System and method for analyzing water samples in a water processing facility

• US 9,618,438 B2
• Filed: 07/09/2013
• Issued: 04/11/2017
• Est. Priority Date: 09/09/2009
• Status: Active Grant

• Current Assignee: Clearcorp Co.
• Original Assignee: Clearcorp
• Inventors: Jorden, Roger M.
• Primary Examiner(s): Keyworth, Peter
• Application Number:
  US13/937,918
• Publication Number:
  US 20130335731A1
• Time in Patent Office: 1,372 Days
• CPC Class Codes: C02F 1/5209 Regulation methods for flocculation or precipitation
• CPC Class Codes: C02F 2101/103 Arsenic compounds
• CPC Class Codes: C02F 2101/105 Phosphorus compounds
• CPC Class Codes: C02F 2101/14 Fluorine or fluorine-containing compounds
• CPC Class Codes: C02F 2101/20 Heavy metals or heavy metal compounds
• CPC Class Codes: C02F 2209/003 Downstream control, i.e. outlet monitoring, e.g. to check the treating agents, such as halogens or ozone, leaving the process
• CPC Class Codes: C02F 2209/006 comprising a software program or a logic diagram
• CPC Class Codes: C02F 2209/44 Time
• CPC Class Codes: C02F 2303/04 Disinfection
• CPC Class Codes: G01N 1/2035 by deviating part of a fluid stream, e.g. by drawing-off or tapping
• CPC Class Codes: G01N 15/0227 using imaging; using holography
• CPC Class Codes: G01N 2001/1012 Suspensions
• CPC Class Codes: G01N 33/18 Water

Abstract

A system and method for isolating and analyzing a water sample in a water processing facility are disclosed. The system uses a chamber for receiving and isolating the water sample from the main water treatment process. An optical detector views and characterizes the particles in a region of the chamber. An analyzer coupled to the optical detector compares the characterized suspended particles at a first time and at with the characterized suspended particles at a second time to produce a report showing suspended particle size as a function of time.

Claims

1. A system for isolating and analyzing a plurality of water and coagulant chemical samples in a water processing facility, the system comprising:

an isolatable chamber for receiving the water and coagulant samples wherein the isolatable chamber further comprises a closable outlet valve located at the bottom of the chamber and an inlet located in a region proximate to the top of the chamber wherein;

the inlet is configured to receive a first sample comprising water and a first quantity of a coagulant chemical at a first time period;

the system comprises the first sample;

the closeable outlet valve and the inlet are configured to isolate the first sample in the chamber from the rest of the water processing facility at a second time period, whereby the first sample in the chamber can become sufficiently quiescent to allow gravitational settling of suspended particles in the first sample in the chamber;

the closable outlet valve is configured to release the first sample at a third time period;

the inlet is configured to receive a second sample comprising water and a second quantity of the coagulant chemical at a fourth time period, wherein the second quantity is different from the first quantity;

the system comprises the second sample; and

the outlet valve and the inlet are configured to isolate the second sample from the rest of the water processing facility at a fifth time period;

an optical detector configured to view and characterize the sizes of a plurality of suspended particles;

in a region of the first sample in the chamber at the second time period; and

in a region of the second sample in the chamber at the fifth time period,

wherein the first sample region and the second sample region protrude into the chamber;

a controller comprising a processor and software wherein the controller is configured to;

send signals that open and close the outlet valve;

receive particle size information from the optical detector, wherein the particle size information comprises;

the characterized suspended particle sizes in the first sample at a first time point, wherein the first time point is during the second time period;

the characterized suspended particle sizes in the first sample at a second time point, wherein the second time point is during the second time period;

the characterized suspended particle sizes in the second sample at a third time point, wherein the third time point is during the fifth time period; and

characterized suspended particle sizes in the second sample at a fourth time point, wherein the fourth time point is during the fifth time period;

wherein;

the first time period, the second time period, the third time period, the fourth time period, and the fifth time period occur sequentially; and

the first time point, the second time point, the third time point, and the fourth time point occur sequentially; and

produce a report showing suspended particle size as a function of time and coagulant chemical quantity;

whereby coagulant dosing is adjusted according to the report.

2. The system as recited in claim 1, wherein:

the inlet further comprises a closable inlet valve;

the controller communicates a mixer control signal to a mixer wherein;

the mixer is at least partially located in the chamber;

the controller is configured to turn the mixer on during the first part of the first time period and to turn the mixer off during the second part of the first time period;

the optical detector is configured to view and characterize the sizes of a plurality of particles during the first part of the first time period and the second part of the first time period;

the controller is configured to turn the mixer on during the first part of the second time period and to turn the mixer off during the second part of the second time period;

the optical detector is configured to view and characterize the sizes of a plurality of particles during the first part of the second time period and the second part of the second time period; and

the controller is configured to send signals that open and close the inlet valve.

3. The system as recited in claim 2, wherein the controller is further configured to process a plurality of time-sequential optical images and recorded times from each image to:

determine a first position of the specific particle in a first time-sequential optical image at a first recorded time wherein the first position further comprises a first vertical position;

track the floc particle from the first time-sequential image to a second time-sequential image at a second recorded time;

determine a second position of the specific particle in the second time-sequential image wherein the second position further comprises a second vertical position;

compute a vertical displacement from the difference between the second vertical position and the first vertical position;

compute a time difference between the first recorded time and the second recorded time; and

compute a gravitational settling velocity in response to the vertical displacement and the time difference.

4. The system as recited in claim 2, wherein:

the mixer control signal further comprises a signal selected from the group of;

an on signal;

an off signal;

a duty-cycle signal;

a power signal; and

a mixing speed signal; and

the mixer control signal is responsive to shear wherein shear is calculated as the mixer power input divided by the unit volume of the mixed volume.

5. The system as recited in claim 2, wherein:

the controller is responsive to the optical detector; and

the mixer control signal is responsive to a characteristic of a suspended floc particle in a region selected from the group of;

the first sample region; and

the second sample region.

6. The system as recited in claim 2, wherein:

the inlet is configured to selectively receive the first sample and the second sample from a location in the water processing facility selected from the group of;

a point downstream from a chemical addition point; and

a point downstream from a simulation coagulation system; and

the outlet is configured to release the first sample and the second sample to a waste location external to the water processing facility.

7. The system as recited in claim 1, wherein:

the system receives the first sample and the second sample from a point in the water processing facility downstream of a chemical addition point;

the inlet comprises a closable inlet valve proximate to the top of the isolatable chamber;

the isolatable chamber is configured to be fully submerged in a tank of the water processing facility; and

the isolatable chamber further comprises a vertical tube section.

8. The system as recited in claim 1, wherein the first sample region and the second sample region have a lower boundary at least 10% above the bottom of the closeable outlet valve in the isolatable chamber and the first sample region and the second sample region have an upper boundary no more than 50% above the bottom of the closeable outlet valve in the isolatable chamber, wherein the 10% and the 50% are measured vertically based on the closable outlet valve being the bottom of the isolatable chamber and the higher of the inlet or the level to which the isolatable chamber is normally filled being the top of the isolatable chamber.

9. The system as recited in claim 1, wherein:

the system further comprises a mixer;

the controller is configured to turn the mixer on and off;

the inlet comprises a closable inlet valve;

the controller is configured to open and close the inlet valve

the controller is configured to open and close the outlet valve; and

the system is configured for;

directly measuring water processing facility floc particle size at a sampling point in the water processing facility by opening the inlet valve, opening the outlet valve, turning the mixer off and using the optical detector to view floc particles;

measuring changes in water processing facility floc particle size as a function of time by closing the inlet valve, closing the outlet valve, turning the mixer on, and using the optical detector to view floc particles; and

measuring floc particle gravitational settling velocity by closing the inlet valve, closing the outlet valve; and

turning the mixer off, and using the optical detector to view floc particles.

10. The system of claim 1 wherein:

the system calculates a suspended particle size by determining a three-dimensional particle volume;

the three-dimensional particle volume for the suspended particle is calculated from a computed perimeter and a computed two-dimensional apparent frontal area;

the controller is responsive to a signal from the water treatment facility control network; and

the water treatment facility control network is responsive to a signal from the controller.

11. The system of claim 1 wherein:

the isolatable chamber further comprises a fresh water spray system; and

the fresh water spray system is configured for cleaning the chamber.

12. The system of claim 1 wherein:

the system is configured for attachment to a water treatment facility control network;

the system further comprises a mixer;

the mixer is configured to be turned on or off by the controller; and

the system is configured for operation in all of the following modes;

the outlet valve is open, the mixer is turned off, and the optical detector measures particle size in liquid and coagulant chemical samples at a sampling point in the processing facility;

the outlet valve is closed, the mixer is turned on, and the optical detector measures particle size changes of isolated stirred liquid and coagulant chemical samples over time; and

the outlet valve is closed, the mixer turned off, and the optical detector measures position changes for floc particles in quiescent isolated liquid and coagulant chemical samples over time.

13. The system of claim 1 wherein:

the coagulant chemical contains an organic polymer coagulant comprising a counterion; and

the quantity of the organic polymer coagulant in the second sample is different from the quantity of the organic polymer coagulant in the first sample.

14. A coagulant chemical test simulation system for a processing facility, the system comprising:

a first liquid and coagulant chemical sample;

a second liquid and coagulant chemical sample;

a chamber for receiving a plurality of discrete samples of liquid and coagulant chemical wherein the chamber further comprises a closable outlet valve located at the bottom of the chamber and an inlet located in a region proximate to the top of the chamber wherein the closeable outlet valve and the inlet are configured to sequentially;

isolate the first liquid and coagulant chemical sample in the chamber from the rest of the processing facility by closing the closable outlet valve, wherein the first liquid and coagulant chemical sample was obtained from the processing facility;

hold the first liquid and coagulant chemical sample in the chamber for a first time period by keeping the outlet valve closed;

open the outlet valve to release the first liquid and coagulant chemical sample;

isolate the second liquid and coagulant chemical sample in the chamber from the rest of the processing facility by closing the outlet valve, wherein the second liquid and coagulant chemical sample was obtained from the processing facility; and

hold the first liquid and coagulant chemical sample in the chamber for a second time period by keeping the outlet valve closed;

open the outlet valve to release the second liquid and coagulant chemical sample;

an optical detector configured to view and characterize the sizes of a plurality of suspended particles;

in the first liquid and coagulant sample when the first sample is located in a region of the chamber at a first time and a second time during the first period; and

in the second liquid and coagulant sample when the second sample is located in the region of the chamber at a third time and a fourth time during the second period;

a controller comprising a processor and software wherein the controller is configured to send signals that;

open and close the outlet valve; and

control the optical detector; and

a computing engine coupled to the optical detector that is configured to compares the characterized suspended particle sizes at;

the first time;

the second time;

the third time; and

the fourth time

to produce a report showing suspended particle size as a function of time and liquid and coagulant chemical sample number.

15. The system as recited in claim 14, wherein the inlet is configured to selectively receive the first discrete sample and the second discrete sample from a location in the processing facility selected from the group of:

a point downstream from a chemical addition point; and

a point downstream from a simulation coagulation system.

16. The system as recited in claim 14, wherein the inlet further comprises a closable inlet valve, and wherein the controller:

is configured to communicates a mixer control signal to a mixer located in the chamber; and

is configured to send signals that open and close the inlet valve.

17. The system as recited in claim 14, wherein:

the computed suspended particle perimeter is determined and stored in memory separately from the computed suspended particle two-dimensional apparent frontal area;

the computed perimeter is responsive to the optical detector and an edge detection algorithm;

the computed apparent frontal area is responsive to the optical detector and a closed object identification algorithm; and

the calculated three-dimensional particle volume is calculated from the stored computed perimeter and the stored computed apparent frontal area using the average of the Heywood equation and the hydraulic equation wherein;

the Heywood equation uses the formula;

18. The system as recited in claim 14, wherein:

the chamber receives the plurality of discrete liquid and coagulant chemical samples from a point downstream of a coagulant chemical addition point;

the inlet comprises a closable valve;

the chamber is configured to be fully submerged in a tank of the processing facility; and

the chamber further comprises a vertical tube section.