Infrared spectrometer measurement of droplets collected from an oil mist in a breather pipe of a gas turbine

• US 9,863,873 B2
• Filed: 03/12/2013
• Issued: 01/09/2018
• Est. Priority Date: 03/27/2012
• Status: Active Grant

• Current Assignee: Siemens AG
• Original Assignee: Siemens AG
• Inventors: Brown, Roger, Pearce, Robert
• Primary Examiner(s): Porta, David
• Assistant Examiner(s): Malevic, Djura
• Application Number:
  US14/385,640
• Publication Number:
  US 20150076352A1
• Time in Patent Office: 1,764 Days
• Field of Search: 25033909, 250301, 2504921, 250343, 25033907, 2503385, 2503391, 250574
• CPC Class Codes: B01D 11/02 of solids
• CPC Class Codes: F01D 21/10 responsive to unwanted deposits on blades, in working-fluid conduits or the like
• CPC Class Codes: F01M 11/10 Indicating devices; Other safety devices
• CPC Class Codes: F01M 13/00 Crankcase ventilating or breathing
• CPC Class Codes: F16N 2250/50 Sampling
• CPC Class Codes: F16N 7/32 Mist lubrication splash lubrication F16N7/26
• CPC Class Codes: G01N 1/2035 by deviating part of a fluid stream, e.g. by drawing-off or tapping
• CPC Class Codes: G01N 1/2205 with filters
• CPC Class Codes: G01N 21/274 Calibration, base line adjustment, drift correction
• CPC Class Codes: G01N 21/3504 for analysing gases, e.g. multi-gas analysis
• CPC Class Codes: G01N 21/3554 for determining moisture content
• CPC Class Codes: G01N 33/2888 Lubricating oil characteristics, e.g. deterioration lubricating properties G01N33/30

Abstract

A method for analyzing a droplet fraction of an oil mist sample of a gas turbine is provided. A collecting device collects the oil mist sample, wherein the collecting device is arranged within a breather pipe which is coupled to the gas turbine such that oil mist is flowing through the breather pipe. The droplet fraction is separated from a gaseous fraction of the oil mist sample by a filter device, wherein the filter device is soaked with the droplet fraction, the droplet fraction is extracted from the filter device by using a tetrachloroethylene solvent. A composition of the droplet fraction is analyzed by a spectrometer.

Claims

1. A method for analysing a droplet fraction of an oil mist sample of a gas turbine, the method comprising:

collecting the oil mist sample by a collecting device, wherein the collecting device is arranged within a breather pipe which is coupled to the gas turbine such that oil mist is flowing through the breather pipe,

separating the droplet fraction from a gaseous fraction of the oil mist sample by a filter device, wherein the filter device is soaked with the droplet fraction,

extracting the droplet fraction from the filter device by using a tetrachloroethylene solvent, and

analysing a composition of the droplet fraction by a spectrometer.

2. The method according to claim 1, wherein the spectrometer is an infrared spectrometer.

3. The method according to claim 1, wherein the separating of the droplet fraction from the gaseous fraction of the oil mist sample is carried out by means of a wool element of the filter device;

and

wherein the filter device is arranged within the collecting device.

4. The method according to claim 3, further comprising after separating the droplet fraction from a gaseous fraction of the oil mist sample, guiding the gaseous fraction by a connecting line to a gaseous fraction analysing unit.

5. The method of claim 3, wherein the separating of the droplet fraction from the gaseous fraction of the oil mist sample is carried out by means of a quartz wool element of the filter device.

6. The method according to claim 1, wherein the filter device is arranged within the collecting device.

7. The method of claim 6, further comprising:

removing the filter device from the collecting device;

positioning the filter device in a separating unit to perform the extracting of the droplet fraction from the filter device; and

placing another filter device in the collecting device during the extracting step.

8. The method according to claim 1, further comprising calibrating the infrared spectrometer.

9. The method of claim 1, wherein the extracting the droplet fraction from the filter device comprises:

positioning the filter device in a separating unit; and

combining the tetrachloroethylene solvent and the filter device within the separating unit to form the composition of the droplet fraction.

10. The method of claim 9, wherein the combining the tetrachloroethylene solvent and the filter device comprises:

evaporating the tetrachloroethylene solvent; and

condensing the tetrachloroethylene solvent with a condenser into a chamber of the separating unit housing the filter device.

11. The method of claim 9, further comprising collecting the composition of the droplet fraction in a flask of the separating unit including directing a flow of the composition into the flask when a level of the composition within the separating unit reaches a predetermined height.

12. The method of claim 1, wherein the filter device is arranged within the breather pipe.

13. The method of claim 1, further comprising:

measuring at least one of a temperature, a pressure and a velocity of the oil mist flowing within the breather pipe; and

adjusting a diameter of an opening section of the collecting device based on the measuring step, such that an isokinetic flow of the oil mist enters the opening section.

14. The method of claim 1, further comprising guiding the gaseous fraction of the oil mist sample to a gaseous fraction analyzing unit to solely determine the gaseous fraction of the oil mist sample.

15. A system for analysing a droplet fraction of an oil mist sample of a gas turbine, the system comprising:

a collecting device for collecting the oil mist sample, wherein the collecting device is arrangeable within a breather pipe which is coupleable to the gas turbine such that oil mist is flowable through the breather pipe,

a filter device for separating the droplet fraction from a gaseous fraction of the oil mist sample, wherein the filter device is soaked with the droplet fraction, and

a spectrometer for analysing a composition of the droplet fraction which is extractable from the filter device by using a tetrachloroethylene solvent.

16. The system of claim 15, further comprising a Soxhlet extractor to extract the droplet fraction from the filter device with the tetrachloroethylene solvent.

17. The system of claim 15, wherein the collecting device is positioned within the breather pipe and includes an internal filter device positioned within the collecting device.

18. The system of claim 15, including a pair of collecting devices positioned within the breather pipe, said pair of collecting devices arranged with a predefined axial offset along a center axis of the breather pipe such that fluid characteristics of the oil mist at a respective opening section of the collecting devices is substantially identical.

19. A method for analysing a droplet fraction of an oil mist sample of a gas turbine, the method comprising:

collecting the oil mist sample by a collecting device, wherein the collecting device is arranged within a breather pipe which is coupled to the gas turbine such that oil mist is flowing through the breather pipe,

separating the droplet fraction from a gaseous fraction of the oil mist sample by a filter device, wherein the filter device is soaked with the droplet fraction,

extracting the droplet fraction from the filter device by using a non-flammable solvent, and

analysing a composition of the droplet fraction by a spectrometer.

20. The method of claim 19, wherein the extracting the droplet fraction from the filter device comprises:

positioning the filter device in a separating unit;

combining the solvent and the filter device within the separating unit to form the composition of the droplet fraction; and

collecting the composition of the droplet fraction in a flask of the separating unit.