Methods for degumming oils

• US 9,410,109 B1
• Filed: 04/15/2016
• Issued: 08/09/2016
• Est. Priority Date: 07/03/2014
• Status: Active Grant

• Current Assignee: Archer Daniels Midland Company
• Original Assignee: Arisdyne Systems Incorporated
• Inventors: Kozyuk, Oleg
• Primary Examiner(s): Carr, Deborah D
• Application Number:
  US15/099,930
• Publication Number:
  US 20160230120A1
• Time in Patent Office: 116 Days
• Field of Search: 554/204
• US Class Current: 1/1
• CPC Class Codes: C11B 3/04 with acids
• CPC Class Codes: C11B 3/06 with bases

Abstract

Processes and systems are provided for effectively degumming vegetable oils with the use of an acid and base pretreated mixture of vegetable oil. The pretreated mixture is subjected to compression and one or more intervals of explosive decompression of the compressed mixture to form a degummed vegetable oil. Also provided are compression and decompression rates and conditions that can be used to effectively degum vegetable oil to achieve reduced levels of phosphorus and metals such as iron, calcium and magnesium.

Claims

1. A process for producing emulsions comprising:

a) mixing water and oil to form an emulsion having droplets of the water in the oil;

b) compressing the emulsion to reduce the volume of the droplets containing the water, thereby forming a compressed mixture;

c) decompressing the compressed mixture, said decompressing step carried out in the range of 1×

10⁵ MPa per second to about 3×

10⁶ MPa per second, causing the droplets containing the water to burst into smaller droplets.

2. The process of claim 1, the compressed mixture of step c) being subjected to at least two decompression step intervals, each decompression interval being carried out in the range of 1×

10⁵ MPa per second to about 3×

10⁶ MPa per second.

3. The process of claim 1, the emulsion of step b) being compressed to a pressure of at least 3 MPa and the volume of the droplets containing the water is reduced at least 0.1%.

4. The process of claim 1, the compression step b) being carried out with a compression device having an inlet for receiving the emulsion, the compression device capable of compressing the emulsion into the compressed mixture at least 3 MPa.

5. The process of claim 3, the emulsion being compressed by a plunger, centrifugal or gear pump.

6. The process of claim 1, the oil being a vegetable oil.

7. The process of claim 6, the vegetable oil being a crude oil or water degummed oil.

8. The process of claim 1, the decompression step c) being carried by a throttle device.

9. The process of claim 8, the throttle device being adjustable.

10. The process of claim 8, the throttle device being non-adjustable.

11. The process of claim 8, the throttle device being an orifice, nozzle or pressure loss fluid control device.

12. The process of claim 8, the throttle device being in series.

13. The process of claim 8, the throttle device being in parallel.

14. The process of claim 1, the water in step a) being an aqueous solution.

15. The process of claim 14, the droplets of step b) containing water and acid.

16. The process of claim 14, the droplets of step b) containing water and base.