Method of manufacturing bulked continuous filament

• US 9,636,860 B2
• Filed: 11/18/2014
• Issued: 05/02/2017
• Est. Priority Date: 05/31/2012
• Status: Active Grant

• Current Assignee: Aladdin Manufacturing Corporation (Mohawk Industries Incorporated)
• Original Assignee: Mohawk Industries Incorporated
• Inventors: Clark, Thomas R.
• Primary Examiner(s): Tentoni, Leo B
• Application Number:
  US14/546,796
• Publication Number:
  US 20150076744A1
• Time in Patent Office: 896 Days
• Field of Search: 264 401, 264101, 264102, 264140, 264169, 2641761, 26421121, 26421122, 26421123
• CPC Class Codes: B29B 13/06 by drying B29B13/08 takes precedence ; drying moulded articles or half products B29C37/0092
• CPC Class Codes: B29B 17/0026 by agglomeration or compacting
• CPC Class Codes: B29B 17/02 Separating plastics from other materials
• CPC Class Codes: B29B 17/0412 to large particles, e.g. beads, granules, flakes, slices
• CPC Class Codes: B29B 2013/005 Degassing undesirable residual components, e.g. gases, unreacted monomers, from material to be moulded
• CPC Class Codes: B29B 2017/0015 Washing, rinsing
• CPC Class Codes: B29B 2017/0279 Optical identification, e.g. cameras or spectroscopy
• CPC Class Codes: B29B 2017/0289 Washing the materials in liquids
• CPC Class Codes: B29B 7/485 with three or more shafts provided with screws
• CPC Class Codes: B29B 7/86 for working at sub- or superatmospheric pressure B01F33/70 takes precedence
• CPC Class Codes: B29C 2791/003 Making articles of indefinite length B29C53/48 takes precedence
• CPC Class Codes: B29C 2791/006 Using vacuum
• CPC Class Codes: B29C 2948/922 Viscosity; Melt flow index [MFI]; Molecular weight
• CPC Class Codes: B29C 2948/92514 Pressure
• CPC Class Codes: B29C 2948/92838 Raw material pre-treatment, e.g. drying or cleaning
• CPC Class Codes: B29C 37/006 Degassing moulding material or draining off gas during moulding venting means in moulds B29C33/10
• CPC Class Codes: B29C 48/0022 combined with cutting
• CPC Class Codes: B29C 48/02 Small extruding apparatus, e.g. handheld, toy or laboratory extruders
• CPC Class Codes: B29C 48/022 characterised by the choice of material
• CPC Class Codes: B29C 48/05 Filamentary, e.g. strands
• CPC Class Codes: B29C 48/144 : at the plasticising zone
• CPC Class Codes: B29C 48/267 : Intermediate treatments, e.g. relaxation, annealing or decompression step for the melt B29C48/76 takes precedence
• CPC Class Codes: B29C 48/38 : using two or more serially arranged screws in the same barrel
• CPC Class Codes: B29C 48/385 : using two or more serially arranged screws in separate barrels
• CPC Class Codes: B29C 48/40 : using two or more parallel screws or at least two parallel non-intermeshing screws, e.g. twin screw extruders
• CPC Class Codes: B29C 48/404 : the screws having non-intermeshing parts
• CPC Class Codes: B29C 48/425 : using three or more screws serially arranged screws B29C48/38, B29C48/385
• CPC Class Codes: B29C 48/43 : Ring extruders
• CPC Class Codes: B29C 48/435 : Sub-screws
• CPC Class Codes: B29C 48/44 : Planetary screws
• CPC Class Codes: B29C 48/69 : Filters or screens for the moulding material
• CPC Class Codes: B29C 48/70 : comprising means for dividing, distributing and recombining melt flows
• CPC Class Codes: B29C 48/92 : Measuring, controlling or regulating
• CPC Class Codes: B29D 99/0078 : Producing filamentary materials
• CPC Class Codes: B29K 2067/003 : PET, i.e. poylethylene terephthalate
• CPC Class Codes: B29K 2105/26 : Scrap or recycled material
• CPC Class Codes: B29L 2031/731 : Filamentary material, i.e. comprised of a single element, e.g. filaments, strands, threads, fibres cables B29L2031/707
• CPC Class Codes: C08J 11/04 : of polymers
• CPC Class Codes: C08J 2367/02 : Polyesters derived from dicarboxylic acids and dihydroxy compounds; C08J2367/06 takes precedence
• CPC Class Codes: D01D 1/103 : De-aerating
• CPC Class Codes: D01D 1/106 : Filtering
• CPC Class Codes: D01D 5/08 : Melt spinning methods D01D5/0023 takes precedence
• CPC Class Codes: D01F 6/62 : from polyesters
• CPC Class Codes: D02G 3/24 : Bulked yarns or threads, e.g. formed from staple fibre components with different relaxation characteristics
• CPC Class Codes: Y02P 20/143 : the feedstock being recycled material, e.g. plastics
• CPC Class Codes: Y02W 30/62 : Plastics recycling; Rubber recycling

Abstract

A method of manufacturing bulked continuous carpet filament which, in various embodiments, comprises: (A) grinding recycled PET bottles into a group of flakes; (B) washing the flakes; (C) identifying and removing impurities, including impure flakes, from the group of flakes; (D) passing the flakes through a PET crystallizer; (E) passing the group of flakes through an MRS extruder while maintaining the pressure within the MRS portion of the MRS extruder below about 18 millibars; (F) passing the resulting polymer melt through at least one filter having a micron rating of less than about 50 microns; and (G) forming the recycled polymer into bulked continuous carpet filament that consists essentially of recycled PET.

Claims

1. A method of manufacturing bulked continuous carpet filament, said method comprising:

(A) providing a PET crystallizer;

(B) passing a plurality of flakes of recycled PET through said PET crystallizer to at least partially dry said plurality of flakes of recycled PET;

(C) at least partially melting said plurality of flakes into a polymer melt;

(D) providing a multi-screw extruder that comprises;

(i) a first satellite screw extruder, said first satellite screw extruder comprising a first satellite screw that is mounted to rotate about a central axis of said first satellite screw;

(ii) a second satellite screw extruder, said second satellite screw extruder comprising a second satellite screw that is mounted to rotate about a central axis of said second satellite screw; and

(iii) a satellite screw extruder support system that is adapted to rotate said first and second satellite screws about a main axis while said first and second satellite screws are rotating about their respective central axes, said main axis being substantially parallel to;

(a) said central axis of said first satellite screw; and

(b) said central axis of said second satellite screw, wherein said first satellite screw and second satellite screw are disposed within respective extruder barrels;

(iv) a pressure regulation system that is adapted to maintain a pressure within said first and second satellite screw extruders below about 18 millibars;

(E) using said pressure regulation system to reduce a pressure within said first and second satellite screw extruders to below about 18 millibars;

(F) after said step of passing said plurality of flakes through said PET crystallizer, melting said plurality of flakes of recycled PET to form a polymer melt and, while maintaining said pressure within said first and second satellite screw extruders below about 18 millibars, passing said polymer melt through said multi-screw extruder so that;

(1) a first portion of said polymer melt passes through said first satellite screw extruder, and (2) a second portion of said polymer melt passes through said second satellite screw extruder; and

(G) after said step of passing said polymer melt through said multi-screw extruder, forming said polymer melt into bulked continuous carpet filament.

2. The method of claim 1, wherein said PET crystallizer comprises:

a hopper screw configured to feed said plurality of flakes into said PET crystallizer; and

a blower configured to blow hot air over said plurality of flakes as said plurality of flakes pass through said crystallizer.

3. The method of claim 2, wherein said crystallizer is configured to maintain a temperature of between about 140 degrees Celsius and about 180 Celsius within said crystallizer.

4. The method of claim 3, wherein said crystallizer is configured to maintain a temperature of about 140 degrees Celsius within said crystallizer.

5. The method of claim 1, wherein said crystallizer is configured to at least partially crystallize said plurality of flakes.

6. The method of claim 1, wherein said crystallizer is configured to at least partially dry at least a portion of a surface of said plurality of flakes.

7. The method of claim 6, wherein said crystallizer is configured to reduce a moisture content of said plurality of flakes to between about 30 ppm and about 50 ppm.

8. A method of manufacturing carpet filament comprising the steps of:

(A) grinding a plurality of recycled PET bottles into a group of polymer flakes;

(B) washing said group of polymer flakes to remove at least a portion of one or more contaminants from a surface of said flakes, said group of flakes comprising a first plurality of flakes that consist essentially of PET and a second plurality of flakes that do not consist essentially of PET;

(C) after said step of washing said first plurality of flakes;

(i) scanning said washed group of flakes to identify said second plurality of flakes,

(ii) separating said second plurality of flakes from said first plurality of flakes;

(D) providing a PET crystallizer;

(E) passing said first plurality of flakes through said PET crystallizer to at least partially dry said first plurality of flakes;

(F) melting said second plurality of flakes to produce a polymer melt;

(G) providing an extruder that extrudes material in a plurality of different extrusion streams and comprises;

at least two satellite screws wherein each respective satellite screw of the at least two satellite screws is mounted to rotate about its respective central axis; and

a single screw drum mounted to rotate about its central axis, wherein;

said central axis of said single screw drum is parallel to each respective central axis of said at least two satellite screws;

said at least two satellite screws are arranged within said single screw drum and at least partially housed within respective extruder barrels; and

each of said at least two satellite screws is configured to rotate about its said respective axis while said single screw drum rotates about said central axis of said single screw drum;

(H) reducing a pressure within said extruder to between about 0 millibars and about 12 millibars;

(I) while maintaining said pressure within said extruder between about 0 millibars and about 12 millibars, passing said polymer melt through said extruder so that said polymer melt is divided into a plurality of extrusion streams and at least a portion of said polymer melt passes through each of said at least two satellite screws, each having a pressure between about 0 millibars and about 12 millibars;

(J) after passing said polymer melt through said extruder, filtering said polymer melt through at least one filter; and

(K) after passing said polymer melt through said filter, forming said polymer melt into bulked continuous carpet filament.

9. The method of claim 8, wherein reducing said pressure within said extruder to between about 0 millibars and about 12 millibars comprises:

determining a source of said recycled PET bottles;

at least partially in response to determining that said source of said recycled PET bottles comprises deposit PET bottles, reducing said pressure within said extruder to a first pressure between about 0 millibars and about 12 millibars; and

at least partially in response to determining that said source of said recycled PET bottles comprises deposit curbside recycled PET bottles, reducing said pressure within said extruder to a second pressure between about 0 millibars and about 12 millibars.

10. The method of claim 9 wherein said first pressure is greater than said second pressure.

11. The method of claim 8, wherein said crystallizer comprises:

a hopper screw configured to feed said plurality of flakes into said crystallizer; and

a blower configured to blow hot air over said plurality of flakes as said plurality of flakes pass through said crystallizer.

12. The method of claim 11, wherein said crystallizer is configured to maintain a temperature of between about 140 degrees Celsius and about 180 degrees Celsius within said crystallizer.

13. The method of claim 12, wherein said crystallizer is configured to maintain a temperature of about 180 degrees Celsius within said crystallizer.

14. The method of claim 8, wherein said crystallizer is configured to at least partially crystallize said plurality of flakes.

15. The method of claim 8, wherein said crystallizer is configured to reduce a moisture content of said plurality flakes to between about 30 ppm and about 50 ppm.

16. The method of claim 15, wherein said crystallizer is configured to sufficiently reduce said moisture content of said plurality of flakes such that said plurality of flakes do not substantially stick to one another.

17. A method of manufacturing bulked continuous carpet filament, said method comprising:

(A) providing a PET crystallizer that comprises;

(i) a hopper screw configured to feed a plurality of flakes into said crystallizer; and

(ii) at least one heating element configured to increase a temperature within said PET crystallizer;

(B) passing a plurality of flakes consisting essentially of PET flakes through said PET crystallizer to at least partially dry said first plurality of flakes;

(C) after passing said plurality of flakes though said PET crystallizer, melting said plurality of flakes to form a polymer melt;

(D) providing a multi-screw extruder that comprises;

(i) a first satellite screw extruder, said first satellite screw extruder comprising a first satellite screw that is mounted to rotate about a central axis of said first satellite screw;

(ii) a second satellite screw extruder, said second satellite screw extruder comprising a second satellite screw that is mounted to rotate about a central axis of said second satellite screw;

(iii) a third satellite screw extruder, said third satellite screw extruder comprising a third satellite screw that is mounted to rotate about a central axis of said third satellite screw;

(iv) a fourth satellite screw extruder, said fourth satellite screw extruder comprising a fourth satellite screw that is mounted to rotate about a central axis of said fourth satellite screw, wherein said first satellite screw, said second satellite screw, said third satellite screw, and said fourth satellite screw are disposed at least partially within respective extruder barrels;

(v) a satellite screw extruder support system that is adapted to rotate said first, second, third, and fourth satellite screws about a main axis while said first, second, third and fourth satellite screws are rotating about their respective central axes, said main axis being substantially parallel to;

(a) said central axis of said first satellite screw;

(b) said central axis of said second satellite screw;

(c) said central axis of said third satellite screw; and

(d) said central axis of said fourth satellite screw; and

(vi) a pressure regulation system that is adapted to maintain a pressure within said first, second, third, and fourth satellite screw extruders between about 0 millibars and about 18 millibars;

(E) using said pressure regulation system to reduce a pressure within said first, second, third, and fourth satellite screw extruders to between about 0 millibars and about 18 millibars;

(F) while maintaining said pressure within said first, second, third, and fourth satellite screw extruders between about 0 millibars and about 18 millibars, passing said polymer melt through said multi-screw extruder so that;

(1) a first portion of said melt passes through said first satellite screw extruder, (2) a second portion of said melt passes through said second satellite screw extruder, (3) a third portion of said melt passes through said third satellite screw extruder, and (4) a fourth portion of said melt passes through said fourth satellite screw extruder; and

(G) after said step of passing said polymer melt through said multi-screw extruder, forming said polymer melt into bulked continuous carpet filament.

18. The method of claim 17, wherein said at least one heating element is configured to maintain a temperature of between about 140 degrees Celsius and about 180 degrees Celsius within said crystallizer.

19. The method of claim 18, wherein said at least one heating element comprises at least one infrared heating element.

20. The method of claim 17, wherein:

said crystallizer is configured to reduce a moisture content of said plurality of flakes to between about 30 ppm and about 50 ppm; and

passing said plurality of flakes consisting essentially of recycled PET through said PET crystallizer to at least partially dry said plurality of flakes comprises reducing said moisture content of said plurality of flakes to between about 30 ppm and about 50 ppm.