Sample cell filling device for use remotely from a polarimeter and method of using the same

• US 9,677,995 B2
• Filed: 01/13/2015
• Issued: 06/13/2017
• Est. Priority Date: 01/13/2015
• Status: Active Grant

• Current Assignee: Rudolph Research Analytical Corporation
• Original Assignee: Rudolph Research Analytical Corporation
• Inventors: Wagner, Jeff, Spanier, Richard C.
• Primary Examiner(s): Chowdhury, Tarifur
• Assistant Examiner(s): Akanbi, Isiaka
• Application Number:
  US14/595,266
• Publication Number:
  US 20160202176A1
• Time in Patent Office: 882 Days
• Field of Search: 356440, 356364, 356436, 356336
• CPC Class Codes: G01J 4/00 Measuring polarisation of light
• CPC Class Codes: G01N 21/11 Filling or emptying of cuvettes
• CPC Class Codes: G01N 21/21 Polarisation-affecting properties G01N21/19 takes precedence

Abstract

A sample cell filling device for filling a sample cell to be used remotely from a polarimeter is provided. The filling device includes a liquid-sealed housing, light source and a diffuser viewing screen. The housing has a recess for receiving the sample cell, the sample cell having first and second optical windows at the respective ends. A light source transmits light from one optical window to the other optical window. A diffuser viewing screen receives light exiting from the sample cell such that light from the viewing screen can be observed by a user to determine the quality of the sample fill.

Claims

1. A sample cell filling device for filling a sample cell to be used remotely from a polarimeter comprising:

a liquid-sealed housing having a recess for receiving and supporting the sample cell at an inclined angle, the sample cell having;

a first optical window at a first end and a second optical window at a second end along a longitudinal axis of the sample cell; and

a first filling port located near the first end and a second filling port located near the second end, at least one of the first and second filling ports adapted to form a temporary liquid tight seal when a sample injecting device is received therein;

a light source that transmits light from the first optical window to the second optical window; and

a viewing screen, wherein light exiting the second optical window is directed to the viewing screen.

2. The sample cell filling device of claim 1, wherein the viewing screen is physically adapted to diffuse light.

3. The sample cell filling device of claim 2, wherein the viewing screen comprises ground glass.

4. The sample cell filling device of claim 1, further comprising:

a focusing lens disposed in an optical path between the second optical window and the viewing screen.

5. The sample cell filling device of claim 4, further comprising an aperture through which the light from the focusing lens passes.

6. The sample cell filling device of claim 5, further comprising a mirror disposed in an optical path between the aperture and the viewing screen to reflect the light from the aperture to the viewing screen.

7. The sample cell filling device of claim 1, further comprising a magnifier to provide a magnified view of the light.

8. The sample cell filling device of claim 1, wherein at least one of the first and second filling ports is positioned at an angle relative to the longitudinal axis of the sample cell such that the sample makes only a single change of direction when the sample is being filled in the sample cell.

9. The sample cell filling device of claim 8, wherein the longitudinal axis of the at least one filling port when the sample cell is positioned in the sample filling device is substantially at 90 degrees to the horizontal plane of the sample cell filling device.

10. The sample cell filling device of claim 1, wherein the inclined angle is between about 10 to 50 degrees relative to a horizontal plane.

11. A sample cell filling device for filling a sample cell externally of and to be used remotely in a polarimeter comprising:

a liquid-sealed housing having a recess for receiving the sample cell at an angle between about 10 to about 50 degrees relative to a horizontal plane, the sample cell having a first optical window at a first end and a second optical window at a second end along a longitudinal axis thereof;

a light source positioned within the liquid-sealed housing and operable to transmit light from the first optical window to the second optical window;

a focusing lens positioned within the sealed housing and to receive light from the second optical window;

a viewing screen, wherein the viewing screen receives light from the focusing lens, and further wherein the viewing screen is physically adapted to diffuse the light it receives.

12. The sample cell filling device of claim 11, wherein the viewing screen comprises ground glass, wherein the ground glass diffuses the light received at the viewing screen.

13. The sample cell filling device of claim 11, further comprising an aperture positioned at a focal point of the focusing lens.

14. The sample cell filling device of claim 13, further comprising a mirror disposed in an optical path between the aperture and the diffuser viewing screen to reflect the light from the aperture to the diffuser viewing screen.

15. The sample cell filling device of claim 11, further comprising the sample cell having a first filling port located near the first end and a second filling port located near the second end, wherein at least one of the first and second filling ports is inclined relative to the longitudinal axis of the sample cell such that the sample makes only a single change of direction when the sample is being filled in the sample cell.