Method and apparatus for measuring hydrogen-induced cracking

• US 10,788,461 B2
• Filed: 11/22/2016
• Issued: 09/29/2020
• Est. Priority Date: 11/27/2015
• Status: Active Grant

• Current Assignee: JFE Steel Corporation (JFE Holdings Incorporated)
• Original Assignee: JFE Steel Corporation (JFE Holdings Incorporated)
• Inventors: Mizuno, Daisuke, Ishikawa, Nobuyuki, Matsui, Yutaka, Yasuda, Kyono, Fujimoto, Koji, Sugimoto, Shigeaki
• Primary Examiner(s): Huls, Natalie
• Application Number:
  US15/778,012
• Publication Number:
  US 20180340913A1
• Time in Patent Office: 1,407 Days
• CPC Class Codes: G01N 2291/0234 Metals, e.g. steel
• CPC Class Codes: G01N 2291/0289 Internal structure, e.g. defects, grain size, texture
• CPC Class Codes: G01N 2291/2626 Wires, bars, rods
• CPC Class Codes: G01N 29/043 in the interior, e.g. by shear waves
• CPC Class Codes: G01N 29/0672 by acoustic tomography medical tomography A61B8/13
• CPC Class Codes: G01N 29/262 by electronic orientation or focusing, e.g. with phased arrays phased arrays per se G10K11/34
• CPC Class Codes: G01N 29/265 by moving the sensor relative to a stationary material
• CPC Class Codes: G01N 29/27 by moving the material relative to a stationary sensor
• CPC Class Codes: G01N 29/28 providing acoustic coupling , e.g. water impedance matching G10K11/02

Abstract

There are proposed a method for measuring hydrogen-induced cracking which can measure hydrogen-induced cracking initiated in an interior of a test specimen during HIC test and a measuring apparatus used in this method. When cracks initiated in an interior of a test specimen 1 immersed in a test solution 5 containing hydrogen sulfide is measured by an ultrasonic probe 2 placed in a vessel 3, the position and size of cracks initiated in the interior of the test specimen 1 are measured with the lapse of time at a state of immersing the test specimen 1 in the test solution by scanning the ultrasonic probe 2 or the test specimen 1.

Claims

1. An apparatus for measuring hydrogen-induced cracking, which comprises a vessel for housing a test solution containing hydrogen sulfide and immersing a test specimen, an ultrasonic probe placed in the test solution and immersed in the same test solution as the test specimen for transmitting an ultrasonic wave toward the test specimen and receiving a reflection echo from the test specimen, a scanning means for relatively scanning the ultrasonic probe and the test specimen every given time, and a visualizing means for visualizing cracks in the interior of the test specimen based on a signal received from the ultrasonic probe every scanning position.

2. The apparatus for measuring hydrogen-induced cracking according to claim 1, wherein the scanning means has a driving mechanism for moving the ultrasonic probe relatively to the test specimen or moving the test specimen relatively to the ultrasonic probe.

3. The apparatus for measuring hydrogen-induced cracking according to claim 2, wherein the driving mechanism comprises a driving shaft connected to the ultrasonic probe or the test specimen, a driving device placed outside the vessel, and a non-contact power-transmitting means for transmitting power of the driving device to the driving shaft at a distance from the vessel at a non-contact state.

4. The apparatus for measuring hydrogen-induced cracking according to claim 3, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

5. The apparatus for measuring hydrogen-induced cracking according to claim 2, which is provided with a bubble-removing means for removing bubbles attached to a measuring face of the test specimen.

6. The apparatus for measuring hydrogen-induced cracking according to claim 5, wherein the bubble-removing means is a brush fitted to the ultrasonic probe for utilizing a relative displacement between the ultrasonic probe and the test specimen by the driving mechanism to sweep a face of the test specimen irradiated with the ultrasonic wave.

7. The apparatus for measuring hydrogen-induced cracking according to claim 6, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

8. The apparatus for measuring hydrogen-induced cracking according to claim 5, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

9. The apparatus for measuring hydrogen-induced cracking according to claim 2, wherein the ultrasonic probe is a linear phased array probe constructed by one-dimensionally arranging a plurality of vibrators for transmitting and receiving an ultrasonic wave so as to scan electronically in a direction perpendicular to a scanning direction through the driving mechanism.

10. The apparatus for measuring hydrogen-induced cracking according to claim 9, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

11. The apparatus for measuring hydrogen-induced cracking according to claim 2, wherein the ultrasonic probe is tightly sealed in a case having a corrosion resistance to the test solution.

12. The apparatus for measuring hydrogen-induced cracking according to claim 11, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

13. The apparatus for measuring hydrogen-induced cracking according to claim 2, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

14. The apparatus for measuring hydrogen-induced cracking according to claim 1, wherein the ultrasonic probe is tightly sealed in a case having a corrosion resistance to the test solution.

15. The apparatus for measuring hydrogen-induced cracking according to claim 14, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

16. The apparatus for measuring hydrogen-induced cracking according to claim 1, wherein the visualizing means is constructed so as to obtain a plurality of ultrasonic tomographic images based on signals received from the ultrasonic probe every scanning position and synthesize the plurality of ultrasonic tomographic images to reconstruct a three-dimensional ultrasonic image of cracking in the interior of the test specimen.

17. A method for measuring hydrogen-induced cracking, the method comprising

immersing a test specimen in a test solution containing hydrogen sulfide inside a vessel;

and

measuring cracks initiated in the interior of the test specimen with an ultrasonic probe, wherein the ultrasonic probe is placed in the vessel and immersed in the same test solution as the test specimen and the test specimen and the ultrasonic probe are relatively scanned every given time to measure a position and size of the cracks initiated in the interior of the test specimen with time at a state of immersing the test specimen in the test solution.

18. The method for measuring hydrogen-induced cracking according to claim 17, wherein the scanning includes a mechanical scanning of moving the ultrasonic probe relatively to the test specimen or moving the test specimen relatively to the ultrasonic probe.

19. The method for measuring hydrogen-induced cracking according to claim 18, wherein a measuring face of the test specimen is arranged approximately vertically in the test solution.

20. The method for measuring hydrogen-induced cracking according to claim 17, wherein a measuring face of the test specimen is arranged approximately vertically in the test solution.