Separation of fluid cracking catalyst particles from gaseous hydrocarbons

• US 4,455,220 A
• Filed: 12/23/1982
• Issued: 06/19/1984
• Est. Priority Date: 12/23/1982
• Status: Expired due to Term

• Current Assignee: Shell Oil Company (Shell Plc)
• Original Assignee: Shell Oil Company (Shell Plc)
• Inventors: Dewitz, Thomas S., Gwyn, John E., Hardesty, Donald E., Parker, Wesley A., Bilgic, A. Haluk, Hinds, George P. Jr.
• Primary Examiner(s): Gantz, Delbert E.
• Assistant Examiner(s): MCFARLANE, ANTHONY R
• Application Number:
  US06/452,599
• Time in Patent Office: 544 Days
• Field of Search: 208/153, 208/161, 208/164, 55/394, 55/426, 55/459 R
• US Class Current: 208/161
• CPC Class Codes: B01J 8/0055 using cyclones
• CPC Class Codes: B04C 2009/004 with internal filters, in the cyclone chamber or in the vortex finder
• CPC Class Codes: B04C 5/103 Bodies or members, e.g. bulkheads, guides, in the vortex chamber cores B04C5/107
• CPC Class Codes: B04C 9/00 Combinations with other devices, e.g. fans, expansion chambers, diffusors, water lockswith filters B01D50/00

Abstract

Catalyst and hydrocarbon vapors are separated in a cyclone zone attached to the discharge of a riser cracking operation. Vortex stabilizing means separating the cyclone zone from a stripping zone allows stripping gas from said stripping zone to be passed upwardly into said cyclone zone countercurrent to the downward flow of catalyst, thereby improving the separation and stripping of gaseous hydrocarbons from separated catalyst. The combined cyclone-stripping zone reduces catalyst hydrocarbon contact time, thereby improving gasoline yield and olefin content, decreasing gas make, and reducing coke deposits.

Claims

1. A method for separating fluid cracking catalyst particles from hydrocarbon conversion products and stripping interstitial and adsorbed hydrocarbon gases therefrom which comprises passing a suspension of catalyst and gaseous hydrocarbons upwardly through a riser conversion zone in a fluid catalytic cracking process under elevated temperature conversion conditions;

passing said suspension from said riser conversion zone into the upper portion of a separator-stripper vessel containing a gas/solids tangential inlet, a swirl zone, a cyclone zone, a vortex outlet, vortex stabilizing means, a catalyst disengaging space and a fluidized bed of catalyst;

forming a fluid vortex in said swirl and cyclone zones from which a cyclonic separation is made between catalyst particles and gaseous hydrocarbon conversion products;

centering the tip of said fluid vortex by contact with said vortex stabilizing means having a diameter of about one vortex outlet diameter or greater and being coaxially located at the bottom of said cyclone separation zone;

defining the length of said cyclone separation zone by spacing said stabilizing means at least about two vortex outlet diameters below the bottom of said vortex outlet, which comprises an open ended vertical coaxial passageway extending from the upper portion of the separator vessel downwardly through said swirl zone to the top of said cyclone zone;

removing separated gaseous hydrocarbon conversion products from the upper portion of the cyclone zone through said vortex outlet;

passing separated catalyst through an annulus formed by the perimeter of said stabilizing means and the separator wall into a lower stripping zone which is in gaseous communication with the cyclone zone, said annulus being sufficiently wide to permit catalyst passage downwardly while simultaneously passing stripping gas in an upwardly direction;

contacting said catalyst with from about 1 to 4 pounds of stripping gas per 1000 pounds of catalyst as it passes downwardly through said annulus and a stripping zone, which includes a catalyst disengaging space, to the fluidized catalyst bed contained within said separator-stripper vessel, the length of said stripping zone being defined as the distance from the stripping gas/catalyst bed contact zone to said vortex stabilizer means, said distance being sufficient to provide disengaging height between the top of said fluidized catalyst bed and the bottom of said stabilizing means so as to avoid slugs of catalyst carryover into said cyclone zone.

2. The method of claim 1 wherein the vortex stabilizing means comprises a solid disk or plate.

3. The method of claim 2 wherein the stabilizer means has attached to the center thereof and extending upwardly into the cyclone zone a vortex finder rod.

4. The method of claim 3 wherein the length of said vortex finder rod is at least one-third the vortex length.

5. The method of claim 1 wherein the vortex stabilizer means includes an open axial passageway through which gas flows from the stripping zone to the core of said vortex in the cyclone zone.

6. The method of claim 5 wherein the stabilizer means comprises a solid disk or plate.

7. The method of claim 6 wherein the stabilizer means has attached thereto an axial upwardly extending vortex finder rod.

8. The method of claim 7 wherein the length of said vortex finder rod is at least one third the vortex length.

9. The method of claim 1 wherein the stripping gas superficial velocity ranges from about 0.2 to about 0.9 feet per second.

10. The method of claim 9 wherein the stripping gas is steam.