Method and system for determining fluid density

• US 9,933,347 B2
• Filed: 09/15/2015
• Issued: 04/03/2018
• Est. Priority Date: 09/15/2014
• Status: Expired due to Fees

• Current Assignee: Universiteit Stellenbosch
• Original Assignee: Universiteit Stellenbosch
• Inventors: Pieterse, Cornelius Louwrens
• Primary Examiner(s): SMYTH, ANDREW P
• Application Number:
  US15/511,121
• Publication Number:
  US 20170276583A1
• Time in Patent Office: 931 Days
• Field of Search: None
• CPC Class Codes: B05B 5/0255 spraying and depositing by electrostatic forces only
• CPC Class Codes: G01N 27/002 by investigating the work function voltage
• CPC Class Codes: G01N 9/00 Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
• CPC Class Codes: G01N 9/24 by observing the transmission of wave or particle radiation through the material

Abstract

A method and system for determining a density of a fluid is provided. The method is carried out using an electrospraying apparatus connected in the system. At a first step fluid is introduced into an emitter of the electrospraying apparatus. A voltage is applied between the emitter and a counter-electrode spaced apart from the emitter for a number of intermittent time periods, wherein the duration of at least some of the time periods during which the voltage is applied progressively decreases. The current between the emitter and the counter-electrode is measured for each time period during which a voltage is applied and the shortest time period for which a current reading is obtained is recorded. The shortest time period is used to calculate the density of the fluid in the emitter.

Claims

1. A method of determining a density of a fluid, the method including the steps of:

introducing the fluid into an emitter of an electrospraying apparatus;

applying a voltage between the emitter and a counter-electrode spaced apart from the emitter for a number of intermittent time periods, wherein the duration of at least some of the time periods during which the voltage is applied progressively decreases;

measuring current between the emitter and the counter-electrode for each time period;

identifying and recording a shortest time period for which a current reading between the emitter and counter-electrode is obtained; and

calculating the density of the fluid as a function of the shortest time period.

2. The method as claimed in claim 1, wherein the density of the fluid is calculated using the function:

3. The method as claimed in claim 1, wherein the voltage applied between the emitter and the counter-electrode during time periods is sufficient to produce an electrospray of the fluid and wherein the voltage is reduced to a voltage that does not produce an electrospray of the fluid, or is switched off, in between the time periods.

4. The method as claimed in claim 1, wherein the time periods during which the voltage is applied start with an initial time period that is associated with a selected upper density limit so as to allocate sufficient time for electrospraying to occur.

5. The method as claimed in claim 1, wherein the duration of the time periods during which the voltage is applied decreases sequentially in a step-wise manner.

6. The method as claimed in claim 5, wherein the duration of the time periods during which the voltage is applied decreases in steps of 1 ms or less.

7. The method as claimed in claim 4, wherein the initial time period is associated with an upper density limit that is more than or equal to 2000 kg/m³.

8. A system for measuring a density of a fluid comprising an electro spraying apparatus having an emitter through which the fluid is drawn,

at least one counter-electrode spaced apart from the emitter, and

a voltage source configured to apply a voltage between the emitter and the counter-electrode to create an electrospray of the fluid from the emitter,

a device for measuring the voltage applied between the emitter and the counter-electrode and

a device for measuring the current flowing in the system as a result of electrospray of the fluid between the emitter and the counter-electrode and for measuring the current between the emitter and the counter-electrode for each time period;

wherein

a processing module in communication with at least the voltage source, the voltage measuring device and the current measuring device, is configured to operate the voltage source to apply a voltage between the emitter and the counter electrode for a number of intermittent time periods,

wherein the duration of at least some of the time periods during which the voltage is applied is progressively decreased, and

wherein the processing module is further configured to read the current measuring device, and to record the shortest time period for which a current reading between the emitter and the counter-electrode is obtained in the system; and

wherein the processor module or an external processor connectable to the processing module is configured to calculate the density of the fluid as a function of the shortest time period.

9. The system as claimed in claim 8, wherein the processing module is configured to calculate the density of the fluid as a function of the shortest time period.

10. The system as claimed in claim 9, wherein the function is:

11. The system as claimed in claim 8, wherein the voltage source is a programmable direct current voltage source.

12. The system as claimed in claim 8, wherein a software application is resident on the processing module and executable by the processing module to progressively decrease at least some of the time periods for which a voltage is applied.

13. The system as claimed in claim 12, wherein a software application is resident on the processing module and executable by the processing module to sequentially decrease the time periods in a step-wise manner, to stop decreasing the time period when a current is no longer detected by the current measuring device and to reduce the voltage to a voltage that does not produce an electrospray, or switch the voltage off, in between the time periods.

14. The system as claimed in claim 8 wherein the electrospray apparatus is configured to electrospray in air and under atmospheric conditions.

15. The system as claimed in claim 8, wherein the electrospray apparatus is configured to electrospray within an insulating gas and wherein at least the electrospray apparatus and the counter-electrode are located within a hermetically sealed container filled with the insulating gas.