Method for fiber loading a chemical compound
First Claim
1. A method for loading cellulosic fibers with calcium carbonate comprising:
- (a) providing a cellulosic fibrous material comprising a plurality of elongated fibers having a fiber wall surrounding a hollow interior, said fibrous material having moisture present at a level sufficient to provide said cellulosic fibrous material in the form of dewatered crumb pulp;
(b) adding a chemical selected from the group consisting of calcium oxide and calcium hydroxide to said pulp in a manner such that at least some of said chemical becomes associated with the water present in said pulp; and
(c) contacting said cellulosic fibrous material with carbon dioxide while subjecting said cellulosic fibrous material to higher shear mixing so as to provide a cellulosic fibrous material having a substantial amount of calcium carbonate loaded within the hollow interior and within the fiber walls of the plurality of cellulosic fibers.
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Abstract
The present invention relates to a method for loading a chemical compound within the fibers of a fibrous material and to the fibrous materials produced by the method. In the method, a fibrous cellulose material is provided which consists of a plurality of elongated fibers having a fiber wall surrounding a hollow interior. The fibrous material has a moisture content such that the level of water ranges from 40-95% of the weight of the fibrous material and the water is positioned substantially within the hollow interior of the fibers and within the fiber walls of the fibers. A chemical is added to the fibrous material in a manner such that the chemical is disposed in the water present in the fibrous material. The fibrous material is then contacted with a gas which is reactive with the chemical to form a water insoluble chemical compound. The method provides a fibrous material having a chemical compound loaded within the hollow interiors and within the fiber walls of the plurality of fibers.
171 Citations
20 Claims
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1. A method for loading cellulosic fibers with calcium carbonate comprising:
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(a) providing a cellulosic fibrous material comprising a plurality of elongated fibers having a fiber wall surrounding a hollow interior, said fibrous material having moisture present at a level sufficient to provide said cellulosic fibrous material in the form of dewatered crumb pulp; (b) adding a chemical selected from the group consisting of calcium oxide and calcium hydroxide to said pulp in a manner such that at least some of said chemical becomes associated with the water present in said pulp; and (c) contacting said cellulosic fibrous material with carbon dioxide while subjecting said cellulosic fibrous material to higher shear mixing so as to provide a cellulosic fibrous material having a substantial amount of calcium carbonate loaded within the hollow interior and within the fiber walls of the plurality of cellulosic fibers. - View Dependent Claims (2, 3, 4, 5, 6, 7, 8, 9, 10)
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11. A method for making a filled paper from cellulose fibers having tubular walls and lumens which contain precipitated calcium carbonate comprising:
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(a) providing cellulose fibers containing water; (b) adding a chemical selected from the group consisting of calcium hydroxide and calcium oxide to the cellulose fibers; (c) contacting said fibers with carbon dioxide gas while subjecting said fibers to high shear mixing so that there is a reaction with the chemical to form precipitated calcium carbonate both in the interior of the fibers and in the fiber walls; and (d) forming paper from said fibers. - View Dependent Claims (12, 13, 14, 15, 16, 17, 18, 19, 20)
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Specification