Producing edible residues from ethanol production

• US 9,961,921 B2
• Filed: 04/05/2012
• Issued: 05/08/2018
• Est. Priority Date: 10/14/2009
• Status: Expired due to Fees

• Current Assignee: Xyleco, Inc.
• Original Assignee: Xyleco, Inc.
• Inventors: Medoff, Marshall
• Primary Examiner(s): Tate, Christopher R
• Assistant Examiner(s): Kosar, Aaron J
• Application Number:
  US13/440,107
• Publication Number:
  US 20120282379A1
• Time in Patent Office: 2,224 Days
• CPC Class Codes: A23K 10/30 from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms obtained by microbiological or biochemical processes, e.g. using yeasts or enzymes, A23K10/10
• CPC Class Codes: A23K 10/38 from distillers' or brewers' waste
• CPC Class Codes: A23L 5/30 Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation cooking A23L5/10
• CPC Class Codes: C08H 8/00 Macromolecular compounds derived from lignocellulosic materials pretreatment thereof B27N
• CPC Class Codes: Y02E 50/10 Biofuels, e.g. bio-diesel
• CPC Class Codes: Y02P 60/87 Re-use of by-products of food processing for fodder production

Abstract

Edible residues of ethanol production, e.g., distillers grains and solubles, are produced that are low in, or substantially free from, antibiotic residues. Antibiotics or bacteria present in edible residues resulting from ethanol production are inactivated by irradiating the edible residues.

Claims

1. A method of producing irradiated edible residues, the method comprising:

irradiating a feedstock comprising a cellulosic and/or lignocellulosic material with a dose of electron beam radiation sufficient to reduce the recalcitrance of the material;

bioprocessing the irradiated feedstock using a cellulolytic enzyme, wherein bioprocessing produces a sugar and edible residues; and

drying the edible residues and irradiating the edible residues with electron beam radiation, wherein the edible residues contain an antibiotic and the step of irradiating the edible residues is performed under conditions selected to inactivate or destroy the antibiotic.

2. The method of claim 1 wherein the bioprocessing comprises fermentation.

3. The method of claim 2 wherein the edible residues comprise distillers grains and solubles (DGS).

4. The method of claim 3 wherein the distillers grains and solubles have been dried, producing dried distillers grains and solubles (DDGS).

5. The method of claim 4 wherein drying is performed prior to irradiation of the edible residues.

6. The method of claim 1 wherein, after irradiation, the edible residues contain less than 100 ppm by weight of active antibiotic.

7. The method of claim 6 wherein, after irradiation, the edible residues are substantially free of active antibiotic.

8. The method of claim 1 wherein, prior to irradiation, the edible residues contain about 500 ppm to about 10,000 ppm by weight of active antibiotic.

9. The method of claim 1 wherein, prior to irradiation, the edible residues contain bacteria, and the irradiating of the edible residues is performed under conditions that destroy the bacteria.

10. The method of claim 9 wherein the bioprocessing is conducted without addition of antibiotics.

11. The method of claim 1, wherein irradiation of the edible residues is delivered at a dose of greater than about 0.5 Mrad.

12. The method of claim 1, wherein irradiation of the edible residues is delivered at a dose of less than about 5 Mrad.

13. The method of claim 1, wherein irradiation of the edible residues is delivered at a dose of from about 1 to about 3 Mrad.

14. The method of claim 1 wherein the dose is sufficient to reduce the recalcitrance by at least 25%.