Methods for forming near net-shape metal parts from binderless metal powder

• US 9,782,828 B2
• Filed: 10/20/2014
• Issued: 10/10/2017
• Est. Priority Date: 10/20/2014
• Status: Active Grant

• Current Assignee: The Boeing Co.
• Original Assignee: The Boeing Co.
• Inventors: Wilkinson, Carey E.
• Primary Examiner(s): Roe, Jessee
• Assistant Examiner(s): MAI, NGOCLAN THI
• Application Number:
  US14/518,997
• Publication Number:
  US 20160107235A1
• Time in Patent Office: 1,086 Days
• Field of Search: None
• CPC Class Codes: B22F 1/06 Metallic powder characterised by the shape of the particles nanosized particles B22F1/054
• CPC Class Codes: B22F 1/065 Spherical particles
• CPC Class Codes: B22F 1/09 Mixtures of metallic powders
• CPC Class Codes: B22F 2998/10 Processes characterised by the sequence of their steps
• CPC Class Codes: B22F 3/02 Compacting only
• CPC Class Codes: B22F 3/04 by applying fluid pressure , e.g. by cold isostatic pressing [CIP]
• CPC Class Codes: B22F 3/093 using vibrations or friction
• CPC Class Codes: B22F 3/10 Sintering only

Abstract

Systems and methods for forming near net-shape metal parts from binderless metal powder are disclosed. Systems include a mold die that defines a die cavity and may include one or more ultrasonic transducers operatively coupled to the mold die. Systems may be configured to introduce binderless metal powder into a die cavity and/or to compact the binderless metal powder within the die cavity. Methods include introducing binderless metal powder into a die cavity of a mold die and compacting the binderless metal powder within the die cavity to form a green part within the die cavity. The binderless metal powder may include spheroidal metal particles and angular metal particles. The methods may further include separating the green part from the mold die and sintering the green part, after separating, to form a sintered near net-shape metal part.

Claims

1. A method for forming a near net-shape metal part, the method comprising:

introducing binderless metal powder into a die cavity; and

compacting the binderless metal powder within the die cavity to form a green part within the die cavity;

wherein the binderless metal powder includes spheroidal metal particles and angular metal particles, and wherein a weight percentage of the angular metal particles in the binderless metal powder is greater than 50%.

2. The method of claim 1, wherein the spheroidal metal particles consist essentially of at least one of titanium particles and titanium alloy particles, and wherein the angular metal particles consist essentially of at least one of titanium particles and titanium alloy particles.

3. The method of claim 1, wherein the introducing includes distributing the binderless metal powder within the die cavity with ultrasonic energy.

4. The method of claim 1, wherein the compacting includes compacting with ultrasonic energy.

5. The method of claim 1, further comprising isostatic pressing the green part.

6. The method of claim 1, wherein the introducing and the compacting are performed to form the green part with a weight percentage of carbon of less than 5%.

7. The method of claim 1, wherein the introducing and the compacting are performed to form the green part with a weight percentage of oxygen of less than 1%.

8. The method of claim 1, further comprising sintering the green part to form the near net-shape metal part.

9. The method of claim 8, wherein the near net-shape metal part after the sintering has a volume at least 80% of a volume of the green part.

10. The method of claim 8, wherein the near net-shape metal part after the sintering has a density of at least 90% of a density of a bulk metal formed from the binderless metal powder.

11. The method of claim 1, wherein the die cavity is defined by a mold die that defines a sprue configured to introduce material into the die cavity and wherein the introducing includes introducing the binderless metal powder through the sprue into the die cavity.

19. The method of claim 1, wherein the angular metal particles have an average effective diameter that is greater than an average effective diameter of the spheroidal metal particles.

12. A method for forming a sintered near net-shape metal part, the method comprising:

introducing binderless metal powder into a die cavity of a mold die;

compacting the binderless metal powder within the die cavity by inducing ultrasonic vibrations in the mold die to form a green part within the die cavity;

separating the green part from the mold die; and

sintering, after the separating, the green part to form the sintered near net-shape metal part;

wherein the binderless metal powder includes spheroidal metal particles and angular metal particles, and wherein a weight percentage of the angular metal particles in the binderless metal powder is greater than 50%.

13. The method of claim 12, further comprising maintaining, during the introducing and the compacting, a temperature of the binderless metal powder at less than 80°

C.

14. The method of claim 12, wherein the compacting includes compacting the binderless metal powder with a pressure of less than 0.5 MPa.

15. The method of claim 12, wherein the introducing includes distributing the binderless metal powder within the die cavity with ultrasonic energy.

16. The method of claim 12, wherein the introducing includes filling the die cavity with the binderless metal powder.

17. The method of claim 12, wherein the mold die defines a sprue configured to introduce material into the die cavity and wherein the introducing includes introducing the binderless metal powder through the sprue into the die cavity.

18. The method of claim 12, wherein the binderless metal powder has a metal weight fraction of titanium of at least 80%.

20. The method of claim 12, wherein the angular metal particles have an average effective diameter that is greater than an average effective diameter of the spheroidal metal particles.