Apparatus and process for treatment of biocomponents

• US 9,422,663 B1
• Filed: 11/05/2015
• Issued: 08/23/2016
• Est. Priority Date: 11/05/2015
• Status: Active Grant

• Current Assignee: Aicardo Roa-Espinosa
• Original Assignee: Aicardo Roa-Espinosa
• Inventors: Roa-Espinosa, Aicardo
• Primary Examiner(s): CALANDRA, ANTHONY J
• Application Number:
  US14/934,115
• Time in Patent Office: 292 Days
• US Class Current: 1/1
• CPC Class Codes: D21C 1/00 Pretreatment of the finely-divided materials before digesting of waste paper D21C5/02
• CPC Class Codes: D21C 1/04 with acid reacting compounds
• CPC Class Codes: D21C 1/06 with alkaline reacting compounds
• CPC Class Codes: D21C 9/001 Modification of pulp properties purification D21C9/08
• CPC Class Codes: D21C 9/004 inorganic compounds
• CPC Class Codes: D21C 9/005 organic compounds
• CPC Class Codes: D21C 9/007 by mechanical or physical means

Abstract

A process for treatment of biomass materials is disclosed. The treatment comprises of applying mechanical rubbing and crushing action to the biomass materials that result in significant reduction in the biomass particle size. The treatment is carried out in a chamber where the biomass is subjected to the action of a plurality of rotating pins against channels disposed on the chamber interior wall. The maceration of the biomass is further aided by impact from a plurality of blocks and sand particles placed inside the treatment chamber that are hurled into motion inside the chamber through collision with the rotating pins. Chemical catalysts may be used to speed up the maceration. These include aluminum silicate, either an acid or alkaline pretreatment, gaseous urea or urea granules. The treatment produces materials that are beneficial in a variety of applications such as soil erosion prevention, biofuel manufacturing, plant growth substrates and animal bedding.

Claims

1. A process for treating biomass materials comprising:

providing biomass materials in fiber or granular particulate form having a moisture level in the range of between about 2 percent and about 10 percent;

providing a treatment apparatus comprising;

a treatment chamber having a feed zone and an exit zone, said treatment chamber being adapted for pressurization, said treatment chamber containing;

a longitudinal central axis, a cylindrical enclosure, an interior portion having an interior surface and an exterior portion, said feed zone being adapted for communication with a biomass feeding device, said chamber being adapted for utilization under pressure;

a shaft disposed along the longitudinal central axis of said chamber, said shaft being adapted for rotation around said axis;

a plurality of pins affixed to said central axis, said pins protruding from the central axis, said pins being substantially perpendicular in relation to the central axis, said central axis and pins being adapted for rotation inside the chamber;

a plurality of channels disposed in an inner wall surface of the cylindrical enclosure having a predetermined width, a predetermined depth and a predetermined clearance from the pins; and

a plurality of blocks adapted for movement inside the treatment chamber, said movement of said blocks being actuated by collision with the pins, said blocks having a diameter in a range between about 0.3 inches to about 0.5 inches and weighing between about 1 gram and about 2 grams;

feeding the biomass materials into the feed zone of a treatment apparatus and moving said biomass materials from the feed zone toward the exit zone;

macerating the biomass materials; and

collecting the biomass at the exit zone of said treatment apparatus.

2. The process of claim 1, wherein the clearance between the channels and an upper portion of the pins ranges from about 0.1 inches to about 0.15 inches.

3. The process of claim 1, wherein the depth and the width of said groves range from about 0.2 inches to about 0.5 inches.

4. The process of claim 1, wherein between about 0.5 and 4 blocks per gram of biomass particles are placed inside the treatment chamber.

5. The process of claim 1, further comprising intermixing aluminum silicate with the biomass at a dry weight ratio of between about 0.25 to about 1.0 of aluminum silicate to a weight of biomass prior to treatment.

6. The process of claim 5, further comprising injecting urea gas into the treatment chamber at a pressure of between about 0.0 KPa and about 2.0 KPa and a temperature of between about 40°

C. and about 60°

C.

7. The process of claim 5, further comprising intermixing dry urea in a granular form with the aluminum silicate at a ratio of between about 1% to about 2% by weight to dry biomass.

8. The process of claim 1, wherein macerating the biomass particles is actuated by rotating the shaft at a speed of between 200 and 2000 revolutions per minute.

9. The process of claim 1, further comprising pretreating the biomass materials with an acid solution at an application rate ranging from about 0.0001% to about 0.1% by weight of the oven dry biomass, said acid being selected from the group consisting of sulfuric acid, phosphoric acid, hydrochloric acid and nitric acid.

10. The process of claim 1, further comprising pretreating the biomass materials with an alkaline solution at an application rate ranging from about 0.01% to about 0.1% by weight of the oven dry biomass, said alkaline being selected from the group consisting of sodium hydroxide, calcium oxide and potassium hydroxide.

11. The process of claim 1 further comprising intermixing a particulate macerating aid with the biomass, said macerating aid being selected from the group consisting of zirconium dioxide (ZrO₂), calcium magnesium carbonate (CaMg(CO₃)₂), silica sand and combinations thereof, said macerating aids being intermixed at a ratio range of between about 0.25 dry grams to about 0.75 dry grams per gram of biomass.