Process for removing magnetic particles from a suspension of solids in a liquid

• US 4,784,758 A
• Filed: 08/27/1986
• Issued: 11/15/1988
• Est. Priority Date: 08/27/1986
• Status: Expired due to Fees

• Current Assignee: Engelhard Corporation (BASF SE)
• Original Assignee: Engelhard Corporation (BASF SE)
• Inventors: Willis, Mitchell J.
• Primary Examiner(s): Reeves, Robert B.
• Assistant Examiner(s): Hajec, Donald T.
• Application Number:
  US06/900,666
• Time in Patent Office: 811 Days
• Field of Search: 209/3, 209/214, 209/215, 209/5, 209/223.1, 209/228, 209/232, 209/225, 210/222, 210/223, 210/695, 210/793, 210/794, 210/798, 134/95, 134/98, 134/99
• US Class Current: 209/214
• CPC Class Codes: B03C 1/032 Matrix cleaning systems

Abstract

A process which is especially useful for effecting magnetic separation of magnetically attractable impurities from an aqueous clay slurry or suspension includes passing the suspension through a porous, ferromagnetic matrix while applying a magnetic field to the matrix, on which impurities are collected, and thereafter regenerating the matrix by flushing collected impurities therefrom with a flush liquid, e.g., water. The improvement comprises, after discontinuing the passage of the suspension through the matrix, but before passing flush liquid therethrough, admitting a pressurized gas, e.g., compressed air, into the separator to displace suspension retained therein, and recovering the displaced suspension. In addition, flush liquid retained in the matrix after the flushing step may be displaced therefrom by the compressed air. By displacing the retained suspension from the matrix with, e.g., compressed air, instead of a flush liquid, e.g., water, the retained suspension is not diluted by flush water and is recovered instead of sewered as in the prior art processes.

Claims

1. A method for effecting wet magnetic separation of magnetically attractable particles from a suspension of solids in a liquid vehicle, including periodic flushing of a matrix on which such particles are collected, the method comprising the steps of:

(a) passing the suspension containing the magnetically attractagle particles upwardly through a stationary ferromagnetic matrix while applying a magnetic field to the matrix to collect the particles on the matrix, the matrix having the property of retaining said suspension therein after discontinuation of its passing through the matrix;

(b) after conducting step (a) for a selected treatment period, maintaining the magnetic field applied to the matrix while discontinuing the passing of the suspension through the matrix and passing a pressurized gas downwardly through the matrix to displace retaining suspension from the matrix;

(c) after step (b), discontinuing the magnetic field and flushing the matrix by passing a flush liquid therethrough in the absence of the magnetic field to flush collected particles from the matrix, the matrix also having the property of retaining said flush liquid therein after discontinuation of its passing through the matrix, and thereafter passing a pressurized gas downwardly through the matrix to displace retained flush liquid therefrom;

(d) recovering the displaced suspension of step (b); and

(e) repeating the above steps for a plurality of cycles.

2. The method of claim 1 wherein the matrix comprises a body of filamentary, ferromagnetic metal.

3. The method of claim 1 wherein the suspension is an aqueous suspension of clay particles.

4. The method of claim 3 wherein the clay particles comprise kaolin clay particles and the impruities comprise colorant impurities naturally occurring in the clay.

5. The method of claim 1 wherein the flush liquid is water.

6. The method of claim 1 wherein the pressurized gas is air.

7. The method of claim 1 wherein the flush liquid is water and the pressurized gas is air.

8. The method of claim 1 wherein the pressurized gas comprises air at a pressure of from about 8 to 18 psig.

9. The method of claim 8 wherein the pressurized air is at a pressure of from about 10 to 15 psig.

10. The method of claim 8 wherein the pressurized air is at a pressure of about 13 psig.

11. The method of claim 1 wherein the intensity of the magnetic field applied to the matrix is from about 5 to 30 kilogauss.

12. The method of claim 11 wherein the intensity of the magnetic field is from about 8.5 to 20 kilogauss.

13. The method of claim 11 wherein the intensity of the magnetic field is about 16 kilogauss.