Method of making cerium oxide nanoparticles
First Claim
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1. A method for making a dispersion of cerium oxide nanoparticles, comprising:
- a) forming an aqueous reaction mixture comprising;
i) a source of cerous ion;
ii) a source of hydroxide ion;
iii) at least one monoether carboxylic acid, wherein the molar ratio of said monoether carboxylic acid to cerous ions is greater than 0.2; and
iv) an oxidant;
b) oxidizing the cerous ion to ceric ion; and
c) thereby forming in the reaction mixture a dispersion of cerium oxide nanoparticles, CeO2-δ
, wherein δ
has a value of about 0.0 to about 0.5.
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Abstract
A process for making cerium-containing oxide nanoparticles includes providing an aqueous reaction mixture containing a source of cerous ion, a source of hydroxide ion, at least one monoether carboxylic acid wherein the molar ratio of said monoether carboxylic acid to cerous ions is greater than 0.2, and an oxidant. The cerous ion is oxidized to ceric ion, thereby forming a product dispersion of cerium-containing oxide nanoparticles CeO2-δ, wherein δ has a value of about 0.0 to about 0.5.
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Citations
17 Claims
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1. A method for making a dispersion of cerium oxide nanoparticles, comprising:
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a) forming an aqueous reaction mixture comprising; i) a source of cerous ion; ii) a source of hydroxide ion; iii) at least one monoether carboxylic acid, wherein the molar ratio of said monoether carboxylic acid to cerous ions is greater than 0.2; and iv) an oxidant; b) oxidizing the cerous ion to ceric ion; and c) thereby forming in the reaction mixture a dispersion of cerium oxide nanoparticles, CeO2-δ
, wherein δ
has a value of about 0.0 to about 0.5. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15, 16, 17)
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Specification