METHODS AND DEVICES FOR MONITORING OF FRYING OIL QUALITY

• US 20110051141A1
• Filed: 03/02/2009
• Published: 03/03/2011
• Est. Priority Date: 03/04/2008
• Status: Active Grant

• Current Assignee: 3M Innovative Properties Company (3M Company)
• Original Assignee: 3M Innovative Properties Company (3M Company)
• Inventors: Wei, Ai-Ping, Sabade, Milind Balwant, Mahmoodi, Abolghassem B.
• Granted Patent: US 8,325,345 B2
• Time in Patent Office: Days
• US Class Current: 356/445
• CPC Class Codes: G01N 21/78 producing a change of colour
• CPC Class Codes: G01N 31/22 using chemical indicators G01N31/02 takes precedence
• CPC Class Codes: G01N 33/03 Edible oils or edible fats

Abstract

Herein are disclosed methods and devices for evaluating the quality of oils (e.g., cooking oil or flying oil). The methods can provide an indication of the free fatty acid content of the oil. The methods use an optical interrogation device to provide an indication of free fatty acid based on quantitative measurements of optical reflectance from test zones on a sampling substrate.

Claims

1. A method of evaluating the quality of frying oil, the method comprising the steps of:

providing frying oil that potentially comprises free fatty acid content;

providing an oil-absorbent sampling substrate,

wherein the sampling substrate contains a plurality of test zones,

wherein each test zone is responsive to free fatty acid;

contacting the oil with the sampling substrate such that a sample of the oil is brought into contact with at least a portion of each of the test zones;

directing light onto the plurality of test zones;

measuring the amount of light reflected from each test zone;

generating signals proportional to the amount of light reflected from each test zone,

summing the signals together so as to provide an integrated signal;

correlating the integrated signal with the free fatty acid content of the oil;

and,

reporting an indication of the oil quality of the oil,

wherein the indication is associated with the free fatty acid content of the oil.

2. The method of claim 1 wherein a separate light source is used to direct light on each test zone.

3. The method of claim 2 wherein at least one of the separate light sources is a broadband light-emitting diode.

4. The method of claim 2 wherein at least one of the separate light sources is a light-emitting diode that emits light in the green wavelength range of from about 510 nm to about 586 nm.

5. The method of claim 2 wherein at least one of the separate light sources is a light-emitting diode that emits light in the red wavelength range of from about 586 nm to about 660 nm.

6. The method of claim 1 wherein a separate photodetector is used to detect light reflected from each test zone.

7. The method of claim 6 wherein the separate photodetectors are photodiodes.

8. A method of evaluating the quality of frying oil, the method comprising the steps of:

providing an interrogation device that comprises a plurality of light source/photodetector pairs;

providing an oil-absorbent sampling substrate,

wherein the sampling substrate contains a plurality of test zones,

wherein each test zone is responsive to free fatty acid;

providing frying oil that potentially comprises free fatty acid content;

contacting the oil with the sampling substrate such that a sample of the oil is brought into contact with at least a portion of each of the test zones;

positioning the interrogation device and the sampling substrate such that each light source/photodetector pair is placed in proximity to a test zone, so as to provide a plurality of light source/photodetector/test zone sets;

for each light source/photodetector/test zone set, directing light onto the test zone from the light source and measuring reflected light therefrom by the photodetector and generating a signal that is proportional to the measured reflected light;

combining the signals from the photodetectors so as to provide a combined signal;

correlating the combined signal with the free fatty acid content of the oil based on information stored in the interrogation device;

and,

reporting an indication of the oil quality of the oil, wherein the indication is associated with the free fatty acid content of the oil.

9. The method of claim 8 wherein combining the signals comprises summing the signals together to form an integrated signal.

10. The method of claim 8 wherein each light source/photodetector pair comprises a light source and a photodetector that are positioned within at most 10 mm from each other.

11. The method of claim 10 wherein for each light source/photodetector pair, the light source and the photodetector are positioned in a coplanar configuration and are mounted on a common circuit board.

12. The method of claim 11 wherein all of the light sources and photodetectors in the interrogation device are mounted on a common circuit board.

13. The method of claim 8, wherein the light source/photodetector pairs in the interrogation device are spatially arranged so as to correspond to the spatial arrangement of the test zones on the sampling substrate.

14. The method of claim 13 wherein, upon positioning the interrogation device and the sampling substrate such that each light source/photodetector pair is placed in proximity to a test zone, all of the test zones are interrogated without moving the sampling substrate and the interrogation device relative to each other.

15. The method of claim 8 including the step in which the interrogation device verifies that the sampling substrate is compatible with the interrogation device.

16. A system for evaluating the quality of frying oil, the system comprising:

an oil-absorbent sampling substrate,

wherein the sampling substrate contains a plurality of test zones,

wherein each test zone is responsive to free fatty acid;

and,

an optical interrogation device that comprises a plurality of light source/photodetector pairs;

wherein the interrogation device and the sampling substrate are configured such that each light source/photodetector pair can be placed in proximity to a test zone, so as to provide a plurality of light source/photodetector/test zone sets;

wherein the interrogation device and the sampling substrate are further configured such that, for each light source/photodetector/test zone set, each test zone can be optically interrogated by the light source/photodetector pair so as to receive a signal therefrom, without moving the interrogation device and the sampling substrate relative to each other;

and,

wherein the interrogation device comprises means to combine the signals received from the test zones into a combined signal, means to correlate the combined signal with the free fatty acid content of the oil, and means to report an indication of the oil quality of the oil, wherein the indication is associated with the free fatty acid content of the oil.

17. The system of claim 16 wherein the sampling substrate comprises a mark.

18. The system of claim 17 wherein the mark can be identified by the interrogation device and the presence of the mark used by the interrogation device to verify that the sampling substrate is compatible with the interrogation device.

19. The system of claim 17 wherein the mark can be used by the interrogation device to determine whether the sampling substrate is aligned correctly with the interrogation device such that the test zones are in proximity to the light source/photodetectors pairs such that the test zones can be interrogated.

20. The system of claim 16 wherein all of the light sources and photodetectors in the interrogation device are mounted on a common circuit board.