Stabilizer composition of microcrystalline cellulose and carboxymethylcellulose, method for making, and uses
First Claim
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1. A stabilizer composition comprisinga. microcrystalline cellulose (MCC), andb. a mixture of a first carboxymethyl cellulose (CMC) having a DS of 0.45-0.85 in an amount of 5% to 25% by weight of the total composition and a second carboxymethyl cellulose having a DS of 0.9-1.5 in an amount of 2%-20% by weight of the total composition,wherein the MCC of part (a) and the CMC of part (b) are present in a ratio of from 50:
- 50 to 95;
5 (MCC;
CMC), and wherein the stabilizer composition has an initial viscosity of at least 750 cps, a set-up viscosity of at least 3200 cps, and a set-up gel strength G′
of at least 20 Pa when dispersed in water at 2.6% solids concentration;
and wherein the composition is made by the following sequential process steps;
1. co-extruding a microcrystalline cellulose wetcake with a first carboxymethyl cellulose having a DS of 0.45-0.85 for sufficient attrition and interaction;
2. eitheri) blending a second carboxymethyl cellulose having a DS of 0.9-1.5 into the product of step 1, followed by extruding;
orii) preparing a water dispersion comprising the microcrystalline cellulose;
carboxymethyl cellulose extrudate of step 1 and a second carboxymethyl cellulose having a DS of 0.9-1.5; and
3. drying the product of step 2.
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Abstract
The subject matter of this invention is a composition and method of making a water-dispersible, stabilizing colloidal microcrystalline cellulose:xarboxymethylcellulose composition. The method of making the composition does not require a salt solution as an anti-slip agent.
100 Citations
12 Claims
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1. A stabilizer composition comprising
a. microcrystalline cellulose (MCC), and b. a mixture of a first carboxymethyl cellulose (CMC) having a DS of 0.45-0.85 in an amount of 5% to 25% by weight of the total composition and a second carboxymethyl cellulose having a DS of 0.9-1.5 in an amount of 2%-20% by weight of the total composition, wherein the MCC of part (a) and the CMC of part (b) are present in a ratio of from 50: - 50 to 95;
5 (MCC;
CMC), and wherein the stabilizer composition has an initial viscosity of at least 750 cps, a set-up viscosity of at least 3200 cps, and a set-up gel strength G′
of at least 20 Pa when dispersed in water at 2.6% solids concentration;and wherein the composition is made by the following sequential process steps; 1. co-extruding a microcrystalline cellulose wetcake with a first carboxymethyl cellulose having a DS of 0.45-0.85 for sufficient attrition and interaction; 2. either i) blending a second carboxymethyl cellulose having a DS of 0.9-1.5 into the product of step 1, followed by extruding;
orii) preparing a water dispersion comprising the microcrystalline cellulose;
carboxymethyl cellulose extrudate of step 1 and a second carboxymethyl cellulose having a DS of 0.9-1.5; and3. drying the product of step 2. - View Dependent Claims (2, 3, 4, 12)
- 50 to 95;
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5. A stabilizer composition comprising
a. microcrystalline cellulose; -
b. a carboxymethyl cellulose having a DS of 0.45-0.85 in an amount of 5%-25% by weight of the composition; and c. at least one additional hydrocolloid in an amount of 5%-50% by weight of the composition; wherein the stabilizer composition has an initial viscosity of at least 750 cps, a set-up viscosity of at least 3200 cps, and a set-up gel strength G′
of at least 20 Pa when dispersed in water at 2.6% solids concentration;wherein the composition is made by the following sequential process steps; I. co-extruding a microcrystalline cellulose wetcake with a carboxymethyl cellulose having a DS of 0.45-0.85 in an amount of 5%-25% by weight of the composition for sufficient attrition and interaction; ii. either (a) preparing a water dispersion comprising the microcrystalline cellulose;
carboxymethyl cellulose extrudate of step i and at least one additional hydrocolloid;
or(b) blending in at least one additional hydrocolloid to the product of step i., then extruding the admixture; and iii. drying the product of step ii. - View Dependent Claims (6, 7, 8, 9)
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10. An industrial suspension comprising a composition comprising microcrystalline cellulose, a first water-soluble carboxymethylcellulose having a degree of substitution of 0.45 to 0.85, and a second water-soluble carboxymethylcellulose having a degree of substitution of 0.9 to 1.5, wherein the weight ratio of the microcrystalline cellulose and the carboxymethyl cellulose is from 95:
- 5 to 70;
30, wherein upon dispersion in water at 2.6% solids the stabilizer composition has an initial viscosity of at least 750 cps, a set-up viscosity of at least 3200 cps, and a set-up gel strength G′
of at least 20 Pa, and wherein the stabilizing suspension is adapted for use in a pharmaceutical product, a nutraceutical product, a cosmetic product, a personal care product, a consumer product, an agricultural product, or a chemical formulation;and wherein the composition is made by the following sequential process steps; 1. co-extruding a microcrystalline cellulose wetcake with a first carboxymethyl cellulose having a DS of 0.45-0.85 for sufficient attrition and interaction; 2. either i) blending a second carboxymethyl cellulose having a DS of 0.9-1.5 into the product of step 1, followed by extruding;
orii) preparing a water dispersion comprising the microcrystalline cellulose;
carboxymethyl cellulose extrudate of step 1 and a second carboxymethyl cellulose having a DS of 0.9-1.5; and3. drying the product of step 2. - View Dependent Claims (11)
- 5 to 70;
Specification