Carbon nanostructure preblends and their applications
First Claim
1. A method for dispersing carbon nanostructures in a polymer comprising:
- wet-mixing in a liquid medium a blend comprising said carbon nanostructures and a particulate solid;
drying said blend to form a preblend of the carbon nanostructures and the particulate for adding to a polymer in a conventional compounding processwherein said preblend forms a core-shell structure comprising a shell of said carbon nanostructures coating a core comprising a particle of said particulate solid; and
wherein said particulate solid comprises polymer beads; and
wherein the carbon nano-structures comprise single-wall carbon nanotubes.
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Abstract
A method for preparing a “preblend” of nano-structured carbon, such as nanotubes, fullerenes, or graphene, and a particulate solid, such as polymer beads, carbon black, graphitic particles or glassy carbon involving wet-mixing and followed by optional drying to remove the liquid medium. The preblend may be in the form of a core-shell powder material with the nano-structured carbon as the shell on the particulate solid core. The preblend may provide particularly improved dispersion of single-wall nanotubes in ethylene-α-olefin elastomer compositions, resulting in improved reinforcement from the nanotubes. The improved elastomer compositions may show simultaneous improvement in both modulus and in elongation at break. The elastomer compositions may be formed into useful rubber articles.
1 Citation
23 Claims
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1. A method for dispersing carbon nanostructures in a polymer comprising:
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wet-mixing in a liquid medium a blend comprising said carbon nanostructures and a particulate solid; drying said blend to form a preblend of the carbon nanostructures and the particulate for adding to a polymer in a conventional compounding process wherein said preblend forms a core-shell structure comprising a shell of said carbon nanostructures coating a core comprising a particle of said particulate solid; and wherein said particulate solid comprises polymer beads; and wherein the carbon nano-structures comprise single-wall carbon nanotubes. - View Dependent Claims (2, 3, 4, 5, 10, 11, 12, 13, 14, 21, 22, 23)
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6. A method for dispersing carbon nanostructures in a polymer comprising:
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wet-mixing in a liquid medium a blend comprising said carbon nanostructures and a particulate solid; drying said blend to form a preblend of the carbon nanostructures and the particulate for adding to a polymer in a conventional compounding process wherein said preblend forms a core-shell structure comprising a shell of said carbon nanostructures coating a core comprising a particle of said particulate solid; wherein said particulate solid comprises polymer beads; and further comprising mixing said preblend into a polymer composition; wherein the primary polymer in the polymer composition is an ethylene-α
-olefin elastomer. - View Dependent Claims (7, 8, 9, 15, 16, 17, 18, 19, 20)
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Specification