Variable capacity multiple-leg packed separation column

• US 9,480,947 B2
• Filed: 05/28/2014
• Issued: 11/01/2016
• Est. Priority Date: 07/02/2013
• Status: Active Grant

• Current Assignee: Saudi Arabian Oil Company (Government of Saudi Arabia)
• Original Assignee: Saudi Arabian Oil Company (Government of Saudi Arabia)
• Inventors: Zahrani, Talal A., Salu, Samusideen Adewale
• Primary Examiner(s): Smith, Duane
• Assistant Examiner(s): HOLECEK, CABRENA L
• Application Number:
  US14/288,820
• Publication Number:
  US 20150343370A1
• Time in Patent Office: 888 Days
• US Class Current: 1/1
• CPC Class Codes: B01D 2252/2023 Glycols, diols or their derivatives
• CPC Class Codes: B01D 2252/20489 with two or more hydroxyl groups
• CPC Class Codes: B01D 2252/504 Mixtures of two or more absorbents
• CPC Class Codes: B01D 2257/80 Water
• CPC Class Codes: B01D 53/1412 Controlling the absorption process
• CPC Class Codes: B01D 53/1493 Selection of liquid materials for use as absorbents
• CPC Class Codes: B01D 53/18 Absorbing units; Liquid distributors therefor B01D3/16, B01D3/26, B01D3/30 take precedence; packing elements B01J19/30, B01J19/32
• CPC Class Codes: B01D 53/263 by absorption

Abstract

An industrial packed column for gas stream processing to remove a component by liquid absorbent contact includes:

• • a. a plurality of packed tubular members having ends aligned in vertical parallel array to form a first bundle,
  • b. an upper lean absorption liquid inlet and lower rich absorption liquid outlet;
  • c. a raw gas feed inlet positioned below the packing material, connected to a raw feed gas manifold via control valves for selectively admitting the feed gas to one or more of the plurality of tubular members,
  • d. an upper treated gas outlet, connected via valved conduit to (i) a treated gas collection manifold and (ii) the raw gas inlet of one or more of the other tubular members, and
    the apparatus equipped with appropriate systems so that desired portions of the treated gas stream exiting a tubular member can be passed for further treatment to at least one other tubular member in the first bundle.

Claims

1. An industrial packed column apparatus configured and dimensioned for processing a raw gas feedstream to a gas-oil separation plant comprising a gaseous hydrocarbon stream containing water to remove at least a portion of the water by contact with a liquid absorbent selected from the group consisting of triethylene glycol (TEG), ethylene glycol, methyl ethylene glycol and methyldiethanolamine, the apparatus comprising:

a. a plurality of tubular members having upper and lower ends, the tubular member being aligned in a vertical parallel array to form a first bundle, one of the tubular members being configured as the final downstream member,

b. each tubular member having a packed section positioned between its upper and lower ends, the packed section containing a packing material,

c. each of the tubular members having a lean absorption liquid inlet positioned above the packed section and a rich absorption liquid outlet positioned below the packed section,

d. each of the tubular members having a raw gas feed inlet positioned below the packed section and a treated gas outlet at the top of the tubular member above the packed section,

e. each of the raw feed gas inlets connected to a raw feed gas manifold via control valves for selectively admitting the raw feed gas to one or more of the plurality of tubular members,

f. each of the treated gas outlets being respectively connected via a valved conduit to (i) a treated gas collection manifold and, with the exception of the final downstream member (ii) the raw gas inlet of one or more of the other tubular members in the first bundle, except the treated gas outlet of the final downstream member in the bundle, whereby all or a portion of a treated gas stream exiting a tubular member, except for the final downstream member can be passed for further treatment to at least one of the other tubular members in the first bundle.

2. The apparatus of claim 1 in which the first bundle consists of at least three tubular members.

3. The apparatus of claim 1 in which each of the lean absorption liquid inlets are in fluid communication with a lean absorption liquid manifold, and each of the rich absorption liquid outlets are connected via valved conduits to a manifold that is in fluid communication with an absorption liquid regeneration system.

4. The apparatus of claim 1 in which the plurality of packed tubular members are contained in a close-fitting array in a pre-existing packed column vessel from which the packing material and internal structure has been removed to provide a retrofitted industrial packed column.

5. The apparatus of claim 1 in which each of the control valves is a flow control valve that is actuated by a signal that corresponds to a condition detected by one or more sensors that monitor a component load in the effluent in the treated gas or a rich absorbent liquid, or both the treated gas and rich absorbent liquid.

6. The apparatus of claim 5 that further comprises a programmed processor controller with associated memory operatively coupled to one or more component sensors and to the flow control valves.

7. An industrial packed column apparatus comprising at least two bundles constructed in accordance with claim 1, the treated gas manifold of the first bundle being in fluid communication via at least one control valve to the raw feed gas manifold of at least one other bundles.

8. The apparatus of claim 7 comprising three bundles, where each bundle contains four tubular members.

9. The apparatus of claim 7 in which the control valves are flow control valves and the flow control valves are adapted and configured to pass the treated gas from one of the tubular members in a bundle to at least one of the other tubular members in the same bundle in response to a signal transmitted by a processor controller.