Apparatus and method for phase equilibrium with in-situ sensing

• US 9,291,585 B2
• Filed: 05/17/2011
• Issued: 03/22/2016
• Est. Priority Date: 08/26/2010
• Status: Active Grant

• Current Assignee: Schlumberger Technology Corporation (Schlumberger NV)
• Original Assignee: Schlumberger Technology Corporation (Schlumberger NV)
• Inventors: Singh, Anil, Schmidt, Kurt, Abbott, Brian, Schroeder, Robert J, Donzler, Eric Paul
• Primary Examiner(s): Jagan, Mirellys
• Application Number:
  US13/818,996
• Publication Number:
  US 20130243028A1
• Time in Patent Office: 1,771 Days
• Field of Search: 374/31, 374/43, 374/208, 374/120, 374/141, 374/143
• US Class Current: 1/1
• CPC Class Codes: G01N 11/04 through a restricted passage, e.g. tube, aperture
• CPC Class Codes: G01N 11/16 by measuring damping effect upon oscillatory body
• CPC Class Codes: G01N 25/00 Investigating or analyzing materials by the use of thermal means G01N3/00 - G01N23/00 take precedence
• CPC Class Codes: G01N 33/2823 raw oil, drilling fluid or polyphasic mixtures hydrocarbon content of earth materials G01N33/241; prospecting G01V; drilling per se E21B
• CPC Class Codes: G01N 9/002 using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis G01N9/34 takes precedence
• CPC Class Codes: G01N 9/34 by using elements moving through the fluid, e.g. vane

Abstract

A technique facilitates the monitoring of thermodynamic properties of reservoir fluids. The technique utilizes a modular sensor assembly designed to evaluate a sample of a hydrocarbon-containing fluid within a cell body. A variety of sensors may be selectively placed into communication with a sample chamber within the cell body to evaluate the sample at potentially high pressures and temperatures. The sensors may comprise a density-viscosity sensor located in-situ to efficiently measure both the density and viscosity of the sample as a function of pressure and temperature. Other sensors, such as an optic sensor, may also be positioned to measure parameters of the sample while the sample is retained in the sample chamber.

Claims

1. An apparatus for measuring thermodynamic properties of reservoir fluids, comprising:

a modular sensor assembly comprising a cell body having a sample chamber for receiving a sample of single phase or coexisting two-phase fluid, an agitation mechanism to agitate the sample in the sample chamber, and a density-viscosity sensor located in-situ to measure the density and viscosity of the sample in the sample chamber as a function of pressure and temperature.

2. The apparatus as recited in claim 1, wherein the agitation mechanism comprises an ultrasonic transducer.

3. A method of measuring thermodynamic properties of reservoir fluids, comprising:

assembling a modular sensor assembly to evaluate a sample of a hydrocarbon-containing fluid;

charging a sample chamber within a cell body of the modular sensor assembly with the sample;

adjusting the temperature and the pressure of the sample within the sample chamber; and

utilizing a single sensor to determine both density and viscosity of the sample while in the sample chamber.

4. The method as recited in claim 3, further comprising using an optic sensor to measure parameters of the sample while in the sample chamber.

5. The method as recited in claim 3, further comprising adjusting the pressure of the sample in the sample chamber with a piston.

6. The method as recited in claim 3, further comprising adjusting the temperature of the sample in the sample chamber with a thermal management system surrounding the cell body.

7. The method as recited in claim 3, further comprising automatically controlling the charging, adjusting, and utilizing steps with a processor-based controller.

8. A method of measuring thermodynamic properties of reservoir fluids, comprising:

providing a portable, modular sensor assembly at a wellsite;

charging a cell body of the portable, modular sensor assembly with a fluid sample from a subterranean reservoir;

pressurizing the fluid sample within the cell body by compressing the fluid sample while in the cell body;

increasing the temperature of the fluid sample with a thermal management system positioned as an integral part of the portable, modular sensor assembly;

agitating the fluid sample while in the cell body to recombine fluid from multiple phases into a single phase; and

utilizing sensors exposed to an inner sample chamber of the cell body to measure desired properties of the fluid sample.

9. The method as recited in claim 8, further comprising utilizing a processor-based control system to automate the charging, pressurizing, increasing, agitating, and utilizing steps.

10. The method as recited in claim 8, wherein utilizing sensors comprises utilizing a single density-viscosity sensor.

11. The method as recited in claim 8, wherein utilizing sensors comprises utilizing a plurality of density-viscosity sensors.

12. The method as recited in claim 8, wherein utilizing sensors comprises utilizing an optic sensor.