Method for making amorphous particles using a uniform melt-state in a microwave generated plasma torch
First Claim
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1. A method of producing amorphous powder particles comprising:
- introducing a feed material as precursor droplets from a feed injection device into a microwave plasma torch;
entraining said feed material using laminar flow towards a microwave generated plasma;
exposing said feed material to the microwave generated plasma to form plasma exhaust gas;
quenching the plasma exhaust gas of said microwave generated plasma at a rate in the same order of magnitude of 106 K/s to form amorphous powder particle products;
filtering the quenched plasma exhaust gas of said microwave generated plasma; and
extracting amorphous powder particle products from said filtered plasma exhaust gas.
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Abstract
Feed material comprising uniform solution precursor droplets is processed in a uniform melt state using microwave generated plasma. The plasma torch employed is capable of generating laminar gas flows and providing a uniform temperature profile within the plasma. Plasma exhaust products are quenched at high rates to yield amorphous products. Products of this process include spherical, highly porous and amorphous oxide ceramic particles such as magnesia-yttria (MgO—Y2O3). The present invention can also be used to produce amorphous non oxide ceramic particles comprised of Boron, Carbon, and Nitrogen which can be subsequently consolidated into super hard materials.
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13 Claims
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1. A method of producing amorphous powder particles comprising:
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introducing a feed material as precursor droplets from a feed injection device into a microwave plasma torch; entraining said feed material using laminar flow towards a microwave generated plasma; exposing said feed material to the microwave generated plasma to form plasma exhaust gas; quenching the plasma exhaust gas of said microwave generated plasma at a rate in the same order of magnitude of 106 K/s to form amorphous powder particle products; filtering the quenched plasma exhaust gas of said microwave generated plasma; and extracting amorphous powder particle products from said filtered plasma exhaust gas. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13)
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