Terahertz imaging devices and systems, and related methods, for detection of materials

• US 9,494,464 B2
• Filed: 02/20/2013
• Issued: 11/15/2016
• Est. Priority Date: 02/20/2013
• Status: Active Grant

• Current Assignee: Battelle Energy Alliance LLC (Battelle Memorial Institute)
• Original Assignee: Battelle Energy Alliance LLC (Battelle Memorial Institute)
• Inventors: Kotter, Dale K.
• Primary Examiner(s): Makiya, David J
• Assistant Examiner(s): Malkowski, Kenneth J
• Application Number:
  US13/771,871
• Publication Number:
  US 20140231648A1
• Time in Patent Office: 1,364 Days
• Field of Search: 250/208.2
• US Class Current: 1/1
• CPC Class Codes: G01J 3/42 Absorption spectrometry; Double beam spectrometry; Flicker spectrometry; Reflection spectrometry beam switching arrangements G01J3/08
• CPC Class Codes: G01J 5/023 Particular leg structure or construction or shape; Nanotubes
• CPC Class Codes: G01J 5/0837 Microantennas, e.g. bow-tie
• CPC Class Codes: G01N 21/3581 using far infrared light; using Terahertz radiation
• CPC Class Codes: G01V 8/005 operating with millimetre waves, e.g. measuring the black losey radiation
• CPC Class Codes: H01Q 21/062 using dipole aerials; H01Q21/067, H01Q21/068 take precedence
• CPC Class Codes: H01Q 9/27 Spiral antennas

Abstract

Terahertz imaging devices may comprise a focal plane array including a substrate and a plurality of resonance elements. The plurality of resonance elements may comprise a conductive material coupled to the substrate. Each resonance element of the plurality of resonance elements may be configured to resonate and produce an output signal responsive to incident radiation having a frequency between about a 0.1 THz and 4 THz range. A method of detecting a hazardous material may comprise receiving incident radiation by a focal plane array having a plurality of discrete pixels including a resonance element configured to absorb the incident radiation at a resonant frequency in the THz, generating an output signal from each of the discrete pixels, and determining a presence of a hazardous material by interpreting spectral information from the output signal.

Claims

1. A terahertz imaging device, comprising:

a focal plane array including;

a substrate; and

a plurality of resonance elements comprising a conductive material coupled to the substrate, wherein;

each resonance element of the plurality of resonance elements exhibits a resonant frequency in the THz range, and is configured to resonate and produce an output signal responsive to incident radiation at about its resonant frequency;

the plurality of resonance elements is arranged in a plurality of sub-arrays;

each sub-array includes resonance elements that are tuned to a different frequency that corresponds to a different spectral absorption peak for at least one material of interest such that resonant elements of a first sub-array are tuned to a first spectral absorption peak for a first material of interest, and resonant elements of a second sub-array are tuned to a second spectral absorption peak of the first material of interest; and

each resonant element includes an antenna coupled detector that includes a diode for converting incident radiation to DC in a time sufficient for imaging.

2. The terahertz imaging device of claim 1, further comprising a spectral selective filter positioned in a path of the incident radiation prior to the focal plane array, wherein the spectral selective filter includes a plurality of resonance elements tuned to exhibit a resonant frequency for a narrow band THz frequency.

3. The terahertz imaging device of claim 2, further comprising a terahertz radiation source configured to illuminate an object of interest to induce an emission from the object of interest that is received by the focal plane array as the incident radiation.

4. The terahertz imaging device of claim 3, wherein a frequency for a signal generated by the terahertz radiation source and the resonant frequency of the plurality of resonance elements of the spectral selective filter are matched.

5. The terahertz imaging device of claim 3, wherein the terahertz radiation source and the focal plane array are arranged relative to the object of interest to operate the terahertz imaging device in a back scatter mode.

6. The terahertz imaging device of claim 3, wherein the terahertz radiation source and the focal plane array are arranged relative to the object of interest to operate the terahertz imaging device in a reflection mode.

7. The terahertz imaging device of claim 2, wherein the focal plane array is tuned for a broader band than the spectral selective filter.

8. The terahertz imaging device of claim 7, wherein the spectral selective filter is tuned for a narrow band selectivity for absorption lines of a pre-determined chemical specie.

9. The terahertz imaging device of claim 1, wherein resonant elements of a third sub-array are tuned to a third spectral absorption peak for the first material of interest, and resonant elements of a fourth sub-array are tuned to a fourth spectral absorption peak of the first material of interest.

10. The terahertz imaging device of claim 1, further comprising a portal including a plurality of discrete sensors, wherein each discrete sensor of the plurality of discrete sensors includes the focal plane array.

11. The terahertz imaging device of claim 1, wherein resonant elements of a third sub-array are tuned to a first spectral absorption peak for a second material of interest, and resonant elements of a fourth sub-array are tuned to a second spectral absorption peak of the second material of interest.

12. The terahertz imaging device of claim 1, wherein the first material of interest is RDX, the first spectral absorption peak being selected from one of the group consisting of approximately 0.82 THz, 1.05 THz, 1.50 THz, 1.96 THz, 2.2 THz, and 3.08 THz, and the second spectral absorption peak being selected from another of the group consisting of approximately 0.82 THz, 1.05 THz, 1.50 THz, 1.96 THz, 2.2 THz, and 3.08 THz.

13. A terahertz imaging system, comprising:

a portal having a plurality of discrete sensors, wherein each discrete sensor comprises a focal plane array having a plurality of pixels, each pixel having a resonance element configured to absorb incident radiation, resonate at a frequency in the THz range, and responsively generate an output, wherein the resonance elements are arranged in a plurality of sub-arrays of the focal plane array that are each tuned to a different frequency corresponding to a different spectral absorption peak for at least one material of interest, wherein the portal is configured to operate a first discrete sensor as a THZ source and read data from the focal plane arrays of the other discrete sensors, and then operate a second discrete sensor as a THZ source and read data from the focal plane arrays of the other discrete sensors, and continue operating a different discrete sensor as a THZ source and reading data from the focal plane arrays of the other discrete sensors until each of the plurality of discrete sensors has been operated as a THZ source; and

a data acquisition system configured to construct a multidimensional image that can identify the location of a threat object in the portal.

14. The terahertz imaging system of claim 13, wherein the resonance element in each focal plane array has a shape selected from the group consisting of a simple dipole, a bowtie dipole, a spiral, a square loop, a square spiral, a circular loop, concentric loops, an ellipse, a rectangle, a triangle, and a cross.

15. The terahertz imaging system of claim 13, wherein the resonance element in each focal plane array includes an electrically conductive material that is selected from the group consisting of manganese (Mn), gold (Au), silver (Ag), chromium (Cr), copper (Cu), aluminum (Al), platinum (Pt), nickel (Ni), iron (Fe), lead (Pb), tin (Sn), and titanium (Ti).

16. The terahertz imaging system of claim 13, further comprising a spectral selective filter for each focal plane array having a plurality of resonance elements configured to pass a narrow band of the incident radiation to each focal plane array.

17. The terahertz imaging system of claim 16, wherein the spectral selective filter is configured as a gangbuster filter.

18. The terahertz imaging device of claim 13, wherein the resonance elements are selected from the group consisting of antennas, microantennas, nanoantennas, and nanoparticles.

19. A method of detecting at least one hazardous material, the method comprising:

filtering incident radiation through a spectral selective filter having a first plurality of resonance elements configured to pass a narrow band of the incident radiation;

receiving the filtered incident radiation by a focal plane array having a plurality of discrete pixels including a second plurality of resonance elements configured to absorb the filtered incident radiation at a resonant frequency in the THz range for a plurality of sub-arrays that are tuned to different frequencies corresponding to different spectral absorption peaks for at least one hazardous material of interest such that resonant elements of a first sub-array are tuned to a first spectral absorption peak for a first material of interest, and resonant elements of a second sub-array are tuned to a second spectral absorption peak of the first material of interest;

generating an output signal from each of the discrete pixels; and

determining a presence of at least one hazardous material of interest by interpreting spectral information from the output signal.

20. The method of claim 19, wherein receiving incident radiation by a focal plane array includes passively receiving the incident radiation that was emitted from an object of interest.

21. The method of claim 19, wherein receiving incident radiation by a focal plane array includes actively receiving the incident radiation that was emitted from an object of interest in response to illuminating the object of interest with a terahertz radiation source.

22. The method of claim 19, wherein the hazardous material of interest is selected from the group consisting of chlorine gas, mustard gas, insecticide, sarin gas, cyclosarin, soman, CS gas, tear gas, anthrax bacteria, and botulinum.

23. A terahertz imaging device, comprising:

a focal plane array including;

a substrate; and

a plurality of resonance elements comprising a conductive material coupled to the substrate, wherein;

each resonance element of the plurality of resonance elements exhibits a resonant frequency in the THz range, and is configured to resonate and produce an output signal responsive to incident radiation at about its resonant frequency;

the plurality of resonance elements is arranged in a plurality of sub-arrays;

each sub-array includes resonance elements that are tuned to a different frequency that corresponds to a different spectral absorption peak for at least one material of interest; and

each resonant element includes an antenna coupled detector that includes a diode for converting incident radiation to DC in a time sufficient for imaging; and

wherein each resonance element of at least one sub-array includes a bowtie dipole antenna having an inner width of approximately 2.51 μ

m, an outer width of approximately 42.36 μ

m, and a port gap width of approximately 2.41 μ

m.