapered surface.

15. The reactor of claim 11, wherein the body having a tapered surface being a conical or frusto-conical body.