Methods of manufacturing steel tubes for drilling rods with improved mechanical properties, and rods made by the same

• US 9,340,847 B2
• Filed: 04/10/2012
• Issued: 05/17/2016
• Est. Priority Date: 04/10/2012
• Status: Active Grant

• Current Assignee: Tenaris Connections AG
• Original Assignee: Tenaris Connections AG
• Inventors: Egger, Pablo, Altschuler, Eduardo
• Primary Examiner(s): WALCK, BRIAN D
• Application Number:
  US13/443,669
• Publication Number:
  US 20130264123A1
• Time in Patent Office: 1,498 Days
• Field of Search: 148/519, 148/547, 148/593
• US Class Current: 1/1
• CPC Class Codes: B21B 23/00 Tube-rolling not restricted to methods provided for in only one of groups B21B17/00, B21B19/00, B21B21/00, e.g. combined processes planetary tube rolling, auxiliary arrangements, e.g. lubricating, special tube blanks, continuous casting combined with tube rollingB21B25/00 takes precedence
• CPC Class Codes: C21D 1/18 Hardening C21D1/02 takes precedence; Quenching with or without subsequent tempering quenching devices C21D1/62
• CPC Class Codes: C21D 1/30 Stress-relieving
• CPC Class Codes: C21D 2211/002 Bainite
• CPC Class Codes: C21D 2211/008 Martensite
• CPC Class Codes: C21D 8/0236 Cold rolling
• CPC Class Codes: C21D 8/0268 between cold rolling steps
• CPC Class Codes: C21D 8/105 of ferrous alloys
• CPC Class Codes: C21D 9/08 for tubular bodies or pipes
• CPC Class Codes: C21D 9/085 Cooling or quenching
• CPC Class Codes: C22C 38/001 containing N
• CPC Class Codes: C22C 38/002 containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
• CPC Class Codes: C22C 38/008 containing tin
• CPC Class Codes: C22C 38/02 containing silicon
• CPC Class Codes: C22C 38/04 containing manganese
• CPC Class Codes: C22C 38/06 containing aluminium
• CPC Class Codes: C22C 38/42 with copper
• CPC Class Codes: C22C 38/44 with molybdenum or tungsten
• CPC Class Codes: C22C 38/46 with vanadium
• CPC Class Codes: C22C 38/48 with niobium or tantalum
• CPC Class Codes: C22C 38/50 : with titanium or zirconium
• CPC Class Codes: C22C 38/54 : with boron
• CPC Class Codes: C22C 38/60 : containing lead, selenium, tellurium, or antimony, or more than 0.04% by weight of sulfur

Abstract

Embodiments of the present disclosure are directed to methods of manufacturing steel tubes that can be used for mining exploration, and rods made by the same. Embodiments of the methods include a quenching of steel tubes from an austenitic temperature prior to a cold drawing, thereby increasing mechanical properties within the steel tube, such as yield strength, impact toughness, hardness, and abrasion resistance. Embodiments of the methods reduce the manufacturing step of quenching and tempering ends of a steel tube to compensate for wall thinning during threading operations. Embodiments of the methods also tighten dimensional tolerances and reduce residual stresses within steel tubes.

Claims

1. A method of manufacturing a steel tube, comprising:

casting a steel having a composition into a bar or slab, the composition comprising;

about 0.18 to about 0.32 wt. % carbon;

about 0.3 to about 1.6 wt. % manganese;

about 0.1 to about 0.6 wt. % silicon;

about 0.005 to about 0.08 wt. % aluminum;

about 0.2 to about 1.5 wt. % chromium;

about 0.2 to about 1.0 wt. % molybdenum; and

the balance comprises iron and impurities;

wherein the amount of each element is provided based upon the total weight of the steel composition;

forming a tube;

quenching the tube from an austenitic temperature to form a quenched tube;

cold drawing the quenched tube to form a final tube; and

tempering the final tube to form the steel tube.

2. The method of claim 1, wherein the forming the tube comprises piercing and hot rolling the bar.

3. The method of claim 1, wherein the forming the tube comprises welding the slab into an ERW tube.

4. The method of claim 1, further comprising cold drawing the tube before quenching the tube from an austenitic temperature.

5. The method of claim 4, wherein cold drawing the tube before quenching the tube reduces a cross-sectional area of the tube by at least 15%.

6. The method of claim 1, further comprising tempering the quenched tube before cold drawing the quenched tube.

7. The method of claim 1, further comprising straightening the quenched tube before cold drawing the quenched tube.

8. The method of claim 1, further comprising straightening the final tube before tempering the final tube.

9. The method of claim 1, wherein a microstructure of the steel tube comprises at least about 90% tempered martensite.

10. The method of claim 1, wherein the steel tube comprises at least one threaded end that has not been heat treated differently from other portions of the steel tube.

11. The method of claim 1, wherein the cold drawing the quenched tube results in at least about a 6% area reduction of the quenched tube.

12. The method of claim 1, wherein the austenitic temperature is at least about 50°

C. above AC3 temperature and less than about 150°

C. above AC3 temperature.

13. The method of claim 1, wherein quenching the tube from an austenitic temperature is at a rate of at least about 20°

C./sec.

14. The method of claim 1, wherein the composition further comprises:

about 0.2 to about 0.3 wt. % carbon;

about 0.3 to about 0.8 wt. % manganese;

about 0.8 to about 1.2 wt. % chromium;

about 0.01 to about 0.04 wt. % niobium;

about 0.004 to about 0.03 wt. % titanium;

about 0.0004 to about 0.003 wt. % boron; and

the balance comprises iron and impurities;

wherein the amount of each element is provided based upon the total weight of the steel composition.

15. A method of manufacturing a steel tube for use as a drilling rod for wireline systems, comprising:

casting a steel having a composition into a bar or slab, the composition comprising;

about 0.2 to about 0.3 wt. % carbon;

about 0.3 to about 0.8 wt. % manganese;

about 0.1 to about 0.6 wt. % silicon;

about 0.8 to about 1.2 wt. % chromium;

about 0.25 to about 0.95 wt. % molybdenum;

about 0.01 to about 0.04 wt. % niobium;

about 0.004 to about 0.03 wt. % titanium;

about 0.005 to about 0.080 wt. % aluminum;

about 0.0004 to about 0.003 wt. % boron;

up to about 0.006 wt. % sulfur;

up to about 0.03 wt. % phosphorus;

up to about 0.3 wt. % nickel;

up to about 0.02 wt. % vanadium;

up to about 0.02 wt. % nitrogen;

up to about 0.008 wt. % calcium;

up to about 0.3 wt. % copper; and

the balance comprises iron and impurities;

wherein the amount of each element is provided based upon the total weight of the steel composition;

forming a tube;

cooling the tube to about room temperature;

cold drawing the tube in a first cold drawing operation to effect an about 15% to about 30% area reduction and form a tube with an outer diameter between about 38 mm and about 144 mm and an inner diameter between about 25 mm and about 130 mm;

heat treating the tube according to a first heat treatment operation to an austenizing temperature between about 50°

C. above AC3 and less than about 150°

C. above AC3 following by quenching to about room temperature at a minimum of 20°

C./second;

cold drawing the quenched tube in a second cold drawing operation to effect an area reduction of about 6% to about 14% to form a tube with an outer diameter of about 34 mm to about 140 mm and an inner diameter of about 25 mm to about 130 mm;

heat treating the tube in a second heat treatment operation to a temperature of about 400°

C. to about 600°

C. for about 15 minutes to about one hour to provide stress relief to the tube; and

cooling the tube after the second heat treatment operation to about room temperature at a rate of between about 0.2°

C./second and about 0.7°

C./second;

wherein the final steel tube after the second heat treatment operation has a microstructure of about 90% or more tempered martensite, an average grain size of about ASTM 7 or finer, a yield strength above about 930 MPa, an ultimate tensile strength above about 965 MPa, elongation above about 13%, hardness between about 30 and about 40 HRC, an impact toughness above about 30J in the longitudinal direction at room temperature based on a 10×

3.3 mm sample, and residual stresses of less than about 150 MPa.

16. The method of claim 15, wherein the forming the tube comprises piercing and hot rolling the bar into a seamless tube at a temperature between about 1000 and about 1300°

C.

17. The method of claim 15, wherein the forming the tube comprises welding the slab into an ERW tube.

18. The method of claim 15, wherein the composition comprises:

about 0.24 to about 0.27 wt. % carbon;

about 0.5 to about 0.6 wt. % manganese;

about 0.2 to about 0.3 wt. % silicon;

about 0.95 to about 1.05 wt. % chromium;

about 0.45 to about 0.50 wt. % molybdenum;

about 0.02 to about 0.03 wt. % niobium;

about 0.008 to about 0.015 wt. % titanium;

about 0.010 to about 0.040 wt. % aluminum;

about 0.0008 to about 0.0016 wt. % boron;

up to about 0.003 wt. % sulfur;

up to about 0.015 wt. % phosphorus;

up to about 0.15 wt. % nickel;

up to about 0.01 wt. % vanadium;

up to about 0.01 wt. % nitrogen;

up to about 0.004 wt. % calcium;

up to about 0.15 wt. % copper; and

the balance comprises iron and impurities;

wherein the amount of each element is provided based upon the total weight of the steel composition.

19. The method of claim 15, wherein the composition consists essentially of:

about 0.2 to about 0.3 wt. % carbon;

about 0.3 to about 0.8 wt. % manganese;

about 0.1 to about 0.6 wt. % silicon;

about 0.8 to about 1.2 wt. % chromium;

about 0.25 to about 0.95 wt. % molybdenum;

about 0.01 to about 0.04 wt. % niobium;

about 0.004 to about 0.03 wt. % titanium;

about 0.005 to about 0.080 wt. % aluminum;

about 0.0004 to about 0.003 wt. % boron;

up to about 0.006 wt. % sulfur;

up to about 0.03 wt. % phosphorus;

up to about 0.3 wt. % nickel;

up to about 0.02 wt. % vanadium;

up to about 0.02 wt. % nitrogen;

up to about 0.008 wt. % calcium;

up to about 0.3 wt. % copper; and

the balance comprises iron and impurities;

wherein the amount of each element is provided based upon the total weight of the steel composition.

20. The method of claim 15, further comprising providing threads on the end of the final steel tube without any additional heat treatments following the second heat treatment operation.

21. The method of claim 20, wherein the final steel tube with the threaded ends has a substantially uniform microstructure.

22. The method of claim 15, further comprising straightening the tube after the first heat treatment operation and before the second cold drawing operation.

23. The method of claim 15, further comprising straightening the tube after the second cold drawing operation and before the second heat treatment operation.

24. The method of claim 15, wherein the first heat treatment operation further comprises tempering the quenched tube at a temperature of 400°

C. to 700°

C. for about 15 minutes to about 60 minutes and cooling the tube to about room temperature at a rate of about 0.2°

C./second to about 0.7°

C./second.

25. A method of manufacturing a wireline system steel tube drilling rod having tight dimensional tolerances for outer diameter, inner diameter, concentricity, and straightness, the method comprising:

casting a steel having a composition into a bar or slab, the composition comprising;

about 0.18 to about 0.32 wt. % carbon;

about 0.3 to about 1.6 wt. % manganese;

about 0.1 to about 0.6 wt. % silicon;

about 0.005 to about 0.08 wt. % aluminum;

about 0.2 to about 1.5 wt. % chromium;

about 0.2 to about 1.0 wt. % molybdenum; and

the balance comprises iron and impurities;

wherein the amount of each element is provided based upon the total weight of the steel composition;

forming a tube;

quenching the tube from an austenitic temperature to form a quenched tube;

cold drawing the quenched tube to form a final tube with a maximum area reduction of about 30%;

tempering the final tube to form the steel tube; and

straightening the tempered tube.

26. The method of claim 25, wherein the cold drawing comprises forming a final tube with an area reduction of between about 6% to about 14%.