High frequency uniform droplet maker and method

• US 9,782,791 B2
• Filed: 04/13/2016
• Issued: 10/10/2017
• Est. Priority Date: 09/28/2012
• Status: Active Grant

• Current Assignee: 6K Incorporated, University of Connecticut (State of Connecticut)
• Original Assignee: Amastan Technologies LLC, University of Connecticut (State of Connecticut)
• Inventors: Redjdal, Makhlouf, Hadidi, Kamal, Wrobel, Gregory, Jordan, Eric
• Primary Examiner(s): Jonaitis, Justin
• Application Number:
  US15/097,493
• Publication Number:
  US 20160228903A1
• Time in Patent Office: 545 Days
• Field of Search: 2391021, 2391022, 239690, 239699, 2392251, 239226, 239230, 239 4, 239260, 347 5, 347 9, 347 10, 347 11, 347 12, 347 20, 347 44, 347 47, 347 48, 347 57, 347 58, 347 59, 347 73, 347 74, 347 75
• CPC Class Codes: B05B 17/0607 generated by electrical means, e.g. piezoelectric transducers
• CPC Class Codes: B05B 17/0646 Vibrating plates, i.e. plates being directly subjected to the vibrations, e.g. having a piezoelectric transducer attached thereto
• CPC Class Codes: B05B 17/0669 Excitation frequencies

Abstract

Systems, methods, and devices are disclosed for producing substantially uniform droplets. The system includes a fluid reservoir vessel defining a fluid reservoir, a separation membrane at one end of the fluid reservoir, at least one capillary channel at an opposite end of the fluid reservoir, a solution dispenser, and a piezo actuator in contact with a separation membrane. The separation membrane has a thickness greater than about 0.2 mm, and the solution dispenser maintains the fluid reservoir filled with fluid such that the fluid simultaneously contacts the separation membrane and the capillary channel. The solution dispenser maintains the fluid reservoir under pressure to create a fluid stream exiting the capillary. The piezo actuator is in contact with the separation membrane on a side opposite that in contact with the fluid, and the piezo actuator transfers a pressure wave through the fluid in the fluid reservoir to break up the fluid stream into uniform droplets.

Claims

1. A system for producing droplets, the system comprising:

a fluid reservoir vessel defining a fluid reservoir;

a separation membrane, which is rigid in form, disposed at a first end of the fluid reservoir, the separation membrane having a thickness greater than about 0.2 mm;

one or more capillary channels disposed at a second end of the fluid reservoir opposite the separation membrane;

a solution dispenser in fluid communication with the fluid reservoir and disposed to maintain the fluid reservoir filled with fluid such that the fluid contacts the separation membrane and the one or more capillary channels, the solution dispenser further disposed to maintain the fluid reservoir under pressure to create a fluid stream exiting the one or more capillary channels; and

a piezo actuator in contact with the separation membrane on a side opposite that in contact with the fluid, the piezo actuator disposed to transfer a pressure wave through the fluid in the fluid reservoir to break up the fluid stream into droplets.

2. The system of claim 1, wherein the one or more capillary channels are formed in a capillary plate disposed at the second end of the fluid reservoir opposite the separation membrane.

3. The system of claim 2, wherein the one or more capillary channels are formed in the capillary plate using laser drilling, lithography, electron beam drilling, ion beam milling, chemical etching, plasma etching, water jet drilling, or electrical discharge machining (EDM).

4. The system of claim 2, wherein the capillary plate is formed of a metal, ceramic, alloy, or polymer material.

5. The system of claim 2, wherein the one or more capillary channels have an upstream diameter greater than a downstream diameter.

6. The system of claim 2, wherein the one or more capillary channels include a plurality of capillary channels formed in the capillary plate.

7. The system of claim 6, wherein the plurality of capillary channels are disposed symmetrically about a center of the capillary plate.

8. The system of claim 6, wherein the plurality of capillary channels are disposed on an area of the capillary plate smaller in diameter than a diameter of the piezo actuator.

9. The system of claim 1, wherein the one or more capillary channels include one or more capillaries received by a capillary plate disposed at the second end of the fluid reservoir opposite the separation membrane.

10. The system of claim 9, wherein the one or more capillaries are press-fitted into one or more holes disposed in the capillary plate.

11. A system for producing droplets, the system comprising:

a fluid reservoir vessel defining a fluid reservoir;

a separation membrane disposed at a first end of the fluid reservoir;

a capillary plate disposed at a second end of the fluid reservoir opposite the separation membrane, the capillary plate having one or more capillary channels formed therein;

a solution dispenser in fluid communication with the fluid reservoir and disposed to maintain the fluid reservoir filled with fluid such that the fluid contacts the separation membrane and the capillary plate, the solution dispenser further disposed to maintain the fluid reservoir under pressure to create a fluid stream exiting the one or more capillary channels; and

a piezo actuator in contact with the separation membrane on a side opposite that in contact with the fluid, the piezo actuator disposed to activate at a resonant frequency to transmit a plurality of perturbation waves through the fluid to break up the fluid stream into substantially uniform droplets.

12. The system of claim 11, wherein the one or more capillary channels include a plurality of capillary channels formed in the capillary plate.

13. The system of claim 12, wherein the plurality of perturbation waves are evenly distributed to the plurality of capillary channels.

14. The system of claim 12, wherein the plurality of capillary channels are disposed symmetrically about a center of the capillary plate.

15. The system of claim 12, wherein the plurality of capillary channels are disposed on an area of the capillary plate smaller in diameter than a diameter of the piezo actuator.

16. The system of claim 11, wherein the one or more capillary channels are formed in the capillary plate using laser drilling, lithography, electron beam drilling, ion beam milling, chemical etching, plasma etching, water jet drilling, or electrical discharge machining (EDM).

17. The system of claim 11, wherein the capillary plate is formed of a metal, ceramic, alloy, or polymer material.

18. The system of claim 11, wherein the one or more capillary channels have an upstream diameter greater than a downstream diameter.

19. The system of claim 11, wherein the solution dispenser is disposed to transfer the fluid to the fluid reservoir proximal to the capillary plate.

20. A method for producing droplet streams, the method comprising:

filling a fluid reservoir vessel with a solution, the fluid reservoir vessel including a separation membrane having a thickness greater than about 0.2 mm disposed at a first end, and a capillary plate disposed at a second end opposite the separation membrane, the capillary plate having one or more capillary channels formed therein;

contacting the solution in the fluid reservoir vessel with a first side of the separation membrane;

ejecting a stream of the solution from the one or more capillary channels;

activating a piezo actuator disposed at a second side of the separation membrane opposite the first side to send a plurality of perturbation pulses to the separation membrane at a resonant frequency to create a plurality of perturbation waves through the solution; and

breaking up the stream of solution into a droplet stream using the plurality of perturbation waves.